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Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.
除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅,张金艳,梁英,沈勇(黑龙江八一农垦大学文理学院,黑龙江大庆 163319)摘要:以33%的氢氧化钠水溶液为缚酸剂,异丙醇胺、环戊酮和二氯乙酰氯为原料,采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷,采用正交实验法得到最佳反应条件:反应原料摩尔比为1∶1∶1.2,苯作溶剂,反应的温度为-15 ℃~-10 ℃,搅拌时间为3 h,产率达到50.0%。
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Firstly, dicyclopentyldichlorosilane, a reaction intermediate, was prepared under the optimal conditions of a reaction pressure range of 1.0-1.2 MPa, a n/n of 1.16, a reaction temperature range of 85-95℃, a catalyst dosage of 1.2 g, an isooctyl alcohol dosage of 2.3 g and a reaction time range of 6-7 h. The conversion of cyclopentene and the yield of DCPDCS were 96.2% and 88.9%, respectively.
首先研究了合成DCPDCS的最佳工艺条件:反应压力1.0~1.2 MPa,n/n= 1.16/1.00,反应温度85~95 C,催化剂用量1.2 g,异辛醇用量2.3 g,反应时间6~7 h,环戊烯转化率可达96%以上,DCPDCS收率可达88%以上。
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In March, May and July, Cyanophyta was the dominant one, with high proportions of 45.6%, 55.9% and 87.7%, respectively, whereas the proportions for Bacillariophyta decreased to 30.1%, 25.9%, and 1.1%, respectively. In November, proportions for Bacillariophyta and Chlorophyta were equivalent, 40% each, and the Cyanophyta composed below 20%. In December, Bacillariophyta made up 25.6% and Cyanophyta 38.2%. In March, May and July, dominant species of Cyanophyta were Microcystis aeruginosa, Pseudoanabaena, and Gloeothece linearis. In dry January, November and December, species of Bacillariophyta were dominated by A chnanthes sp., Melosira ambigua, Melosira granulata and Cyclotella meneghiniana.
全年中,蓝藻与硅藻比例变化较大,二者呈相反的变化趋势。1月份硅藻占较高比例(63.1%),蓝藻较低(〈20%);3、5、7月份蓝藻比例较高(分别为45.6%、55.9%、87.7%),而硅藻较低(30.1%、25.9%、1.1%);11月份硅藻与绿藻比例相当(各占40%),蓝藻低于20%;12月份硅藻与蓝藻比例分别为25.6%与38.2%。3月份和丰水期浮游植物优势种主要为铜绿微囊藻、假鱼腥藻和线形粘杆藻等蓝藻种类,枯水期的1月、11月和12月主要以曲壳藻类、模糊直链藻、颗粒直链藻和梅尼小环藻等硅藻种类为优势种。
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A novel method for determination of benzoyl peroxide with spectrophotometry was developed. Inclusion ratio of β cyclodextrin to dibenzoy peroxide and benzoic acid is obtained with spectrophotometry.The mechanism of the inclusion was studied,too. The results showed that β-CD react with dibenzoyl peroxide to form a 1:1 or 2:1 host-guest complex, with the apparent formation constants of 5.0× 10~2and 2.5× 10~4 , respectively.β-CD reacts with benzoic acid to form a 1:1 host-guest complex with the apparent formation constant of 6.9 × 10~2 after the dibenzoyl peroxide was reduced by hydroxyl ammonium chloride.
建立了用β环糊精测定过氧化苯甲酰的分光光度法,并测定了β环糊精与过氧化苯甲酰和苯甲酸的包结比,随着β-CD浓度的增大,可与BPO分别形成1:1或2:1的包容络合物,包结常数分别为5.0×10~2和2.5×10~4,与苯甲酸形成1:1的包容络合物,包结常数为6.9×10~2;由于包结物的吸光度值比过氧化苯甲酰的吸光度值大大增加,建立了一种当β-CD存在下,在水溶液中测定过氧化苯甲酰的方法。
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Among all adhesion molecules sereted by endotheliocyte, intercellular adhesion molecule-1(ICAM-1) and vascular cell adhesion molecule-1(VCAM-1) have considerable effect on the occurrence and development of diabetic retinopathy.
在内皮细胞分泌的粘附分子中,细胞间粘附分子-1(intercellular adhesion molecule -1,ICAM-1)对糖尿病视网膜病变的发生和发展有着重要的作用。
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The positioning result of phase and broadcast ephemerides are gained using time-satellite differential model after canceling SA, the precision for 24 hours phase observation data is about 1.1 metre,the precision for 2 hours phase observation data is about 1.3 metre,the precision for 1 hour phase observation data is about 1.6 metre ,the precision for 20 minutes phase observation data is about 2.7 metre.
