可结晶性

The results show that AREEC liquid crystal enables the flow behavior of PC to change from quasi-Newtonian type to pseudo-plastic type, and it can act as heterogeneous nuclei to accelerate greatly crystallization of PET, and then to improve evidently their injection moldability.

将AREEC液晶与PC、PET熔体共混，研究了共混体系的流变行为、结晶特性和可模塑性，证明AREEC液晶能使PC流变行为由准牛顿型变为假塑性幂律型，能对PET起异相成核和显著加速结晶作用，从而大大改善它们的注塑可塑模性。

The results showed that compared with traditional fluorite and phosphorous slag, phosphorous slag composite mineralizer was effective on reducing amount of f-CaO in cement clinker and improving burnablity of raw meals, but the effect was still obvious when sintering temperature and sintering time were increasing. The analysis of XRD, SEM and petrographic structure showed that phosphorous slag composite mineralizer decreased viscosity of liquid, promotes the formation of Alite in clinker and improves crystal form and size of minerals.

结果表明，与传统的萤石和磷渣矿化剂相比，磷渣与萤石复合的矿化剂可有效降低水泥熟料中游离氧化钙的含量，改善生料的易烧性；在燃烧温度与时间增加的情况下，改善作用仍然明显；通过XRD、SEM与岩相结构分析表明，磷渣与萤石的复合矿化剂降低了液相的粘度，促进了A矿的生长，对矿物的结晶形态有改善作用，有利于晶体尺寸的生长发育。

This work, concentrated on the asymmetric allylation of aldehydes controlled by different chiral auxiliaries prepared from rotational pure tartaric acid, can be divided into three parts.The first part aims to review the developments of chiral drugs and asymmetric synthesis, from which derived the present research topic backgrounds and works.Synthesis and applications of allylation from aldehydes are the second part of the thesis. By optimizing the reaction conditions, such as solvents, temperature, time and chiral auxiliaries like N,N\'-dibenzyl tartamide, N,N\'-p-dimethylphenyl tartamide, N,N\'-o-dimethylphenyl tartamide, N,N\'-o-dichlorophenyl tartamide, N,N\'-a-dinaphyl tartamide, N,N\'-dicyclohexyl tartamide and N,N\'-diphenyl tartamide, ideal experimenttal conditions are obtained according to HPLC monitoring, as well as the auxiliaries\' recoveries experiments. Starting from benzaldehyde and 3-bromopropaldehyde, N,N\'-dibenzyl tartamide is considered the best auxiliary in this reaction.

本文介绍了醛的不对称烯丙基化反应，以光学纯酒石酸为原料，研究了不同构型手性配体在醛的烯丙基化反应中的立体选择性，全文共分三部分十个章节：第一部分对当前手性药物和手性技术进行了概述，并由此展开了本文的研究背景和任务；第二部分为有机合成部分，对醛的不对称烯丙基化反应进行了深入探讨，以苯甲醛为原料对反应条件进行优化，在优化的反应条件下对制备的七种可回收手性酰胺配体(N-苄基酒石酸二酰胺、N-对甲苯基酒石酸二酰胺、N-邻甲苯基酒石酸二酰胺、N-邻氯苯基酒石酸二酰胺、N-a-萘基酒石酸二酰胺、N-环己基酒石酸二酰胺和N-苯基酒石酸二酰胺)进行筛选，优化配体回收实验条件，最终确定出N-苄基酒石酸二酰胺在苯甲醛的不对称烯丙基化反应中具有较大优越性，结晶回收的手性配体光学纯度保持不变。

No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8％, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

在扫描电子显微镜下观察，在微球内外未发现尼群地平的完整结晶，X-射线粉末衍射和差示扫描量热试验结果也显示，尼群地平已经被高度分散在微球中；微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制；制备温度和搅拌速度对微球的质量影响较大；溶出仪的搅拌速度，释放介质的浓度和pH对微球的释放有较大的影响；制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显；方程拟合的结果表明缓释微球的释药行为符合扩散机制；测定三批微球样品的包封率均在96.8％以上，表明该法适合于制备难溶性药物的缓释微球。

It was worthy to note that Si-O stretching vibration infrared absorption could be regarded as an index in assessing the quality of synthetic 2:1 trioctahedral smectite sample.

红外光谱分析说明其中Si-O伸缩振动可作为成皂石样品结晶度的一个简单而有效的指示性参数。

It is shown that solvents may be classified by its effect into the active solvent and unactive solvent, and then, according to change of cold crystal peak area, effects of unactive solvents on the PET may be classified into three types: unchanged, reduced behind time and quickly reduced.

同时，对于非反应性的作用，依冷结晶峰面积的变化，又可分为三种类型：冷结晶峰面积不变，经诱导期后下降，无诱导期而迅速下降。

When the undrawn films were annealed atthose temperatures, the morphologies in the lamellar crystals had change. WAXDand iR studies shown that the crystallinities incrcand, dimensions in (002) and(020) normals increased while that in (200) fold had slight decreases. The rela-tionship between the orientation of the drawn UHMWPE gel-films and the struc-ture changes and the optimum drawing temperature had been disscussed.

通过IR及X－ray衍射等方法研究发现，拉伸前用不同温度退火处理后，凝胶膜的片晶微结构产生明显变化，在对应于超高拉伸温度范围内，其结晶度增加，微晶的c和b轴方向尺寸变大，而a轴方向的尺寸减小，从理论上对这一变化过程作了考察，并讨论了超高拉伸取向性与这些结构变化的关系以及可超拉伸取向性的最佳温度范围。

The system was a crystal achieved through the studying,specifying,colligating and programming of the agricultural economy and technology information,which truly reflected the fact of agricultural economy and technology information.

农业经济技术信息服务系统是对农业经济技术信息实际研究、细化、综合、流程化的结晶，系统贴近农业经济技术信息实际情况，科学进行合理分类，完善了农业经济技术信息的可维护性。

Lincomycin hydrochloride is a white or practically white, crystalline powder and is odorless or has a faint odor.

盐酸林可霉素是一种白色或几乎白色结晶性粉末，是无味或有微弱的气味。

Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来，英国，在此地早期居住的是凯尔特人，已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。