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A process for the preparation of trimesic acid by the catalytic oxidation of mesitylene with air in liquid phase was presented in this paper.

介绍以均三甲苯为原料,采用液相空气氧化法制取均苯三酸的工艺方法。

In this paper, the studies on the preparation of high pure mesitylene usingMTBE tail gas are made in both experimental and theoretical, different factorsaffecting the alkylation reaction to produce mesitylene by MTBE tail gas areinvestigated, the optimal condition of reaction is defined and the alkylationreaction kinetics of different components are studied, moreover, the comparisonbetween C4 raffinate oil and isobutene used for alkylation agent is made too.

本文对MTBE尾气烷基化法制备高纯度均三甲苯过程进行了实验研究和理论分析,确定了不同因素对烷基化反应的影响,得到了MTBE尾气制备均三甲苯的最佳反应条件,并对不同组分的烷基化反应动力学进行了研究。此外,对乙烯C4抽余油和异丁烯做为烷化剂的实验结果进行了分析和比较。

The most common method for determination of drug residues in surface water is GC-MS,which often requires derivatization as a sample preparation step.

测定地表水中药物残留的最常用方法是GC-MS,它需要一个衍生步骤。

This invention publishes a preparation method for methyl acetate and a reaction distillation column with combined trapezoid spray trays.

本发明公开了一种乙酸甲酯的制备方法和具有立体传质塔板的反应精馏塔。

The influences of preparation method, the calcined temperature and auxiliary forming reagent on the activity of the Fe Mo Co O catalyst for oxidation of methylal to formaldehyde were studied.

考察了制备方法、焙烧温度和成型助剂对甲缩醛氧化制甲醛铁钼钴三元催化剂活性的影响。

A process for preparation of the potassium methylate with the potassium-mercury amalgam and methanol using Fe/C as catalyst was provided.

本文主要研究了甲醇与钾汞齐在铁/碳催化剂作用下合成甲醇钾的工艺。

Due to the ability of the bivalent magnesium cation to form stable chelate complexes with carbonyl compounds,magnesium methylate for example is used as a selective carbonyl condensing agent. Three synthesis routes was proposed based on literatures and comprehensive comparison with other ways. First,Magnesium methylate is prepared by reacting magnesium metal with dry methanol.The magnesium salts of"higher"primary alcohols,i.e.alcohols with ≥ 2 carbon atoms,do not react directly with pure alcohols under normal conditions.In fact catalysts are required to set the reaction in motion and the preparation is performed under pressure at the higher temperatures.

一、直接合成法:本文将镁与无水甲醇直接反应制得甲醇镁;"更高级"的醇(比如C≥ 2的醇)在无催化剂的条件下无法直接和镁进行反应,本文以CCl4为催化剂将无水乙醇与镁直接反应制得乙醇镁,但是以原甲酸三乙酯为催化剂无水乙醇与镁无法反应;不论是以CCl4为催化剂还是以原甲酸三乙酯为催化剂,丙醇均无法与镁直接反应。

Due to the ability of the bivalent magnesium cation to form stable chelate complexes with carbonyl compounds,magnesium methylate for example is used as a selective carbonyl condensing agent.Three synthesis routes was proposed based on literatures and comprehensive comparison with other ways.First,Magnesium methylate is prepared by reacting magnesium metal with dry methanol.The magnesium salts of higherprimary alcohols,i.e.alcohols with ≥ 2 carbon atoms,do not react directly with pure alcohols under normal conditions.In fact catalysts are required to set the reaction in motion and the preparation is performed under pressure at the higher temperatures.

一、直接合成法:本文将镁与无水甲醇直接反应制得甲醇镁;"更高级"的醇(比如C≥2的醇)在无催化剂的条件下无法直接和镁进行反应,本文以CCl_4为催化剂将无水乙醇与镁直接反应制得乙醇镁,但是以原甲酸三乙酯为催化剂无水乙醇与镁无法反应;不论是以CCl_4为催化剂还是以原甲酸三乙酯为催化剂,丙醇均无法与镁直接反应。

A new technique for rapid 3D microstructure preparation using micropipette is investigated.

本文提出了一种利用毛细管微探针进行快速制备三维微结构的新方法。

Midori responsible for the research and development staff have years of experience and the high title of the post, they rooted in their location, as in the past are dedicated to the preparation of the code.

负责此次Midori的研发人员都有着多年的经验和很高的职位头衔,他们扎根于自己的所在地,正在像过去那样兢兢业业地编写代码。

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In this paper, the requirement analysis, design and implementation of the system are introduced in detail.

此论文详细介绍了系统的需求分析,系统设计和具体实现。

In the context of economic globalization is increasingly deepening, China's economy can not be spared.

在经济全球化日益加深的背景下,中国经济不可能做到独善其身。

Results:(1)Increased expression of ICAM-1 appeared in cultured endothelial cells after anoxia and enhanced after reoxygenation.

结果:(1)体外培养的内皮细胞缺氧后ICAM-1表达上调,随复氧时间的延长ICAM-1呈增强趋势。