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TEM shows that drying by direct heating might result in hard aggregation of the tourmaline powder, while hard aggregation might be avoided by azeotropic distillation. Raman spectroscopy reveals that there are O_H and C_H on the surfaces of the tourmaline powder obtained by azeotropic distillation, which indicates that butoxy is chemically adsorbed on the surfaces of tourmaline particles, but not adsorbed on those formed by direct drying. X_ray powder diffraction shows that the intensity of diffraction peaks decreases after grinding. There is no damage to the tourmaline crystal lattice in the process of direct heating, azeotropic distillation, or ultrafine grinding.

透射电镜分析结果表明,直接加热脱去水或正丁醇会使电气石超细颗粒发生硬团聚,而共沸蒸馏法则可有效防止硬团聚的产生;拉曼光谱结果表明,共沸蒸馏法制备的电气石粉末表面存在O—H和C—H键,说明正丁醇在颗粒表面为化学吸附,而直接干燥法得到的电气石粉末表面则没有;X射线粉晶衍射结果表明,研磨过程降低了粉末衍射峰的强度,但直接加热干燥和共沸蒸馏干燥均未破坏电气石的晶格结构。

The models of auricular edema in mice by dimethyl benzene and increased permeability of celiac blood capillary by acetic acid were studied,the results showed that the petroleum ether and acetic ester fraction of fermentation product of Calvatia gigantea could inhibit ear edema;acetic ester and n-Butanol fraction of fermentation product could reduce the permeability of celiac blood capillary by acetic acid.

大秃马勃Calvatia gigantea发酵液的石油醚、乙酸乙酯和正丁醇提取物进行二甲苯诱导小鼠耳廓急性炎症和醋酸所致小鼠腹腔毛细血管通透性实验,结果表明大秃马勃Calvatia gigantea发酵液石油醚提取物处理组、乙酸乙酯提取物处理组对二甲苯诱导小鼠耳肿胀具有明显的抑制作用;大秃马勃Calvatia gigantea发酵液乙酸乙酯提取物处理组、正丁醇提取物处理组对醋酸所致小鼠腹腔毛细血管通透性具有明显的抑制作用。

Mixing and dilution heterotactic enthalpies of aqueous n-butanol solutions and aqueous amino acids (glycine, L-alanine, L-proline, L-valine) solutions were determined at 298.15 K by flow microcalorimetric system of 2277 Thermal Activity Monitor. The data were analyzed by using the McMillan-Mayer theory to obtain the enthalpic interaction coefficients.

利用2277热活性检测仪的流动测量系统获得了298.15K时甘氨酸、L-丙氨酸、L-缬氨酸和L-脯氨酸分别与n-丁醇在水溶液中混合过程的焓变以及各自的稀释焓,依据McMillan-Mayer理论关联得到异系焓相互作用系数,讨论了不同氨基酸与n-丁醇分子的作用机理。

The inhibition effect of chloroform fraction was the most potent, with the inhibition rate about more than 83% to 5 plant pathogenic fungi under the concentration of 15mg/mL. Under the concentration of 15mg/mL, the ethyl acetate fraction and n-butanol fraction thoroughly inhibited the growth of Alternaria solani and Valsa mali, with the inhibition rate up to 100%. The n-butanol fraction showed the highest potent virulence, with EC50 to Alternaria solani and Valsa mali about 0.09 and 0.279 mg/mL respectively.

其中氯仿部分的抑菌效果较好,当质量浓度为15mg/mL时,其对5种植物病原菌的抑制率均在83%以上;15mg/mL乙酸乙酯部分和正丁醇部分分别对番茄早疫病菌和苹果腐烂病菌有强烈且稳定的抑制作用,抑制率达100.00%,正丁醇部分对这两种菌丝生长抑制毒力最好,EC50分别为0.090和0.279mg/mL。

The phase diagram and the structure change of W/O→bi-continuous structure→virgulate liquid crystals→lamellar liquid crystals→bi-continuous structure→O/W studied by conductivity measurement were established for this system at 25℃.

在25℃时,作出SDS/正丁醇/正庚烷/水体系中SDS和正丁醇质量比为1:1时的拟三元相图,用电导率曲线讨论了该体系由W/O型→双连续型→棒状液晶→层状液晶→双连续型→O/W型的微观结构转变。

The methyl pheophorbide-a (5) was oxidized with osmium oxide and sodium periodate to give chlorin 8 which was converted into aldehyde purpure-18 (9) and purpure-7 trimethyl ester (10) by air-oxidation in butanol in the presence of sodium.

选用四氧化锇和高碘酸钠将5氧化成卟吩醛(8),在丁醇中以丁醇钠作催化剂, 8的氧化和重排反应给出3-甲酰基紫红素-18酯(9)和紫红素-7三甲酯衍生物10。

Two 0.5-ml volumes of an isobutanol internal standard (10 mg/ml water; pipette 12.4 ml of isobutanol and dilute to 1 liter with water) are pipetted into two different 2-dram (7.4-ml) shell vials, one market "known."

将两份0.5毫升的异丁醇内标物(浓度为10mg/ml水,其配制法为:用吸量管吸取12.4ml 异丁醇用水稀释至1L ),用吸量管分别吸入两个不同的2-打兰(7.4毫升)的壳型小瓶中,一个标为&已知&,另一个标为未

Two 0.5-ml volumes of an isobutanol internal standard (10 mg/ml water; pipette 12.4 ml of isobutanol and dilute to 1 liter with water) are pipetted into two different 2-dram (7.4-ml) shell vials, one market "known."and the other "unknown."

将两份0.5毫升的异丁醇内标物(浓度为10mg/ml水,其配制法为:用吸量管吸取12.4ml 异丁醇用水稀释至1L ),用吸量管分别吸入两个不同的2-打兰(7.4毫升)的壳型小瓶中,一个标为&已知&,另一个标为&未知&。

Nano-cobalt blue precursor was prepared by mixing two types of microemulsion solutions of oleic acid/butanol/sodium carbonate solution and oleic acid/butanol/sodium hydroxide solution for reaction, into which Co~(2+) and Al~(3+) were solubilized respectively.

将Co2+和Al3+分别溶于油酸/正丁醇/碳酸钠水溶液和油酸/正丁醇/氢氧化钠水溶液制成微乳液,再将2种微乳液混合,反应生成纳米钴蓝前驱体。

The TLC of them were concordance.They presented the same color fluorescence in the corresponding position at the ultraviolet light(365nm). After the vanillic aldehyde sulphuric acid ethanol solution developed, violet color spots presented at the same place. Reference substance of Polysaccharide presented violet color ,but in the corresponding position the crude and the prepared didn't show the spots .

生远志正丁醇部位色谱和蜜远志正丁醇部位色谱基本一致:紫外灯(365 nm)下二者在相应位置呈相同颜色荧光,香草醛硫酸乙醇溶液显色后二者在相应位置的几个斑点均呈紫罗兰色,且远志皂苷元对照品斑点呈紫罗兰色,而在与其相应位置生远志供试品和蜜远志供试品均未检视到相应斑点。

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