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化学分析

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According to the traditional classification, analytical chemistry can be divided into chemical analysis and instrumental analysis.

按照传统的分类,分析化学可分为化学分析和仪器分析。

At last, we has indeed confirmed the increase of oxygen contained on the sample's surface relative to background concentration in the bulk by the measurement of ESCA as well.

文中,我们也对湿氧化法处理过的试片,进行化学分析电子光谱仪,分析表面的氧含量,结果显示相较於背景氧浓度,表面氧含量确实有增多的现象。

Chemical methods such as surface contact angle analysis etc. were used to study the mechanism of microwave activated crumb rubber powder. The mechanism of the modified asphalt improved by MACR was analyzed by microcosmic measures and tests such as SEM etc.

通过接触角等化学分析方法研究微波辐射活化胶粉的机理;利用扫描电子显微镜等微观测试手段分析活化胶粉改善沥青性能的机理。

The failure of a gear shaft was analyzed by SEM analysis,macrograph,metallographical examination,mechanical test,chemical analysis and etc.

采用扫描电镜、低倍检验、金相检验、力学试验和化学分析等方法,分析了人字齿轮轴发生劈裂的原因。

Analysis of K and Na in nepheline were curried out with higher precision and repeatability by means of adding fluohydric acid during sample melting to remove SiO2 ,adjusting the ratio of K and Na in the solution to reduce the mutual interference of the two elements, and adding cesium chloride to eliminate ionization interference.

摘要本方法用于测定霞石中的钾、钠,主要通过在溶样时加入氢氟酸除去二氧化矽,调整溶液中钾、钠的含量,消除互相之间的干扰,加入氯化铯消除电离因素的干扰,提高了分析结果的准确性和重现性,使测定结果更接近化学分析值。

Analysis f K and Na in nepheline were curried out with higher precision and repeatability by means of adding fluohydric acid during sample melting to remove SiO2, adjusting the ratio of K and Na in the solution to reduce the mutual interference of the two elements, and adding cesium chloride to eliminate ionization interference.

摘要本方法用于测定霞石中的钾、钠,主要通过在溶样时加入氢氟酸除去二氧化矽,调整溶液中钾、钠的含量,消除互相之间的干扰,加入氯化铯消除电离因素的干扰,提高了分析结果的准确性和重现性,使测定结果更接近化学分析值。

The compositions of complexes were determined as, by chemical and elemental analyses, Mn2CI2, Mn2Cl2, Cu2Cl2-2H2O, Cu(NO3)2-H2O, Cu(CH3COO)2, Zn2Cl2, Zn2(NO3)2-4H2O,ZnSO4 and Zn4(NO3)2, respectively. These complexes were characterized by IR,'H NMR and XPS. The crystal structures of these complexes were determined by single crystal X-ray diffraction techniques. The thermstability of the complexes was investigated by TG-DTG and the processes of their thermal decomposition were speculated. The constant-volume combustion energies of complexes, cU, were determined by a precision rotating bomb calorimeter at 298.15 K. Their standard enthalpies of formation, Hm, were calculated respectively. Finally, their biological activity was researched after the bactericidal activity was determined by selection of 1-2 bacteria.

通过化学分析、元素分析确定化合物分子组成分别为Mn_2Cl_2,Mn_2Cl_2,Cu_2Cl_2·2H_2O,Cu(NO_3)_2·H_2O,Cu(CH_3COO)_2,Zn_2Cl_2,Zn_2(NO_3)_2·4H_2O,ZnSO_4和Zn_4(NO_3)_2;借助IR、~1H NMR和XPS对化合物的键型特征进行了表征,运用X-射线单晶衍射分析法测定了个别化合物的晶体结构;以TG-DTG技术研究了化合物的热稳定性,阐明了它们的热分解机理;用精密转动弹热量计测定了化合物在298.15 K的恒容燃烧能,并计算了它们的标准燃烧焓和标准生成焓;选取1~2种病菌,初步测定了化合物的杀菌活性,进而研究了它们的生物活性。

The content of cellulose in the carya crust was lower but its lignin content was higher. The ash content in the carya inner shell was only 8.2gkg^(-1). The chemical components of the quick-growing Chinese fir scrap were the same as those of natural forests.

化学分析结果表明:桔杆的纤维素质量分数为378.8~462.5gkg^(-1),木质素为164.0~253.0gkg^(-1),其主要成分与木材接近;山核桃外壳的纤维素较低,木质素和灰分较高,内壳的纤维素和木质素均较高,灰分较低,只有8.2gkg^(-1);速生杉木木屑的化学成分与天然林的相同。

Chemical analysis, laboratory testing of materials, chemical engineering and synthetic organic chemistry.

化学分析及物质属性的实验测试,化学工程及复合有机化学

In this study, we used poly L-latcide, poly DL-latcide-co-glycolide 75:25 (PLGA7525) and poly DL-latcide-co-glycolide 50:50 (PLGA5050) during citric acid inducing ammonium bicarbonate gas forming process to form porous polymer film, and rolled the porous polymer film to make nerve conduits with pores and multi-layered. Electron Spectroscopy for Chemical Analyzer and Attenuated Total Reflectance – Fourier-Transform Infrared Spectrometer were employed for determining elements' functionabilities and chemical compounds. Charge Coupled Device camera and Scanning Electron Microscope were employed for macroscopic and microscopic morphologies and structural observation. Differential Scanning Calorimetry was employed for measuring glass-transition temperature. Nano-indentation system was employed for measuring elastic modulus and hardness. Biodegradation and water absorption ratios were measured to analyze their chemical properties and SEM was employed for microscopic morphology of the tested nerve conduit.

本研究将以聚乳酸、聚乳酸-聚甘醇酸共聚合物(75:25)、聚乳酸-聚甘醇酸共聚合物(50:50)做为研究材料,以柠檬酸诱发碳酸氢铵发泡之气泡成型法制作具有相连通孔隙之高分子薄膜,再将高分子薄膜卷制成特殊多层的导管,制作具有多层孔隙之新型神经再生导管,以电子能谱化学分析及减弱式全反射-傅立叶转换红外线光谱分析进行成份分析及化学元素测定;以电荷耦合元件摄影机、扫瞄式电子显微镜进行多层孔隙型神经导管巨观及微观形态结构观察;以示差扫瞄热量量测分析玻璃转换温度、奈米三维量测弹性模数及硬度;以及进行降解性质测定,并以扫瞄式电子显微镜进行降解后之导管微观结构形态观察。

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