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Residual monomer of the four groups is far lowest than ISO standardization. Groups of traditional mixing are lower than the malaxation ones. Group of traditional mixing+ hot water polymerization is lower than group of malaxation + electrical heat-polymerization .

4,残余单体含量四组均远远低于标准中所要求的值2.2%,常规混合组残单含量小于捏炼混合组,两者有显著性差异( P<0.05),常规混合组+水浴固化组的残单含量低于捏炼混合组+电加热固化组(1:4 P<0.05)。

The method adopts the following steps: after mixed, phosphorus source, silicon source, aluminum source, an organic template agent, water and a precursor of the SAPO molecular sieve are hydrothermally crystallized for at least 0.1 hour at the temperature ranging from 110 to 260 DEG C to obtain the SAPO molecular sieve; wherein, the preparation method for the precursor of the SAPO molecular sieve has the following steps:, the molar ratio is 0.03 to 0.6 R:(Si0.01 to 0.98: Al 0.01 to 0.6: P0.01 to 0.6): 2 to 500 H2O; wherein, R stands for mixture solution of raw materials which is blended by the phosphorus source, the silicon source, the aluminum source, the an organic template agent and water of the template agent;, the mixture solution of raw materials prepared in step reacts at the temperature which is at least 50 DEG C lower than the crystallization temperature for at least 0.1 hour.

本发明通过采用包括以下步骤:将磷源、硅源、铝源、有机模板剂、水和SAPO分子筛前驱体混合后在110~260℃的温度下水热晶化至少0.1小时获得SAPO分子筛;其中SAPO分子筛的前驱体的制备包括以下步骤:将摩尔配比为0.03~0.6R∶(Si0.01~0.98∶Al0.01~0.6∶P0.01~0.6)∶2~500H 2 O,式中R代表模板剂的磷源、硅源、铝源、有机模板剂和水混合成原料混合液;将步骤制备的原料混合液在低于晶化温度至少50℃的温度下反应至少0.1小时的技术方案较好地解决了该问题,可应用于含氧化合物制烯烃催化剂的制备过程。

ABSTRACT Objective To discuss the clinical pathologic features and differential diagnosis of mixed germ cell sex cord stromal tumorwith malignant variant of germ cell tumor Methods The clinical pathologic datum and immunophenotype were studied in the case of ovary MGCSCST with malignant variance of germ cell tumor Results The patient's genital anatomy and female phenotype were normal,karotypes was 46xx with uterogestation The tumor tissue consisted of mixed germ cells and sex cord stromal cells with evident malignancy of mixed germ cells There was no atypical structure of gonadoblastoma in tumor tissue Conclusion MGCSCSST has complex morphosis,thus,to prevent misdiagnosis,more samples should be collected and more slices be cut The patient may have prognosis malo when there are high malignant variants of mixed germ cells in tumor tissue

目的 探讨混合性生殖细胞性索间质肿瘤(mixed germ cell sex cord stromal tumor,MGCSCST)伴恶性生殖细胞肿瘤变异型的临床病理特点及鉴别诊断。方法卵巢MGCSCST伴恶性生殖细胞肿瘤变异型的病例进行临床病理特征和免疫表型分析。结果患者生殖器的解剖结构和女性表型正常,染色体组型是46xx,足月妊娠。肿瘤组织由混合性生殖细胞和性索间质肿瘤构成,混合性生殖细胞有显著的恶性特征。瘤组织中没有典型的性腺母细胞瘤结构。结论 MGCSCST有复杂的形态结构,因此更多的取材和切片可以防止误诊,当肿瘤组织中的混合性生殖细胞有高度恶性变异时,患者预后不良。卵巢肿瘤;生殖细胞性索间质肿瘤;免疫组织化学

Tests on road performance of SMA mixture with terylene long fiber and xylon fiber were conducted at both high temperature and low temperature. It was found that the resistances of lignin fiber to asphalt run-off, deflection at high temperature, and water damage were higher than those of terylene long fiber, while the effects of lignin fiber and terylene long fiber on anti-dispersion loss performance and anti-cracking performance at low temperature were basically similar.

通过沥青混合料路用性能试验,研究了涤纶长纤维与木质素纤维对SMA混合料高、低温等路用性质影响,发现同等掺量情况下,木质素纤维对SMA混合料抗析漏性能、抗高温变形性能和抗水损害的贡献好于涤纶长纤维;而二者对混合料的抗飞散损失性能和低温抗裂性能的影响基本相同。

Authors designed four mixtures of dense-graded asphalt stabilized macadam base with the method recommended by Technical Specifications for Construction of Highway Asphalt Pavement, Superpave design method, coarse aggregate voids filling method and Bailey method separately, and determined the pavement performances of asphalt stabilized macadam base mixture under the optimal oil-stone rate which include resistance capacity to vertical deformation and fatigue. Then, four design methods were compared and appraised. Based on the above study, a new asphalt-stabilized macadam base mixture gradation design method-five control sieve design method was put forward.

