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Thus the sample size can be increased, and the nugget effect and detection limits can be decreased compared with normal Carius tube technique. This new technique is capable of digesting 12 g samples in a 75 mL Carius tube with 35 mL aqua regia at 320℃, and Re and all the PGEs can be measured.

由此可以加大取样量,降低铂族元素测定过程中的块金效应及检出限,使超低含量铂族元素的测定成为可能。12g样品在75mL卡洛斯管中用35mL王水于320℃溶解15h,基本上可以使各种地质样品中的铂族元素矿物完全溶解。

Its universality: its democratic equality and constancy to its nature in seeking its own level: its vastness in the ocean of Mercator's projection: its unplumbed profundity in the Sundam trench of the Pacific exceeding 8000 fathoms: the restlessness of its waves and surface particles visiting in turn all points of its seaboard: the independence of its units: the variability of states of sea: its hydrostatic quiescence in calm: its hydrokinetic turgidity in neap and spring tides: its subsidence after devastation: its sterility in the circumpolar icecaps, arctic and antarctic: its climatic and commercial significance: its preponderance of 3 to 1 over the dry land of the globe: its indisputable hegemony extending in square leagues over all the region below the subequatorial tropic of Capricorn: the multisecular stability of its primeval basin: its luteofulvous bed: its capacity to dissolve and hold in solution all soluble substances including millions of tons of the most precious metals: its slow erosions of peninsulas and islands, its persistent formation of homothetic islands, peninsulas and downwardtending promontories: its alluvial deposits: its weight and volume and density: its imperturbability in lagoons and highland tarns: its gradation of colours in the torrid and temperate and frigid zones: its vehicular ramifications in continental lakecontained streams and confluent oceanflowing rivers with their tributaries and transoceanic currents, gulfstream, north and south equatorial courses: its violence in seaquakes, waterspouts, Artesian wells, eruptions, torrents, eddies, freshets, spates, groundswells, watersheds, waterpartings, geysers, cataracts, whirlpools, maelstroms, inundations, deluges, cloudbursts: its vast circumterrestrial ahorizontal curve: its secrecy in springs and latent humidity, revealed by rhabdomantic or hygrometric instruments and exemplified by the well by the hole in the wall at Ashtown gate, saturation of air, distillation of dew: the simplicity of its composition, two constituent parts of hydrogen with one constituent part of oxygen: its healing virtues: its buoyancy in the waters of the Dead Sea: its persevering penetrativeness in runnels, gullies, inadequate dams, leaks on shipboard: its properties for cleansing, quenching thirst and fire, nourishing vegetation: its infallibility as paradigm and paragon: its metamorphoses as vapour, mist, cloud, rain, sleet, snow, hail: its strength in rigid hydrants: its variety of forms in loughs and bays and gulfs and bights and guts and lagoons and atolls and archipelagos and sounds and fjords and minches and tidal estuaries and arms of sea: its solidity in glaciers, icebergs, icefloes: its docility in working hydraulic millwheels, turbines, dynamos, electric power stations, bleachworks, tanneries, scutchmills: its utility in canals, rivers, if navigable, floating and graving docks: its potentiality derivable from harnessed tides or watercourses falling from level to level: its submarine fauna and flora, numerically, if not literally, the inhabitants of the globe: its ubiquity as constituting 90 percent of the human body: the noxiousness of its effluvia in lacustrine marshes, pestilential fens, faded flowerwater, stagnant pools in the waning moon.

