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二-十进制

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Water,c12-20 acid peg-8 ester,octyldodecanol,cetearyl isononanoate,butylene glycol,biosaccaride gum-1,peg-40 hydrogenated caster oil,ethylhexyl menthoxycinnamate,phenoxyethanol,potassium cetyl phosphate,macadamia ternifolia seed oil,dimethicone,carbomer,propylene glycol,glyceryl stearate,cocoglycerides,butyrospermum parkii,c12-13 alkyl lactate,methylparaben,benzophenone-3,pentadecalactone,sorbic acid,citrus aurantium dulcis oil,sodium hydroxyde,tocopheryl acetate,disodium edta,iris germanica root extract,retinyl palmitate,equisetum arvense extract,butylparaben,peg-8,propylparaben,ethylparaben,sodium hyaluronate,chlorhexidine digluconate,citrus aurantium amaraoil,tocopherol,ascorbyl palmitate,citric acid,ascorbic acid,limonene,linalool

水,c12-20 acid peg-8 ester,辛基十二烷醇,鲸蜡硬脂醇异壬酸酯,丁烯二醇,多醣物质,PEG-40氢化蓖麻油,4-甲氧基肉桂酸-2-乙基己基酯,苯氧乙醇,十六烷基磷酸钾,澳洲胡桃子油,地美司康,卡波姆,丙烯乙二醇,甘油硬脂酸,椰油脂酸甘油酯类,牛油果,c12-13烷醇乳酸酯,对羟基苯甲酸甲酯,二苯甲酮-3 ,环十五内酯,山梨酸,甜橙油,氢氧化钠,维生素E醋酸酯,乙二胺四乙酸二钠,鸢尾花萃取,维他命A酯,问荆萃取,对羟基苯甲酸丁酯,聚乙二醇- 8,羟苯丙酯,羟苯乙酯,透明质酸钠,洗必泰葡萄糖酸盐,苦橙油,维生素E ,维生素C棕榈酸酯,柠檬酸,抗坏血酸,柠檬精油,沉香醇水:几乎所有护肤品成分第一位都是水。辛基十二烷醇:界面活性剂、乳化剂、稠化剂,有一定刺激性

EH detected in Lanzhou reach of the Yellow River included naphthalene, phenanthrene, DBP, DEHP and benzothiazole and the detection rates of the five EH were 40%, 60%, 100%, 100% and 20% respectively.

结果 共定性检出有机类环境激素10种,即邻苯二甲酸二异丁酯、邻苯二甲酸正丁酯、邻苯二甲酸二(2-乙基己基)酯、邻苯二甲酸丁酯、邻苯二甲酸异辛基酯、邻苯二甲酸丁环己酯、苯并噻唑、萘、菲、苯并异噻唑。C断面检出的环境激素浓度最高,菲、DBP、DEHP浓度分别高达0.320、13.89、109.93μg/L.A断面次之,B断面检出的环境激素浓度与A断面相比有所下降,E断面检出的环境激素与其他断面相比,浓度相对较低,D断面所检出的环境激素与C断面比较,有一定下降,但下降不明显。

Co condensation type polyamides were prepared by using 1,2 dihydro 2 (4 aminophenyl) 4 [4 (4 aminophenoxyl) phenyl] phthalazin 1 one and 4,4′ diamino biphenyl ether or 4,4′ diamino biphenyl methane as the co diamine monomers and aromatic diacid as the co condensation monomer.

采用 1 ,2 -二氢-2 -( 4-氨基苯基)-4 -[4 -( 4-氨基苯氧基)-苯基 ]-二氮杂萘-1 -酮、4 ,4′-二氨基二苯醚、4 ,4′-二氨基二苯甲烷为共缩聚二胺单体与对苯二甲酸进行共缩聚反应,制备共缩聚型聚酰胺。

This work, concentrated on the asymmetric allylation of aldehydes controlled by different chiral auxiliaries prepared from rotational pure tartaric acid, can be divided into three parts.The first part aims to review the developments of chiral drugs and asymmetric synthesis, from which derived the present research topic backgrounds and works.Synthesis and applications of allylation from aldehydes are the second part of the thesis. By optimizing the reaction conditions, such as solvents, temperature, time and chiral auxiliaries like N,N\'-dibenzyl tartamide, N,N\'-p-dimethylphenyl tartamide, N,N\'-o-dimethylphenyl tartamide, N,N\'-o-dichlorophenyl tartamide, N,N\'-a-dinaphyl tartamide, N,N\'-dicyclohexyl tartamide and N,N\'-diphenyl tartamide, ideal experimenttal conditions are obtained according to HPLC monitoring, as well as the auxiliaries\' recoveries experiments. Starting from benzaldehyde and 3-bromopropaldehyde, N,N\'-dibenzyl tartamide is considered the best auxiliary in this reaction.

