查询词典 one-step method

All synthetic methods of the μ-oxo-bismetallo- tetraphenylporphyrins are comprehensively discussed, involving the two-step method, the chromatographic column method, the one-step method, the auto-oxidation method and the one-pot method developed by our group.

重点介绍了μ-氧代四苯基双核金属卟啉的合成方法，即两步合成法、柱色谱分离法、一步合成法、自氧化法以及本课题组最新开发的一锅法。其中一步合成法和自氧化法由于具有适用范围广、收率高等优点，将成为μ-氧代四苯基双核金属卟啉的主要合成方法。

Firstly, this paper investigated roundly the basic theory of the ambient vibration method, analyzed systematically the main methods of ambient vibration identification, and discussed their advantages and disadvantages. Then we established the finite element model of structural dynamics and test model and analyzed their mutual relation, improved MUSIC method and correlation function method in the harmonic identification, and gave the subspace method and correlation function method based on continuous model, which is multi-harmonic retrieve technique. And then, this paper also puts forward least-squares method to estimate directly structural physical and modal parameters; this approach replaced the derivative operator in the continuous time model with an equivalent approximation, and estimated the physical parameters of structures by the least-squares method. And then, we discussed the approximation methods of derivative and their convergence. Finally, this paper researched the modal parameters of a frame structure by the simulation and test. The results demonstrated that subspace method, correlation function method and the least-squares method are effective and stable respectively.

全面地研究环境振动识别方法的基本理论，系统地分析环境振动识别方法的主要方法，讨论它们的优点和不足；建立结(来源：6666AB44C论文网www.abclunwen.com)构动力学的有限元模型和试验模型，分析有限元模型与试验模型之间的相互关系；改进谐波识别中的MUSIC识别方法和相关函数识别方法，给出大型结构模态识别的连续型的子空间分解识别方法和相关函数识别方法，这个方法是多元谐波识别方法；提出直接识别结构的物理参数和模态参数的最小二乘方法，这个方法利用导数的近似值代替导数值，并运用最小二乘方法识别结构的物理参数，讨论导数近似值的选择方法，分析算法的收敛性；通过仿真计算和模型实验，研究高层框架结构的模态参数识别，验证子空间分解识别方法、相关函数识别方法和最小二乘识别方法的有效性，算法的稳定性；从理论和试验两个方面分析和研究噪声对识别精度的影响，影响识别精度的因素，以及部分模态成分的模态参数不能够被识别的原因。

The revised Hargraves formula has the best result compared with Penman-Monteith formula, the average relative error is 6%, moreover, Hargaves method requiring the least data in calculating ETo, so this method has the high actual application value; The following are Radiation method and Blaney-Criddle method ; The worst is the Pan method, even after revised, the highest and average relative error is 36% and 10%, respectively. So, in this study, Penman-Monteith method, Radiation method, Blaney-Criddle method and Hargraves method are used except Pan method.

在这四种方法中，修正后的Hargraves方法与彭曼—蒙特斯方法的计算结果符合最好，其平均相对误差为6％，而Hargraves方法需要的气象数据只有计算时段的最高、最低温度，该方法具有较高的实际应用价值；辐射方法和布兰尼—克里德尔方法次之；蒸发皿方法最差，即使在修正后，E601型蒸发皿的最大误差也高达36％，平均为10％，所以在预报系统的研究设计中采用了除蒸发皿方法之外的四种方法。

The primary studying works and characteristics:1 To summarize reinforcing theory of cement mixing pile composite foundation2 To analyze the primary mechanics characters and changing rules of cement mixing pile, based on analysis of test data both indoor and outdoor.3 To discuss siding frictional resistance, ending resistance, ultimate bearing capacity of simple mixing pile and effectiveness factor of grouped piles, loading ratio of soil between piles under cushion cap of grouped piles and stress ratio of pile and soil and so on, and use many computation method and experimentation method to ensure bearing capacity of mixing piles composite foundation.4 To point out and analyze eight sides flaws and problems of the bearing capacity calculation method of mixing pile compositefoundation which ensured by national and normative method/ formula.5 To apply test results of loading tests and a few settlement observation data, use gray theory to predicate ultimate bearing capacity of deep mixing piles, actual example demonstrate engaging between theoretical predicted value and actual value.6 To apply groovy layerwise summation method to discuss entity piles method, double foundation method, equivalent layerwise summation method and consolidation theoretical method and so on, especially by combination of engineering example, use FEM to calculate or discuss the settlement and changing rules of composite foundation.7 To discuss problems of critical length of composite foundation by combination of engineering example and numerical analysis method, and analyze the contrast of critical length between simple pile load and most area load of composite foundation, not only critical length of composite foundation is relative to modulus ratio between piles and soil, but also upside load distribution area of composite foundation.