50它的普遍性,它的民主的平等性,以及保持着它自身求平的本质。用墨卡托投影法在地图上所标示出的浩淼的海洋;太平洋中巽他海沟那超过八千噚的不可测的深度;永不消停、后浪推前浪地冲刷着海岸线每一部位的波涛以及水面上的微粒子;水的单位粒子的独立性;海洋变幻莫测;根据液体静力学,风平浪静时它纹丝不动;根据液体动力学,小潮大潮时它便涨了起来。暴风雨后一片沉寂;北极圈与南极圈冰冠地带的不毛性以及对气候及贸易的影响;跟地球上的陆地相比占三对一优势;它在亚赤道带南回归线以南的整个区域延伸无数平方海里的绝对权威;其在原始海盆里数千万年以来所保持的稳定性;它那橙红色海床;它那把包括数百万吨贵金属在内的可溶解物质加以溶解,并使之保持在溶解状态的性能;它对半岛和有下陷趋势的岬角所产生的缓慢的浸蚀作用;其冲积层;其重量、容积与浓度;它在咸水湖、高山湖里的静谧;其色调因热带、温带和寒带而变为或浓或淡;与陆上的湖泊、溪流及支流汇合后注入海洋的河川,还有横跨大洋的潮流所构成的运输网。沿着赤道下面的水路自北向南的湾流;海震、水龙卷、自流井、喷泉、湍流、漩涡、河水暴涨、倾盆大雨、海啸、流域、分水岭、间歇泉、大瀑布、漩流、海漩、洪水、泛滥、暴雨等滥施淫威;环绕陆地的上层土壤那漫长的曲线;源泉的奥秘可用探矿杖来占卜或用湿度测定器来揭示;阿什汤大门的墙壁上的洞、空气的饱和与露水的蒸发能够证明那潜在的湿度;水的成分单纯,是氢二、氧一的化合物;水的疗效;水的死海里的浮力;它在小溪、涧谷、水坝的缝隙、船舷的裂口所显示的顽强的浸透性;它那清除污垢、解渴、灭火、滋养植物的性能;作为模范和典型,它的可靠性;它变化多端:雾、霭、云、雨、麦、雪、雹;并在坚固的消防龙头上发挥出压力;而且千姿百态:湖泊、湖岔、内海、海湾、海岬、环礁湖、环状珊瑚岛、多岛海、海峡、峡江、明奇、潮汐港湾、港湾;冰河、冰山、浮动冰原显示出它是何等坚硬;在运转水车、水轮机、发电机、发电厂、漂白作坊、鞣皮厂、打麻厂时,它又是那样驯顺;它在运河、可航行的河川、浮船坞和干船坞所起的作用;潮汐的动力化或利用水路的落差使它得以发挥潜力;海底那些成群的动物和植物虽然并非名副其实地栖息在地球上,论数目却占地球上生物的一大半;水无所不在,占人体的百分之九十;在沼泽地、闹瘟疫的湿地、馊了的花露水以及月亏期那淤积污浊的水塘子,水所散发的恶臭充满了毒气。

Deformation greatly promoted carbonitride isothermal precipitation and made C-curve shift leftwards. The position and shape of C-curve depended on the content of Nb and N to a great extent, C-curve shifted leftwards a little when N content increased and its nose temperature was raised with Nb content increased. 3 when cooling rate increased, start temperature and finish temperature of continuous cooling precipitation decreased, full precipitation became difficult to take place, the volume fraction of carbonitride precipitation decreased, molar fraction of Nb and C dissolved in austenite increased, and the precipitation grain was further refined. Deformation shorten precipitation start time during continuous cooling, raised precipitation start temperature, accelerated precipitation kinetics of carbonitrides.

计算表明:1在Fe—Nb—C系统中,随着温度的降低,析出相的平衡体积分数增加,溶解在奥氏体中的Nb、C的摩尔分数降低,析出相中C和Nb的原子分数的比值v增加;2变形大大促进了碳氮化物的等温析出,使C曲线左移,Nb和N的含量与C曲线的位置和形状有一定的关系,N含量的增加,使C曲线略有左移,而Nb的含量的增加使得C曲线的鼻子区上移;3随着冷却速率的增大,连续冷却析出的开始温度和结束温度均有所降低,并且析出变得越来越不充分,析出相体积分数明显减小,溶解在奥氏体中Nb和C的摩尔分数增大,析出相粒子被明显细化,变形大大缩短了CCP过程碳氮化物析出的开始时间,提高了析出的开始温度,促进了析出动力学。

Even if energy saving window could be work when the molarity was decreased, but might not phase separation in real situation.

