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The optimum reaction conditions are as follows: diphenylmethanethiol : methyl chloroacetate is 1:1.5, and the reaction carried out at 100℃ for 4 h, 2- acetamide can be carried out in the room temperature for 20 h, the yield of 2- acetamide was 76%, hydrogen dioxide: 2- acetamide is 1:1, and the reaction carried out at 60℃ for 3 h, the yield of modafinil was 79%, the total yield of reaction can be reached 48%.

研究表明,采用氯乙酸甲酯作为醚化试剂,反应时间4h,反应温度100℃,二苯甲硫醇:氯乙酸甲酯=1:1.5,室温下氨解反应20h,二苯甲硫乙酰胺收率76%;采用过氧化氢作为氧化试剂,反应时间3h,反应温度60℃,过氧化氢:二苯甲硫乙酰胺=1:l,莫达非尼收率79%,反应总收率可达48%。

The result showed that the best time for sampling was 7 to 14 days after the first bud flowering on the main anthotaxy. The capacity of embryoid production varied significantly in different genotypes. Among them, twelve genotypes yield embryos successfully, which the rate could reach 71%. Genotype 102 was an ideal material for embryoid induction, and the frequency could reach 32.78 embryos per bud. Genotype that with a highest yield produced 546 times as many embryos as that with a lowest yield. The embryoid induction ability of normal bolting genotypes were higher than easy bolting and hard bolting genotypes.

结果表明:在秋冬季日光温室内,供试植株主花序第一朵花开后第7~14天取样,即初花期是最佳取样时期;不同基因型间小孢子胚胎发生能力差异很大,在接种的17个基因型中,有12个诱导出胚,诱导成功率71%;其中102号产胚量最高,达到32.78个/蕾;在已产胚材料中,产胚量最高的基因型是产胚量最低的基因型的546倍;较易抽薹型材料的产胚能力大于易抽薹型和不易抽薹型。

First, a chlorinator was self-designed in this paper, and dichloride of 2-methyl-1-propene was synthesized by 2-methyl-1-propene reacted with chlorine fast in this reactor. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield and selectivity of dichloride of 2-methyl-1-prop-ene were more than 65% and 80% respectively. Second, the preparation of 2-methylene-1, 3-propanediol, which dichloride of 2-methyl-1-propene reacted with alkali was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the conversion of dichloride of 2-methyl-1-propene was 100%. Moreover the preparation of MPO, which 2-methylene-1, 3-propanediol reacted with hydrogen, in presence of Al_2O_3-Pd catalyst, was gotten, and the product was appraised.

本文在氯化反应过程中,自行设计制作出了氯化管式反应器,在该反应器中异丁烯和氯气迅速混合反应生成二氯异丁烯,根据该氯化反应特征利用正交试验和单因素试验考察了有关因素的影响并优化得到了最佳工艺条件,二氯异丁烯的总收率达65%以上,选择性达80%;接着,对二氯异丁烯进行水解反应制得了2-甲烯-1,3-丙二醇,讨论了相关因素对水解反应的影响,并通过正交试验和单因素试验得到了较佳工艺条件,二氯异丁烯的转化率达100%;同时还对制备的2-甲烯-1,3-丙二醇在常压下采用三氧化二铝负载钯催化剂催化加氢得目的产物MPO,并对产品进行了鉴定,从而打通了整个工艺路线。

The average heterosis of spike number per plant and 1 000-grain-weight were high and obviously related to yield heterosis at 0. 01 and 0. 05 level, respectively; the average yield heterosis of F1 hybrids between common wheat and club wheat was 77. 19%(ranged from-2. 18% to 143. 42%), the average heterosis of spike number per plant and spike grain number were high and both was also obviously related to yield heterosis at 0. 01 level.

结果发现:小麦种间杂种在产量上具有明显的杂种优势,其中斯卑尔脱小麦与普通小麦所配的30个种间杂交组合产量杂种优势平均为109.24%(43.14%~187.96%),单株穗数及千粒重平均优势较大且与产量优势的相关分别达极显著水平和显著水平;密穗小麦与普通小麦所配的30个种间杂种的杂种优势为77.19%(-2.18%~143.42%),单株穗数和主穗粒数优势较大且与产量优势的相关均达极显著水平。

The correlation coefficients of 12 of the 35 meteorological factors with wheat yield were significant at the 0.05 level. The precipitation during filling stage and winter wheat yield was significantly corelated, and the direct path coefficient was the highest, and it contributed the most to wheat yield, followed by the precipitation of elongating stage and turning green period. The evapotranspiration in April and May negatively correlated significantly with winter wheat yield at the 0.05 and 0.01 levels, respectively.

在与小麦产量相关的35个气象因子中,有12个因子的相关系数达到了显着或极显着水平,其中灌浆期降水与冬小麦产量呈极显着相关,且直接通径系数最高,对小麦产量贡献率最大;其次是拔节期降水量和返青期降水量;4、5月份的蒸发量与冬小麦产量密切相关,分别接近显着和达到极显着水平,它们对小麦产量形成起较大的负向作用;小麦越冬期间的气温也是不可忽视的气象因素。

Hm~-2, the four cultivation facts all had extremely significant effect on lint cotton yield; boll numbers per ha changed from 692400 to 1073250; single boll weight changed from 4.38 to 5.71 g and the lint percent changed from 41.0 to 42.8%. Different treatments had extremely different effect on yield component factors;(2) According to mathematical model established by lint cotton yield, in 95% confidence interval, when lint cotton yield is more or equal to 2100Kg.