分别采用现行规范推荐法、Superpave法、主骨架空隙体积填充法和贝雷法设计了4种密级配沥青稳定碎石基层混合料,然后采用力学指标设计法确定了所设计的4种级配沥青稳定碎石基层混合料的最佳油石比,并对最佳油石比下的沥青稳定碎石基层混合料进行了抗永久变形性能和抗疲劳性能等路用性能的研究;根据设计过程和设计结果对4种级配设计方法进行了比较评价,在此基础上提出了新的密级配沥青稳定碎石基层混合料的级配设计方法-五控制点级配设计方法。

Authors designed four mixtures of dense-graded asphalt stabilized macadam base with the method recommended by Technical Specifications for Construction of Highway Asphalt Pavement,Superpave design method,coarse aggregate voids-filling method and Bailey method separately,and determined the pavement performances of asphalt stabilized macadam base mixture under the optimal oil-stone rate which include resistance capacity to vertical deformation and fatigue.

分别采用现行规范推荐法、Superpave法、主骨架空隙体积填充法和贝雷法设计了4种密级配沥青稳定碎石基层混合料,然后采用力学指标设计法确定了所设计的4种级配沥青稳定碎石基层混合料的最佳油石比,并对最佳油石比下的沥青稳定碎石基层混合料进行了抗永久变形性能和抗疲劳性能等路用性能的研究;根据设计过程和设计结果对4种级配设计方法进行了比较评价,在此基础上提出了新的密级配沥青稳定碎石基层混合料的级配设计方法——五控制点级配设计方法。

The quadratic regression orthogonal rotary method was adopted to study the offect of three different mixing homogeneity : mixing time, block coefficient and rotary speed of the paddle shaft, also study the dominant effect, the single effect and interactive effect.

通过二次回归正交旋转组合试验,对影响翻转式双轴桨叶混合混合均匀度的3个因素(混合时间、充满系数及桨叶轴转速)以及对混合的主效应、单因素效应、两因素间的交互效应进行了分析,并且得出了各因素水平间的最佳组合工艺。

For understanding the workability and precision of these prediction equations, at first this study not only simulates the MHs of Taipei, Taichung, Kaoshung cities and Kao-ping area but also compares these results with meteorological models of CLAMET and TPAQM. And the comparisons show the high correlation (up to 0.8) between them. When the results of MH prediction equations model are compared with TPAQM, they get higher or lower values than TPAQM. The reasons are that Holzworth method can not concern about the warm and cold advections effect and the upper air data used do not get enough finer space-spread. About the results spread on the domain of my model, they show more different MH fields between the land and the sea around and get more sharply change of the land MHs on daytime than TPAQM.

为了解此预测式之可行性及准确度,本研究针对台北、台中、高雄及高屏地区作混合层高度值的模拟,并将模拟结果与实际观测值、CALMET气象模组及光化学轨迹模式输出结果作比对,结果显示均有0.80以上之高相关性;但与TPAQM计算结果间有明显的高估或低估现象,此为Holzworth method无法考量温度平流效应对混合层发展之影响及探空资料空间解析度不足所致;而在空间分布上,本模式所计算的混合层高度场相较於TPAQM在海陆分布上有较明显的分野,且更能够显示出内陆地区混合层高度的日变化。

The influence of the inlet solution concentration, solution flow rate, inlet air flow rate and temperature, air humidity on the absorbed process were studied for different liquid desiccants (calcium chloride, lithium chloride and calcium chloride mixture), and the dehumidifying effects of various mixture ratios on lithium chloride and calcium chloride mixture were also analyzed. The results show that the CELD (Cost-Effective Liquid Desiccant, the mixture ratio is 1:1) is more economical than pure lithium chloride solution, while its dehumidifying performance is better than calcium chloride solution.

针对不同的实验工质:氯化钙溶液、不同混合比的氯化钙和氯化锂混合溶液,研究了除湿器入口溶液浓度、入口空气流量、溶液流量及空气入口温度、湿度变化对除湿器除湿量的影响;以及氯化钙和氯化锂的混合质量比分别为1:1.5、1:1、1.5:1时的除湿效果;实验结果表明:用氯化钙和氯化锂混合质量比为1:1时的除湿溶液代替氯化锂溶液能节省费用,同时也改善了用纯氯化钙浓溶液作除湿剂时的除湿性能。

As a result, some ideas about the fabrication are put forward.The EPMA experiment results show that the main element such as W, Mo, Ti, Ni, Cu, Fe element are changed gradually in W-Mo and W-Mo-Ti FGM. In the layer rich in W, the grain are intervained and are mixed mechanismly. The same is to the layer rich in Mo and W-Mo. These grain felt up by some sinter. In Mo-Ti layer rich in Mo, the grains are also mixed mechanismly. Ni, Cu, Fe element assembled at interface. Ni melt by Cu plays an vital role in sinter effect. The microstructure characteristics result show that the compactness of W-Mo and W-Mo-Ti FGM is good.

电子探针实验结果表明W-Mo系、W-Mo-Ti系梯度功能材料中主要元素W、Mo、Ti、Ni、Fe、Cu分布整体上具有梯度变化规律,发现富W区、富Mo区、W-Mo混合区中颗粒交错分布,基本上以机械混合的形式存在,颗粒之间主要靠烧结剂的粘结作用实现致密化;以Mo为主要组分的Mo-Ti混合区,也是以机械混合的形式存在;Cu溶解于Ni形成固溶体更好地起到活化烧结能力,Ni、Cu、Fe在宏观层间界面富集,有利于烧结致密化。

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