经比较可以发现当浓度降低其节能效率下降、临界溶解温度范围提高、反应速度加快,虽然浓度降低仍可以达到节能的目的且反应速度加快,但临界溶解温度范围提高可能使实际运用上会有所困难,有机会产生节能窗材无法相分离的情形,加上在低体积莫耳浓度时相分离后水胶粒子会沉淀的现象,使节能窗材无法顺利运作,故实际运用上不适合降低节能窗材的浓度。

Through the experiments on hydration of AH in the following sulphate(Li_2SO_4、MgSO_4 、 Al_2(SO_4)_3 、MnSO_4 、CuSO_4 、CoSO4 、CdSO_4 、ZnSO_4 、NiSO_4 、FeSO_4), dissoluble sulfate hydrate origining from hydration process of AH affects it's hydrous rate, hydrous rate of AH does not connect with Z/R of cation in stimulation, theory that Z/R affect hydrous rate of AH does not exist. Third, hydration of AH in dissoluble sulfate complies with dissolve-nucleate -grow theory, concentration of Ca~2+ from dissolving of CaSO_4 is higher than one of CaSO_4·2H_2O, calcium sulphate dihydrite gets a motivity of crystallization. dissoluble sulfate takes the following function: double-salt or dissoluble sulfate hydrate from hydration of AH in it becomes heterogeneous particle and a kind of nucleation catalyzer, and reduces surface barrier when DH becomes crystal because the crystal of DH precedently appears in uneven place. Results indicate hydration of AH does not conform with double-salt theory, but it conform with this mechanism: dissolve-nucleate-grow, formation of DH is an uneven nucleation and crystalizaion process.

通过对CaSO_4在Na_2SO_4 、K_2SO_4 、Rb_2SO_4 、Cs_2SO_4 、(NH_4)_2SO_4溶液中水化过程,以及CaSO_4·2H_2O、CaSO_4与以上硫酸盐反应速度、产物的研究,说明复盐理论不正确;CaSO_4在(Li_2SO_4、MgSO_4 、 Al_2(SO_4)_3 、MnSO_4 、CuSO_4 、CoSO_4 、CdSO_4 、ZnSO_4 、NiSO_4 、FeSO_4)溶液中水化,水化过程中硫酸盐水合物的析晶影响着无水硫酸钙水化,与激发剂阳离子Z/R值大小无关,阳离子的Z/R参数影响水化率的规律并不存在; 3、无水硫酸钙在可溶性硫酸盐中的水化按照溶解-成核-生长理论进行,CaSO_4达到溶解平衡时Ca~2+的浓度大于CaSO_4·2H_2O溶解平衡的Ca~2+的浓度,CaSO_4·2H_2O获得结晶的驱动力,可溶性硫酸盐起到形成晶核的作用:水化过程与CaSO_4生成复盐或析出水合物所形成的细小物相,作为异质微粒使母相中存在不均匀性,这些不均匀性有效地降低成核时的表面能位垒,使CaSO_4·2H_2O晶核优先地在这些具不均匀性的地方形成,因此这些物质起成核催化剂作用。

The oxidant 〓 plays indirect role in dissolving gold, and mainly controls the mix potential of Au in the alkaline thiourea solution. In which the "mix potential"is the decisive factor affecting the dissolution of gold. The reaction driving force is enough to have formamidine disulfide oxidize Au to Au〓 at the potential of about 0.4V. And then thiourea molecular complexes with Au〓 ion soon, which causes the fast dissolution of gold in the alkaline thiourea media. The dissolved weight of gold in 0.25 M thiourea solution with 0.05M Na〓SO〓 and 0.1M 〓 of pH 12. 5 by air at the temperature of 303K is 7. 8mg·cm〓 within 1hr.

