查询词典 synthesis

The replacement of toxic and volatile organic solvents as reaction media or an efficient catalyst with environmentally acceptable alternatives are an area of tremendous importance in modern organic synthesis. Basing the review about solid-phase synthesis with simple separation, the liquid phase organic synthesis supported by the solution polyethylene glycol and the chemical reactions in the medium of PEG, herein we are going to study the synthesis of 1-amidoalkyl-2 -naphthols in presence of the solution catalyst or the solid catalyst and the synthesis of thiourea in PEG-400 medium.

难溶性载体试剂参与下的固相合成使分离操作简单易行；可溶性聚乙二醇支载下的液相合成显示出液相反应的稳定高效性，同时兼顾大分子聚合物容易沉降分离的优点；无毒且稳定的小分子PEG作为反应介质，往往表现出醚和醇的双重性质和功能。

It was observed after 24hrs of reaction that this lipase could compete very well with lipase from Candida antartica (93. 0％ for isoamyl butyrate synthesis and 95. 0％ for ethyl caproate synthesis) and lipase from Mucor miehei (75. 0％ for isoamyl butyrate synthesis and 93. 64％ for ethyl caproate synthesis).

反应24h后，来自Candida antartica脂肪酶合成丁酸异戊酯和己酸乙酯的转化率分别为93.0％和95.0％，来自Mucor miehei脂肪酶合成丁酸异戊酯和己酸乙酯的转化率分别为75.0％和93.64％。

By the algorithm, the surfaces are first divided into a series of mapping areas and synthesis areas using the constraints of the triangles' normal and texture attributes. Then the mapping areas are textured by harmonic mapping from the 2D mapping sample, by a patch-based synthesis method. Finally, the synthesis areas are textured by a triangle-based synthesis method.

首先以三角形法向量、切向矢量与纹理尺度为约束，将三角网格曲面分割为一系列映射区与合成区；然后用基于块的平面纹理合成方法生成大面积样图，用调和映射方法对映射区进行纹理映射；最后采用基于三角块的合成方法生成合成区纹理。

There are three main synthesis routes:direct synthesis of imines;one-pot synthesis of imine with oxidation;one-pot synthesis of imine with reduction.

主要有三种合成路线：直接合成亚胺；一锅法氧化合成亚胺；一锅法还原合成亚胺。

The word-to-sound rule and the structure of a speech database are modified during the implementation of TTS system, and then a filter algorithm based on part-of-speech is proposed to solve the polyphone problem. Prosodic research on Chinese characters plays a great role in speech recognition and speech synthesis system. In order to improve the naturalness of a speech synthesis system, the relationship among the sentence structure, the length of a sentence and the breath boundaries is analyzed and a breath boundary assigning algorithm based on such relationship is put forward. In addition, the author analyzes the process of a speech synthesis system and builds a prosodic markup language suitable for Chinese speech synthesis.

呼吸群边界划分作为汉语韵律的一种表现方式，它在语音感知和文语转换系统的性能方面起着十分重要的作用，作者在对汉语句法结构、句子长度和和呼吸群划分之间关系的研究基础上，设计并实现了基于句子长度和句法结构的呼吸群边界划分算法；为更好地描述文语转换过程，作者提出了适合汉语语音合成的SSML韵律标注语言，该标注语言不仅从声学层上对语音的韵律进行描述，而且从语言学层上标注句法结构信息，最后本文对基于语言理解的韵律规则用SSML进行了描述并用实验验证了语言学层面的标注对系统自然度的影响。

Main on-going research works include:"Expressive speech synthesis system","Spontaneous Speech Generation in Natural Human Computer Interaction"(863),"High performance distributed speech synthesis and recognition engine"(863),"The evaluation system of Chinese information processing"(863),"Multilingual speech synthesis system","emotional speech synthesis and classification","text independent voice conversion", etc.

当前正在进行的研究工作包括：具有表现力的语音合成系统，自然人机交互中的口语产生系统（863），高质量分布式语音合成和语音识别引擎的研究（863），中文信息处理评价系统（863），多语言语音合成系统，情感语音合成与情感分类，文本独立的语音转换系统等。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, acetochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、电化学法、乙醛酸钙法、尿素三氯乙醛合成法、尿酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

Based on broad information collection, author compared and studied on the old synthesis process, and proposed the better process that started from benzyl chloride, then according to the sequence of " synthesis of benzylamine, synthesis of N-benzyl-N--acetamine, synthesis of 2-chloro-5-methylpridine ,2-chloro-5-trichloromethylpyridine,2-chloro-5-trifluropyridine " five steps to get the final product, CTFP.

本文在查阅大量文献资料和对2-氯-5-三氟甲基吡啶合成路线进行分析比较的基础上，提出了较佳合成路线，即以氯化苄为原料，合成的反应步骤为&苄胺&合成、&N-苄基-N--乙酰胺&合成、&2-氯-5-甲基吡啶&合成、&2-氯-5-三氯甲基吡啶&合成、&2-氯-5-三氟甲基吡啶&合成五步。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, ace-tochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、化学法、醛酸钙法、素三氯乙醛合成法、酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

Based on these, an improving μ-synthesis is presented, with which the high-purity distillation is designed well. 2. The robust performance problem of MIMO plant is explained with the plant direction angle, which shows that the robust performance varies with different input uncertainties and the μ-synthesis should be applied correctly according to the uncertainty structure. 3. Condition number and bandwidth are the important items for robust performance design in MIMO system. The H〓 two-block problems can not deal with the robust performance design of MIMO system because of the condition number cancellation. A general μ-synthesis procedure for MIMO system with uncertainties is presented. 4. For the SISO system, the object function in robust performance is amplified by at most 〓 than that of H〓 two-block problems in value: So the robust performance of SISO system can be done with the H〓 two-block problems to avoid the complicated μ-synthesis procedure. 5. All the conclusions and methods presented in this paper are demonstrated by some typical design examples.

从而形成一种改进的μ综合方去，并对精馏塔病态对象进行了鲁棒性能设计，得到令人满意的结果；（2）利用对象的方向角解释了MIMO对象鲁棒性能设计出现问题的原因，并提出不同输入摄动形式下系统的鲁棒性能问题也并不相同，因此利用μ综合处理鲁棒性能设计时，应根据不同的摄动情况采用不同的结构进行设计：（3）条件数问题和带宽问题是MIMO系统鲁棒性能设计的两个主要问题，指出由于条件数对消的存在使得一般H〓两块问题无法处理MIMO系统的鲁棒性能设计，而μ综合方法则是处理MIMO系统鲁棒性能设计的有效方法，并给出了其处理MIMO系统鲁棒性能设计的一般性方法；（4）提出对于SISO系统H〓两块问题（S/T问题、S/KS问题）的设计指标函数与鲁棒性能设计的μ指标函数在数值上最大差〓倍，因此对于一般SISO系统的鲁棒性能设计可以简单地用一般的H〓的两块问题处理，而避免μ综合设计的复杂过程；（5）本文中提出的结论和算法都利用H〓/μ发展中的典型例子：Doyle-Stein问题，Safonov的战斗机模型，精馏塔对象等进行了设计验证。

The changes of the HAF after liver injury may be related to the volume of blood loss, the intraabdominal pressure and the pneumoperitoneum duration.

肝撞击伤伴失血后肝动脉血流量的变化与失血量、气腹压力以及气腹持续时间等有密切联系。

Reneging on our commitments to the world's poor cannot be an austerity measure, she said.

放弃我们给世界上的穷国的承诺不能成为一种紧缩措施。