结果表明:(1)皮棉产量变幅为1609.5-2337.0Kg·hm~(-2),说明不同处理对皮棉产量有极显著的影响;铃数变幅为692400-1073250个·hm~(-2),单铃重变幅为4.38-5.71克,衣分变幅为41.0-42.8%,表明不同处理对产量构成因素也有极大影响,但与对产量的作用不同步。

In the first stage, when environment temperature arrived to 37.5℃, Ta of A and B dairy barn was 35.5 and 36.7℃, respectively. And at the same time Tr was higher than 39.5℃. Specially, the high yield dairy in A barn raised to 41 ℃ at 22:00 and RR was 90/min, the RR of low yield dairy was 65/min at this time. mTs was 37.6℃ at 15:00. In the third stage, Ta of the barn was higher than outside when outside Ta was lower than 27.6℃. When the ambient temperature was lower than 28℃, the Tr of low yield dairy was between 38.5 and 39℃; if the Ta was down to 24℃, Tr of high yield dairy was lower than 39℃.

第一阶段,舍外Ta平均达37.5℃时,A、B舍内Ta分别为35.5和36.7℃,此时Tr达到39.5℃以上,尤以A舍内高产奶牛22:00最高,平均达41℃;第一阶段平均RR在65次/min以上,高产奶牛在22:00、低产奶牛在15:00最高,分别为94和95.9次/min;平均mTs高产奶牛在15:00高达37.6℃;第三阶段,舍外平均Ta在15:00最高为27.6℃时,此阶段舍内Ta均高于舍外。

Changing formula forms of single-shear, twin-shear and three-shear yield strength criteria, show that many of yield strength criteria of rock and soil materials can be expressed by the τ8 = gf function forms unter the ordinary condition, and that the main differ ences of yield strength value will mainly forcus on the different function forms of gθσ among single-shear, twin-shear and three-shear yield strength criteria.

对岩土体常用的单剪屈服强度准则、双剪屈服强度准则和三剪屈服强度准则进行了系统的论述,通过对单剪、双剪和三剪屈服强度准则进行转化,指出岩土的屈服强度准则一般可表达为τ8=gf的函数形式,阐明了单剪、双剪和三剪屈服强度准则的差异主要表现在g函数的不同,并进一步解释了中间主应力σ2对岩土类材料屈服强度的影响。

This course is an attempt to give the students the basic idea and method of forest management in order to prepare the management plan; Place of forest management in forestry; Content of forest management; Guide principles of forest management; Sustained working; Silvicultural system; Forest yield; Increment; Volume increment; Quality increment; Price increment; Total price increment; Forest maturity; Indicating percent; Productive stage; Physical rotation; Technical rotation; Rotation of maximum volume yield; Highest forest rent rotation; Financial rotation; Cutting cycle of selection system; Normal forest; Normal distribution of age classes; Normal arrangement of stands; Normal increment; Normal growing stock; Normal yield; Improvement of actual forest; Reserve forest; Reserve fund; Planning and plan of forest management; Forest regulation; Area allotment; Volume allotting method; Volume frame work; Area-volume combined frame work; Growing stock; Utilization percent method; Difference method; Pure age-class; Growth method; Control method; Forest subdivision; Forest surveying; Forest survey; Certainty of future policy of forest; Selection of species; Decision of silvicultural system; Decision of rotation; Regulation of future yield; Preparation of management plan; Working the plan; Control and revision of management

本课程之目的为使学生了解森林经营之基本观念及方法,以期编订经营计划,课程包括森林经营学在林学上之地位、森林经营学之内容、森林经营之指导原则、保续作业、森林作业法、森林收获、生长、材积生长、形质生长、腾贵生长、总价格生长、林木成熟期、指率、生产期、自然轮伐期、工艺轮伐期、材积收获最多轮伐期、森林纯益最大之轮伐期、财政轮伐期、择伐林之回归期、法正林、法正龄级分配、法正林分排列、法正生长、法正蓄积、法正伐采额、现时林之改良、预备林、预备金、森林经营上之规划及计划、收获预定、面积配分法、材积配分法、材积平分法、折衷平分法、蓄积法、利用率法、较差法、纯粹龄级法、生长量法、稽核法、森林区划、森林测量、森林调查、将来森林经营方针之确定、树种之选定、作业法之决定、轮伐期之判定、将来收获之预定、经营管理计划之编订、计划之执行、经营管理计划之稽核与检订。

The second section analyzes the restraint conditions of establishing zero-coupon bond yield curve in China. In order to analyze the constraint conditions of establishing zero-coupon bond yield curve, we should firstly study the current situation and problems of Chinese bond market because the data estimating zero-coupon bond yield curve mainly come from bond market which can't be separated from the analysis of the development history of bond market. So the main content of this section includes the development history of bond market, the present problems of Chinese bond market and the restraint conditions of establishing zero-coupon bond yield curve in China.

第二节分析中国零息票债券收益率曲线构造的约束条件,由于估计零息票债券收益率曲线所需要的数据主要来自债券市场,这样,要研究零息票债券收益率曲线构造的约束条件,首先必须研究中国债券市场的现状和问题,而这一切又离不开对中国债券市场发展历史的分析,因此本节的内容包括中国债券市场发展的历史沿革、中国债券市场目前存在的主要问题和中国零息票债券收益率曲线构造的约束条件三个部分。

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