在碱性硫脲溶金过程不起直接作用,而是通过S〓O〓来控制二硫甲脒有效形成的金在溶液中的混合电位;&混合电位&是影响碱性硫脲溶液溶金与否的决定性因素,在0.4V左右,有足够的推动力致使二硫甲脒氧化Au成Au〓,随后硫脲与Au〓络合形成稳定的络离子Au〓,从而使金快速溶解;温度为303K、pH为12.5时,在含0.05MNa〓SO〓、0.1M 〓及0.25M硫脲的溶液中,鼓入空气,金的溶解量在1hr内为7.8mg·cm〓;铜只有微量溶解,银、镍、铁则几乎不溶解。

Due to great amount of double bond on rubber chain,a lot of intramolecular reaction occurred in the system,which made the uncontrolled cross-linked system into a controlled cross-linked copolymerization,resulting in chain growth can't go illimitably in cross-linking process.

苯乙烯和二乙烯苯共聚体系是典型的不可控制的交联聚合体系,加入天然橡胶后,通过阳离子聚合方法,生成三元共聚物线团,由于橡胶分子链上含有大量的双键,聚合体系中能进行分子内反应,使不可控的交联聚合体系成为可控的交联聚合体系,其链增长不能无限制进行,从而可以合成可溶解的交联的聚苯乙烯-二乙烯苯-天然橡胶聚合物。

SHILLS cherry polyphenol Skin Firming Cleansing Oil uses natural plant essence olive oil as the base, as long as you can gently massage deep pore, so accumulation of make-up, dirt completely dissolved floats, unique balance of sebum Jie Yan efficient system, the event water that is emulsified fully achieved thorough cleansing, skin-friendly high-energy removable durable powder-type heavy makeup, and even Keana in the sebum and blackheads, the old waste horny and dirty, also with reduced time them altogether have been resolved; and add the cherry extract the unique flavor, so that post-up remover, like moisturizing the skin to relieve the skin smooth and clean instant restore the delicate baby-like luster

SHILLS樱花多酚柔肤紧致卸妆油采用天然植物橄榄精华油为基底,只要轻轻按摩就可深入毛孔,使堆积的彩妆、污垢彻底溶解浮出,独特的高效平衡皮脂洁颜系统,遇水即乳化完全达到彻底清洁,亲肤性高能卸除持久型浓妆粉料,连毛穴中的皮脂与黑头粉刺、老废角质及脏污,也都无所遁形一次通通都解决;并添加樱花萃取物的独特香味,让卸妆后的肌肤一样保湿、纾缓,肌肤瞬间光滑洁净,恢复婴儿般的娇嫩光彩

A method for the analysis of zinc oxide phase content in sulfide ore was studied. On the basis of the characteristics of each phase component, the sulfide ore sample was leached twice with NaOH and acetic acid-ascorbic acid, respectively, so that the oxide mineral and zinc oxide were dissolved completely. The leaching rate of zinc oxide phase was up to 98 Vo. Moreover, the dissolution of zinc sulfide phase was effectively inhibited, solving the problems of selective leaching and determination for zinc oxide.

研究了硫化矿中氧化锌相含量的分析方法,根据硫化矿中各物相组分特点,提出了用氢氧化钠溶液和乙酸-抗坏血酸溶液二次浸取硫化矿,使锌氧化矿、氧化锌充分溶解,氧化锌相的浸取率达到98%以上,同时有效地抑制了硫化锌相的溶解,较好地解决了氧化锌相选择溶解测定的问题。

Its preparing process includes dissolving the salts containing metal in group VIB or VII or their mixture in ammonia water until full dissolving, and adding citric acid to stabilize the solution.

其制备方法为:先用氨水溶解含ⅥB族金属或Ⅷ族金属的盐,或二者混合物,使之完全溶解后,加入柠檬酸以使溶液稳定。该溶液稳定性好,制备过程快速、简便、节能。

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