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Raman spectrum of saturated aqueous solution of ammonium dimolybdate crystal was recorded, and compared with those of ammonium dimolybdate crystal , ammonium heptamolybdate crystal, saturated aqueous solution of ammonium heptamolybdate crystal and monomolybdate anion in aqueous solution respectively.

记录了常温下二钼酸铵晶体饱和水溶液的Raman光谱，并分别与二钼酸铵晶体、仲钼酸铵晶体、仲钼酸铵晶体饱和水溶液、水溶液状态下单钼酸根离子的Raman光谱进行了比较研究。

METHODS: 15 g/L silk fibroin solution was made by degumming, salvation and dialysis. Chitosan was dissolved in 2% acetic acid solution to prepare 25 g/L chitosan-acetic acid solution. Two solutions were mixed to prepare six silk fibroin/chitosan solutions, and mass ratio was 10: 0, 5: 5, 4: 6, 3: 7, 2: 8, 0: 10. These solutions were separately sucked in a 24-well plate. Following exhausting gas vacuole at 4 ℃, precooling was performed at -20 ℃ for 12 hours, followed by cryodesiccate for 30 hours.

通过脱胶、溶解、透析这3个主要步骤制成质量浓度为15 g/L的丝素溶液，将壳聚糖溶解在2%的醋酸溶液中制成25 g/L的壳聚糖-乙酸溶液，然后将两者混合，配制成丝素/壳聚糖质量比分别为10∶0，5∶5，4∶6，3∶7，2∶8，0∶10的6种溶液，分别吸入24孔板中，4 ℃排出气泡后，-20 ℃预冷冻12 h，再冷冻干燥30 h。

The method comprises heating up the lactic acid solution to gasify at 150-200 degree C, mixing the obtained mixed vapour of lactic acid and water with the carrier gas, entering into gas-solid catalytic reactor to get the reaction product gas by the action of a modified Y zeolite molecular sieve catalytic agent and dewatering after heating up the mixed gas to 200-450 degree C, obtaining the propenoic acid solution through gas-liquid dissociation after cooling the reaction product gas, obtaining coarse propenoic acid products form the propenoic acid solution by gas stripping, azeotropic distillation, extraction and rectification in turns.

其特征在于将乳酸水溶液加热至150～200℃气化得到的乳酸-水混合蒸气与载气混合，将混合后的气体继续加热到200～450℃后进入气-固相催化反应器中经改性Y沸石分子筛催化剂作用脱水得反应产物气体，反应产物气体冷却后经气液分离得到丙烯酸溶液，丙烯酸溶液再依次经过气提、共沸蒸馏或萃取、精馏得到粗丙烯酸产品。

The self-oxidation of pyrogallic is studied in the vesicle solution, DSB aqueous solution, and AOT aqueous solution, respectively.

在DSB/AOT自发形成的囊泡体系中，首先分别测定了相同盐度下单纯的DSB和AOT水溶液分别对邻苯三酚自氧化的影响。

The Ca2+ salt solution as a new regenerant was presented in this paper. The influences of the calcium salt proportioning, temperature, dosage and flow rate on anion exchange fiber regeneration were studied. High regeneration can be obtained with 0.5 mol/L CaCl2+8 g/L CaO+6.5 °Bx sucrose solution at 70～80 ℃, the dosage of the Ca2+ salt solution was about half of the raw decoloring syrup, the regenerant flow rate should be lower than that of the raw decoloring syrup. It was shown that stable decolorization rate and lower decline in exchange capacity could be achieved with the new regenerant. It performed more effectively than the traditional sodium salt regenerant with less discharge of waste water.

选用二价钙离子蔗糖溶液为再生剂，再生蔗糖脱色后的强碱性阴离子交换纤维，研究了再生液的配比、再生温度、再生液用量、再生液流速等因素对再生效果的影响，结果表明配比为0.5 mol/L CaCl2+8 g/L CaO+6.5 °Bx蔗糖的再生液在70～80℃温度下，再生剂的用量约为脱色糖汁的一半，流速应低于脱色时的流速时，再生效果优于传统的钠盐再生剂的再生效果，重复再生后的纤维脱色率能保持稳定，交换容量下降少，且再生液能回收利用，废水排放量小，是一种环保型再生液。

The Ca(superscript 2+) salt solution as a new regenerant was presented in this paper. The influences of the calcium salt proportioning, temperature, dosage and flow rate on anion exchange fiber regeneration were studied. High regeneration can be obtained with 0.5mol/L CaCl2+8g/L CaO+6.5 °Bx sucrose solution at 70~80℃, the dosage of the Ca(superscript 2+) salt solution was about half of the raw decoloring syrup, the regenerant flow rate should be lower than that of the raw decoloring syrup. It was shown that stable decolorization rate and lower decline in exchange capacity could be achieved with the new regenerant. It performed more effectively than the traditional sodium salt regenerant with less discharge of waste water.