采用时星差模型得到取消SA后相位和广播星历的定位结果:用24小时的相位观测数据定位精度在1.1米水平;用2小时的观测数据定位精度在1.3米水平;用1小时的观测数据定位精度在1.6米水平;用20分钟的观测数据定位精度在2.7米水平。
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Without evaginate issueing eyelid, furrow of skin issueing eyelid decreases apparently, happen without any complication. 2 nurse nurse before 1 art of 2 · 1 effective psychology communicates 1 · of 2 · [before 1] hairdressing operation must each other communicate adequately, the requirement of art of adversary of the person that know an operation, have without scar hyperplasia tendency and menstruation history.
无下睑外翻,下睑皮肤皱纹明显减少,无任何并发症发生。2护理2·1术前护理2·1·1有效的心理交流[1]美容手术前必须彼此充分交流,了解手术者对手术的要求,有无瘢痕增生倾向以及月经史。
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The results showed that at the anaerobic phase, the PHB concentration in the cell and orthophosphate concentration of the anaerobic effluent obviously increased, the poly-P concentration in the cell decreased, and the cucci and bacilli with a size of 1.0~1.5 μm were dominant and formed grapy cellular cluster. At the anoxic phase, the PHB concentration and orthophosphate concentration decreased significantly, the amount of poly-P increased, and the elliptical cucci of 0.5~1 μm and spheral bacilli of 1.0~1.5 μm were dominant. At the aerobic phase, the PHB and orthophosphate concentration almost reduced to zero, the poly-P increased significantly, cucci appeared single or in pair, and the contour of sphere was blur and almost disappeared.
试验结果表明,在厌氧阶段,微生物细胞内PHB的量大幅提高,上清液中磷酸盐的含量上升,聚磷酸盐含量明显下降,粒径为1~1.5 μm、呈球状和棒状的菌群构成的葡萄状细胞簇占居优势;在缺氧阶段,微生物细胞内PHB的量下降,上清液中磷酸盐含量下降,聚磷酸盐含量上升,粒径为0.5~1 μm的椭球菌与1.0~1.5 μm的球杆菌占优势;在好氧阶段,微生物细胞内PHB的量较低或接近零,上清液中磷酸盐的含量接近零,聚磷酸盐含量明显上升,此时粒径1.0~1.5 μm的球菌以单个或成对出现,球菌不再饱满,呈现接近消失的状态。
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Mm,humeroradial joint cavity 0.69±0.44 mm, proximal radioulnar joint cavity 0.90±0.56 mm, thethickness of joint cartilage (joint cartilage of humerus 1.15±0.35 mm, joint cartilage of ulna 1.04±0.16 mm, joint cartilage of radius 0.98±0. 17 mm) and the collateral ligament (thickness ofthe ulnar collateral ligament 1.38±0.42 mm, thickness of the radial collateral ligament 1.32±0.42 mm) were all measured.
结果:肱尺关节腔为0.70±0.44 mm,肱桡关节腔为0.69±0.44 mm,桡尺近侧关节腔为0.90±0.56 mm;关节软骨厚度,骨关节软骨厚度为1.15±0.35 mm,尺骨关节软骨厚度为1.04±0.16 mm,桡骨关节软骨厚度为0.98±0.17mm;侧副韧带:尺侧副韧带厚度为1.38±0.42mm,桡侧副韧带厚度为1.32±0.42mm。
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The optimum reaction conditions were that the molar ratio of maleic anhydride and p-nitroaniline was 1.2:1, the volume ratio of toluene and DMF was 10:1, the amination temperature was 20~30℃ the cyclization temperature was 145~150℃ and the cyclization time was 6 h over; the amount of p-toluene sulfonic acid was 12% of total reactant mass, the amount of copper sulfate was 0.1~0.5% of total reactant mass, the amount of hydroquinol was 0.1% of total reactant mass.
得到的最佳工艺条件是:n:n为1.2:1,V:V为10:1;胺化反应温度为20~30℃,环化反应温度为140~150℃,环化反应时间为6h以上;对甲基苯磺酸用量为反应物总质量的1%~2%;硫酸铜用量为反应物总质量的0.1%~0.5%;对苯二酚用量为反应物总质量的0.1%。
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- 推荐网络例句
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I will endeavour to find you some assistance.
我尽力帮你找人帮忙。
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At first I only know bruck is the idol of American younglings, afterwards I returned back to Taiwan ,even in Beijing last year ,I saw her poster everywhere, I was so surprised at her charm.
起初我只晓得布鲁克雷德丝是美国少男少女崇拜的偶像,后来回台湾,甚至去年在北京,居然也四处看见她的海报,才惊讶她的魅力之大。
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Ah may dee:You are chinese living in a democratic country.
你是居住在民主国家的中国人吧。