本文介绍了醛的不对称烯丙基化反应,以光学纯酒石酸为原料,研究了不同构型手性配体在醛的烯丙基化反应中的立体选择性,全文共分三部分十个章节:第一部分对当前手性药物和手性技术进行了概述,并由此展开了本文的研究背景和任务;第二部分为有机合成部分,对醛的不对称烯丙基化反应进行了深入探讨,以苯甲醛为原料对反应条件进行优化,在优化的反应条件下对制备的七种可回收手性酰胺配体(N-苄基酒石酸二酰胺、N-对甲苯基酒石酸二酰胺、N-邻甲苯基酒石酸二酰胺、N-邻氯苯基酒石酸二酰胺、N-a-萘基酒石酸二酰胺、N-环己基酒石酸二酰胺和N-苯基酒石酸二酰胺)进行筛选,优化配体回收实验条件,最终确定出N-苄基酒石酸二酰胺在苯甲醛的不对称烯丙基化反应中具有较大优越性,结晶回收的手性配体光学纯度保持不变。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&(One—pot Synthesis),由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4,4\'—二氨基二苯醚、3,4\'—二氨基二苯醚、2,2—双[4—(4—氨基苯氧基苯基]丙烷和2,2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&O(来源:88AB57C论文网www.abclunwen.comne—pot Synthesis,由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4,4\'—二氨基二苯醚、3,4\'—二氨基二苯醚、2,2—双[4—(4—氨基苯氧基苯基]丙烷和2,2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

Firstly, the reactions of glutaric acid, sebacic acid and propargyl alcohol afforded two dipropargylesters:(CH≡CCH_2OCO)_2(CH_2)_3 (compound 1) and (CH≡CCH_2OCO)_2 (CH_2)_8 (compound 2),respectively.

首先,本文分别选用戊二酸,癸二酸与丙炔醇反应得到了两个新的有机二酸二丙炔醇酯:戊二酸二丙炔醇酯(CH≡CCH_2OCO)_2(CH_2)_3(化合物1)和癸二酸二丙炔醇酯(CH≡CCH_2OCO)_2(CH_2)_8(化合物2)。

Niobic acid; catalytic synthesis; di-2-ethylhexyl phthalate; di-n-octyl phthalate; di-2-ethylhexylmaleate; di-n-octyl maleate; cyclohexene; modification of catalyst; dynamics of esterification

工程科技I,化学,有机化学铌酸;催化合成:邻苯二甲酸二辛酷;邻苯二甲酸二异辛酯;顺丁烯二酸二辛酯:顺丁烯二酸二异辛酯:环己烯;改性;动力学

The density, binding energy and radical distribution function of HTPB/plasticizers blends and binder hydroxyl-terminated polybutadiene, and plasticizer dioctyl sebacate, dioctyl adipate, dibutyl phthalate, dioctylphthalate were calculated by molecular dynamics simulation for evaluating compatibility of HTPB and plasticizers.

为评价端羟基聚丁二烯与增塑剂相容性的优劣,采用分子动力学模拟方法对纯HTPB、增塑剂癸二酸二辛酯、己二酸二辛酯、邻苯二甲酸二丁酯、邻苯二甲酸二辛酯及HTPB与增塑剂组成的共混物的密度、结合能和径向分布函数等进行了计算。

It is necessary to carry out a thorough study on pest control technology with DMDS, with an expectation of obtaining a new fumigant of methyl bromide alternative.2. Investigation of the toxicity of fumigation on adult and mixed stages of the three most tolerant insect species -- Sitophilus oryzae, Rhyzopertha dominica and Tribolium castaneum -- under a range of EtF、DMS and DMDS doses in a Flow-through Fumigation System shows that the FTFS procedure offers a constant concentration of fumigant with low CO2 concentrations and ensures that the fumigant toxicity is effectively not compromised by CO2. In comparison with chamber fumigation method, the toxicity data of EtF、DMS and DMDS obtained from this experiment is more accurate by using FTFS.

主要研究结果如下:1、甲酸乙酯和二甲基二硫对仓储害虫具有良好的控制作用,应加快甲酸乙酯替代溴甲烷防治仓储害虫开发应用,同时,二甲基二硫是很有潜力的仓储害虫防治熏蒸剂,要深入进行二甲基二硫控制有害生物的技术研究,以期获得新的溴甲烷替代熏蒸剂。2、利用循环熏蒸系统测定了甲酸乙酯、二甲基二硫和甲硫醚对米象Sitophilus oryzaeL。

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