选用二价钙离子蔗糖溶液为再生剂，再生蔗糖脱色后的强碱性阴离子交换纤维，研究了再生液的配比、再生温度、再生液用量、再生液流速等因素对再生效果的影响，结果表明配比为0.5mol/L CaCl2+8g/L CaO+6.5 °Bx蔗糖的再生液在70~80℃温度下，再生剂的用量约为脱色糖汁的一半，流速应低于脱色时的流速时，再生效果优于传统的钠盐再生剂的再生效果，重复再生后的纤维脱色率能保持稳定，交换容量下降少，且再生液能回收利用，废水排放量小，是一种环保型再生液。

2Soil column leachate experiment shows, soil texture and soil section form are the main factors affecting the nitrate leaching; in soil organic fertilizer produce a nitrate leaching process, during five-month experiment, nitrate content has be increasing in leakage solution, organic fertilizer applying decrease the pH and increase the electric conduction of leakage solution, there is positive action between nitrate content in leakage solution and electric conduction, which shows that nitrate-N accumulation during organic fertilizer applying is one of the main factors for soil salification; for decrease the leaching of the nitrate-N in soil, in sandy moisture soil the best amount of organic fertilizer should be 7.5～ 15 t·hm~(-2), in Loamy moisture

在小麦-玉米轮作体系上投入化肥氮300kg·hm~(-2)N和有机肥22.3t·hm~(-2)折N261.2kg·hm~(-2，能使农田氮素收支达到平衡，在兼顾环境效益的基础上获得了较高的产量效益。并通过肥料效应函数和硝态氮累积效应函数进一步预测最佳施肥组合，即化肥氮施用量为N226.5kg·hm~(-2)，有机肥用量为39.9t·hm~(-2)折N466.8kg·hm~(-2，其中小麦季施化肥氮105.85kg·hm~(-2)N、有机肥30t·hm~(-2)折N351kg·hm~(-2，玉米季施化肥氮120kg·hm~(-2)N，有机肥9.9t·hm~(-2)折N115.8kg·hm~(-2。同时，磷素平衡分析表明，在施用有机肥的基础之上，化学磷肥的施用量应适量的减少或不施。

And the extreme centrifugal force from the enlarged higher impeller stops the solution as it entering the higher impellr. At the same time, the full solution in the chamber stops the air mixed with the solution in the chamber to go down. This way masterly eliminates both big problems of vertical sealless pump, overflow at high pressure and bubbles at big flow.

上部叶轮时，即受加大之背叶的强大阻力而无法上升，但上部叶轮所卷入液体中的空气，却受阻於水室中贮满的液体而无法下降，如此巧妙地排除了立式无轴封泵高压时溢流，或大流量时吸入空气的两大难题。

A set of apparatus for determining solid-liquid equilibrium data at atmospheric pressure has been established. The solubility of sebacic acid in water, 20% ethanol aqueous solution, 50% ethanol aqueous solution, 80% ethanol aqueous solution and ethanol were determined. Wilson equation, ideal thermodynamics equation and λh equation were applied to describe solid liquid equilibria data.

建立了一套常压固液平衡测定装置，测定了癸二酸在水、20％乙醇-水溶液、50％乙醇-水溶液、80％乙醇-水溶液、无水乙醇体系中的溶解度，并用Wilson方程、热力学简化方程和λh方程模型对实验数据进行关联。

2 The analysis step by 125mL separatory funnel, a fartoo 0.1mL cadmiun forcultivation added liquid (equivalent 1 μ g cadmiun) and 50mL acetate (4%), and the other one is to join the 50.0mL sample lixivium, separatory funnel and 2mL in the seignette solution,-amoxycillin sodium hydroxide solution and potassium cyanide-2mL hydroxylammonium hydrochloride solution, each adding a reagent shake after.

9.2.2 分析步骤取125mL分液漏斗两只，一只加入0.1mL镉标准使用液(相当1μg镉)及50mL乙酸(4%)，另一只加入50.0mL样品浸泡液，分别向分液漏斗中各加2mL酒石酸钾钠溶液，10mL氢氧化钠－氰化钾溶液及2mL盐酸羟胺溶液，每加入一种试剂后均须摇匀。

Chimborazo and Cotopaxi, took me by the hand.

越过琴博腊索山和科托帕克西山。

This car is in a good condition.

这辆车的状况很好。