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By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

Vogel law and the initial solution than the beginning of the smallest element method Only solution is closer to the optimal solution.

而伏格尔法得到的初始解比最小元素法的初始解更接近最优解。

In order to investigate the physical attack of different crystal products of sodium sulfate solution including Na2SO4 ments were carried out by partial soaking with 150 g/L sodium sulfate solution and an index was introduced to evaluate the resistance of mortar to physical attack of sodium sulfate solution.

采用150 g/L的硫酸钠溶液半浸泡的试验方法,以砂浆抗蚀系数为指标,研究了相对湿度和温度变化条件下,硫酸钠溶液的不同结晶产物Na2SO4与Na2SO4·10H2O对砂浆试件的物理侵蚀作用和不同条件下硫酸钠溶液的物理侵蚀特性及相关机理。

In Chapter two, it is given of the three-dimensional boundary element and the boundary element space, Sobolev space for the contact boundary element problem with friction; it is proved of existence and uniqueness of the solution by variation inequality for the contact Boundary Element Method matrix equation under two kinds of condition that the contact zone is fixed and the contact zone is increasing along with the load; it is given of the expressionfor the error of the exact solution and the boundary element solution.

第2章,给出三维边界单元及边界元空间、有摩擦接触边界元问题的Sobolev空间,利用变分不等式证明了不变接触区和随载荷可变接触区两种情况下的接触边界元法矩阵方程解的存在唯一性,给出了准确解与边界元解的误差表达式,还证明了三维弹塑性摩擦接触问题凝缩矩阵解的存在唯一性,为三维弹塑性摩擦接触边界元法奠定数学基础。

The conclusion was drawn by the synthesis of molecular sieve: after mixed soluble glass and aluminium sulfate with proper proportion under room temperature, it was stirred stormily to react. And then we mixed with potassium hydroxide solution after filtrating. At last, the molecular sieves of potassium type was synthesized after the mixture reacted in the oven or autoclave for 24 hours. The molecular sieve was remodeled more than twice with ammonium chloride solution that the concentration was 3mol/L and then remodeled twice with the saturated sodium chloride solution. Finally the molecular sieve was changed into the sodium type. It was named W zeolite.

通过对分子筛的合成得到:以泡花碱、硫酸铝为原料,以硅铝比按一定比例于室温下将二者混合,激烈搅拌,抽滤后与氢氧化钾溶液混合放于烘箱或高压釜中高温晶化24小时,晶化后的分子筛为钾型,先后用3mol/L氯化铵溶液和饱和食盐水各对其改型两次以上,最后改为钠型,可制得W型沸石分子筛。

The suitable detection wavelength was selected through qualitative determination of wave spectrum. With 95% ethanol as the reference solution, the standard curve was drawed with a series of different concn. of standard solution of chlorogenic acid, and the Absorbance of extracting solution was determined and the chlorogenic acid content in filtrate was calculated.

波谱定性检验选择适宜的测定波长,以95%乙醇为参比溶液,用配制好的一系列不同浓度的绿原酸标准溶液绘制标准曲线,测定提取液的吸光度,计算滤液中绿原酸的含量。

To realize the simple and accurate measurement of solution density,the calculation formula for solution density was deduced after establishing the relation between solution pressure and density.

为了实现对溶液密度的简单、精确测量,建立了溶液压力与溶液密度之间的关系,推导出溶液密度的计算公式,确定了利用差压传感器来实现对溶液密度的间接测量,指出了测量的难点和解决的方法。

To realize the simple and accurate measurement of solution density, the calculation formula for solution density was deduced after establishing the relation between solution pressure and density.

摘 要:为了实现对溶液密度的简单、精确测量,建立了溶液压力与溶液密度之间的关系,推导出溶液密度的计算公式,确定了利用差压传感器来实现对溶液密度的间接测量,指出了测量的难点和解决的方法。

The solution for the non-stationary system is obtained through the stationary disturbed system. The gradients of the system performances to all design variables are derived and they can be used to obtain optimal solution of the systems. More generally, if the performance of the system is a function of the solution of a set of generalized Lyapunov equation, then the gradients of the performance function to the coefficient matrices of the equation can be found in closed form.

文中显示,非静态干扰系统的解可由静态干扰系统求得,而此干扰系统之最佳解,则经由本文所推导的对所有设计变数之系统性能函数梯度获得;一般而言,如果系统之性能函数是一组通式化 Lyapunov 方程式解的函数,则此方程式的系数矩阵之性能函数梯度,可用封闭解表示之。

Aiming at the problem that solution FEMequation set needs too much memory, segregated solotion methOd has beenadopted and for the first in China E l em ent- B y- E lement has been introduc edwhen solving flow field parameter equation sets. EBE technology need notassemble and store the global stiffness matrix, and minish effectively memoryrequires of solution equation set, moreover it has inherent high parallelity, andadvance equation solution.

针对求解流场有限元方程组占用计算机内存资源过多、限制求解规模的缺点,采用分离式求解法,在求解流场各参数方程时,在国内首次引入EBE技术,EBE技术不必组集和存储总刚矩阵,能有效地减小了方程组求解时对内存空间的要求,同时EBE技术具有内在的高度并行性,能有效提高方程组的求解速度。

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Don not attempt to do something which you can not to do.

不要企图做那些办不到的事情。

The expression of CTGF and TNF-αweredetected by immunochemistry and the number of Clara Cells was calculated.

光镜下观察肺组织的病理变化,采用免疫组化染色观察肺组织中结缔组织生长因子和肿瘤坏死因子-α的表达和Clara细胞的数量。

The latest results are published online January 13 in the Journal of the National Cancer Institute. They come from a case–control study that involved 459 cases,"which, for the rarity of this cancer, is a very big study," Dr. Stang said.

Stang医师表示,这项最新的研究结果线上发表在1月13日的国家癌症机构期刊上,研究来自一项收纳459个病例的病例控制研究,这是一项非常大的研究。