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The isothermally crystallized films of the low temperature fractions of the two PPEs possess the similar crystalline morphology, i. e., thinner and high content of cross-hatching lamellae. The main reason to create the different crystallization behavior between the two PPEs and their fractions was due to the different distribution of the copoymerized ethylene unit.

对于分级样品,PPE1和PPE2高温级份的结行为差别较大:PPE1的高温级份结时形成的片较厚并且交叉片的数量也较低,剪切时产生较多纤维;两个样品的低温级份结形态类似,即结时形成的交叉片的含量都较高,剪切产生纤维数量差不多。

Probably, during the formation of spherical Au nanocrystals, PVP or PAM can be selectively adsorb on certain crystal planes of Au nanocrystals by the complexing effect between N or O with Au atom, thus leading to the different growth rates at different crystal planes of spherical Au nanocrystals and resulting in the formation of faceted Au nanocrystals and Au nanoplates.

研究表明,多面体和片状Au纳米是由球形Au纳米转变而来,这个转变是由于在球形Au纳米的形成过程中,PVP和PAM借助于其特有的N原子和O原子吸附到Au纳米的Au原子上,造成了体不同面生长速率的差异而导致的结果。

Cu6Zr5, the basic cluster of the primary devitrification phase of Cu-based amorphous alloys, is selected as cluster model based the on structure heredity existing between amorphous alloys and primary devitrification phases.

根据非与其化相存在结构遗传关系,以Cu-Zr基非化相Cu10Zr7中的Cu6Zr5阿基米德反棱柱为团簇模型,利用离散变分方法从电子层次研究了Al元素对Cu基非合金团簇稳定性的影响。

The Fe57-xCo18Nb4Al2Si4B15Smx(x=0-3) amorphous alloy ribbons were prepared byvacuum arc melting and melt spinning. The influences of Sm addition on the glass forming ability, thermal stability, crystallization behavior and magnetic properties of Fe57-xCo18Nb4Al2Si4B15Smx amorphous alloys were studied by X-ray diffraction, differential thermal analyzer and vibration sample magnetometer survey.

摘 要:采用真空电弧熔炼和真空熔融甩带法制备Fe57-xCo18Nb4Al2Si4B15Smx(x=0~3)非合金,借助X射线衍射、差热分析以及振动样品磁强计等手段研究稀土元素Sm对制备合金的非形成能力、非热稳定性、非化行为以及磁性能的影响。

Nd and Y showed more evident effects than Gd and La due to lower temperature of eutectic reaction with aluminum. In order to investigate mechanism of the formation of the intercellular dispersoid which is being in debate and possibility of suppressing the dispersoid, a nucleation kinetic model which including unsteady nucleation and effect of alloy element was established.

Al-Fe-Mo-Si-Zr-Ti合金粉末具有四种凝固组织,初生Al〓〓,α-Al与Al〓共,胞及显微胞,合金元素Mo的加入,显著提高合金粉末凝固前的过冷度,使10~40μm粉末的凝固机制发生了变化,由导热控制型转变成溶质扩散控制型,从而基本上消除了该尺寸范围内粉末凝固组织中共成分和初生相,但对大于40μm的粉末,因共区富Zr核心的优先形成而使Mo的作用效果不明显。

This invention discloses a preparation method for anti-corrosion rare earth magnet material characterizing that it takes the optimized grain-boundary phase design as the starting point on the basis of a dual alloy method to select Nd base alloy with high crystal forming ability as the assist alloy and reduces the temperature of the press mold blank in a quartz container to room temperature from over grain-boundary phase melting point with the water extraction way to get enough cooling rate and guarantee the non-grain-boundary phase, compared with the material of the same composition prepared by ordinary method, the weightlessness of this invented material reduces over 30% after testing the weightlessness of the material by laying it for 96 hours under 121deg.C, 2 atmosphere and 100% humid environment to show the advanced performance of anti-corrosion.

本发明公开了一种耐腐蚀稀土永磁材料的制备方法,其特征是它在双合金法制备工艺的基础上,以优化界相设计为出发点,选取具有较高非形成能力的Nd基合金为辅合金,并在烧结回火时将置于耐高温石英容器中的压型坯件,从界相熔点以上以水淬冷却的方式降温至室温,以达到足够的冷却速率,确保得到非界相,根据本发明制得的耐腐蚀稀土永磁材料,通过测量在121℃、2个大气压以及100%湿度环境下放置96小时后材料的失重情况,结果显示本发明得到的材料与常规方法制备的相同成分的稀土永磁材料相比失重减少了30%以上,充分证明其具备了更优越的耐腐蚀性能。可广泛应用于电子、汽车、计算机、电力、机械、能源、环保、国防、医疗器械等领域。

According to the experimental observations from Fujiwara et al, when the undercooling is low enough, the (111) silicon will be the dominant orientation in the polycrystalline silicon. As the undercooling becomes much higher, the (100) will be the dominant orientation.

根据Fujiwara等人所进行的矽粒竞争生长实验,当过冷度很小时,生长出的多矽中,(111)向的矽占了大多数;然而在过冷度较大时,(100)向的矽则为多数。

The results show that the microstructures of MMCs layer presents a hypereutectic structure.

结果表明:熔注层基体的微观组织为过共组织;熔注层不同位置的过共相具有不同的形貌,熔池上部主要为含有十字花状、鱼骨状、蝶状先共相W(下标 1-xAlC的过共组织,而底部的先共相呈现块状形态。

In order to reach the purpose of using pre-laser cladding method preparation of Ni-based amorphous alloy coatings on 45 steel substrate surface by the method was carried out. The principles of the three clusters and the amorphous line of the law of composition rules were used. The Ni59.35Nb34.45Sn6.2 alloying powder which has a great glass-forming ability in conventional preparation methods of amorphous alloys was chosen. In the protection of atmosphere, the amorphous surface coating was prepared. The microstructure, micro-hardness and performance of the different output power of the laser cladding were analyzed.

中文摘要:为了达到研究预置激光熔覆可以在45钢上制备Ni基非合金涂层的目的,采用非形成能力三判据原则及非成分团簇线定律法则,选择了采用常规非合金制备方法中具有极大玻璃形成能力的Ni59.35Nb34.45Sn6.2合金粉末,在保护气氛下,制备非涂层,并对不同输出功率下得到的涂层进行微观组织和结构表征及性能测试。

Liaoning Cando Microcrystal Glass Co., Ltd. is a high new technique enterprises together with development and production of Micorc rystal Glass.

辽宁德微玉石有限公司是一家集微石技术研发和产品生产为一体的高新技术企业,采用清华大学的专利技术,生产德微玉石系列产品。

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