主要的研究工作与特色为：(1)总结了水泥搅拌桩复合地基的加固原理；(2)在对室内外试验资料进行统计分析的基础上，系统分析了搅拌桩水泥土的主要力学特性及其变化规律；(3)探讨了搅拌单桩的侧摩阻力、端阻力、极限承载力及群桩效率系数、群桩承台下桩间土荷载分担比及桩土应力比等，提出用多种计算方法并结合试验方法来综合确定搅拌桩复合地基的承载力；(4)明确指出和分析了按国家有关规范的方法确定搅拌桩复合地基承载力所存在的八个方面的缺陷与问题；(5)利用过去没有加载至破坏阶段的载荷试验成果和较少的沉降观测数据，尝试了用灰色理论预测深层搅拌桩的极限承载力，实例表明理论预测值与实测值吻合较好；(6)在常规分层总和法的基础上，探讨了复合地基沉降计算的实体墩基法、双层地基法、等效作用分层总和法、固结理论法等，特别是结合工程实例，用有限元数值计算等方法计算和讨论了搅拌桩复合地基的沉降及其变化规律；(7)结合工程实例，用数值分析方法探讨了复合地基临界桩长的问题，指出和分析了单桩荷载下的临界桩长与复合地基大面积荷载下的临界桩长存在很大的差别，复合地基的临界桩长不仅与桩土模量比有关，而且与复合地基上部荷载分布面积有关。

Because of the problem of convergence, the key techniques to complete the one step simulation were explored thoroughly. The geometry mapping method based on finite element model and inverse deformation was developed to get the approximate initial blank for one step simulation. The effective selection of convergence factor in Newton-Raphson method was studied. The divergence criterion in iterative process for one step simulation was put forward. Also the countermeasure to ill equations coefficient matrix was studied.

由于存在收敛性的问题，本文重点研究了一步模拟方法计算机实现的关键技术：提出了基于有限元模型的几何映射方法和反向变形方法来确定初始毛坯的近似解，研究了带收敛因子的Newton-Raphson方法中如何高效地选取收敛因子，提出了一步模拟迭代求解过程中的发散准则，并研究了病态方程组系数矩阵的修正方法。

For household users to establish simple antifreeze dilution disposal ways of applying gender-controlled embryo freezingly-preserved technique by one-step vitrification dilution method,A,B,and C structure approaches of liquid layers in canaliculi were applied to investigate their survival capacity after embryos freshly-split by one-step dilution;and minimum capacity refrigerant method in specific canaliculus and above structure approach of liquid layer B were also applied to compare their survival capacity of frozen and melted embryos freshly split,and frozen and melted IVF embryos splited by one-step dilution.

为了创立在用户庭院就能应用的玻璃化保存性别控制胚胎的冷冻剂稀释处理方法，采用细管内3种不同液体层构成法，对新鲜分割胚一步法稀释后的存活能力进行了研究；其次用特定细管最小容量冷却法与上述3种不同液体层构成中效果较好的B法对玻璃化冷冻溶解的新鲜分割胚、体外受精分割胚及冷冻溶解的体外受精分割胚进行一步法稀释后的存活能力予以对比。

This project was established based on the first cooperative development of optical in situ real time detecting technique probing the atomic scale layer-by-layer epitaxy growth of oxide film. Over the last three years, we have given full play to the advantages and characteristics of both sides and have finished the assumptions and plans of this subject satisfactorily. 1. In Institute of Physics, we set up advanced oblique-incidence reflectivity difference equipment and wrote one data acquisition procedure that made the simultaneous detection of optical signal and RHEED signal into reality. 2. The first observation of sustained oscillations over hundreds of monolayers in both real and imaginary signals during the epitaxy growth of SrNb0.1Ti0.9O3 on SrTiO3 substrate in LMBE testifies that oblique-incidence is an excellent method to detect and monitor film epitaxy growth real time. 3. For the first time, we verify that oblique-incidence reflectivity difference method can be used to monitor the layer-by-layer growth mode during continuous growth through the correspondence between optical signals to atomic or molecular step edge density on the growth surface. 4. Phenomenological analysis shows that optical signals comprise three parts, the first is proportional to the average thickness of the film and depends on the bulk phase dielectric response; the second is proportional to the coverage of terraces and depends on the dielectric response of atoms or unit cells in the terrace; the third is proportional to the coverage of step edges and depends on the effective dielectric response of atoms or unit cells at step edges. This makes oblique-incident reflectivity difference technique a quantitative macroscopic method to monitor film growth.

中文摘要：本课题是在合作首次发展了氧化物薄膜原子尺度层状外延生长光学原位实时探测方法的基础上立项的，三年来，我们充分发挥双方的优势和特点，圆满完成了课题的设想和计划。1、在物理所建立了一套先进的光反射差法装置，编写了计算机系统的数据采集程序，实现了两路光学信号和RHEED数据的同步采集和显示。2、用激光分子束外延在SrTiO3基底上生长SrNb0.1Ti0.9O3薄膜，首次观测到连续外延几百个原胞层，周期振荡的光反射差实部和虚部信号，证明了光反射差法是一种能原位实时探测与监控薄膜层状外延生长的好方法。3、首次验证了通过对生长表面原子或分子台阶密度的响应，光反射差法可用于原位实时监测在连续生长条件下薄膜的层式生长模式。4、通过唯象理论的研究，证明光反射差信号由三项组成，第一项只与薄膜的平均厚度和宏观光学电介质常数有关；第二项与分子台阶面覆盖度和台阶面上分子层的光学电介质常数有关；第三项与台阶边缘的覆盖度成正比，并和在台阶边缘的分子的有效光学介电常数有关。

No sleep no time no mercy i gotta hit em low low ground i'm low key when i spit it less carb more protein my body fitted one step to two step the routine no sign of morphine my body need iy take a trip to oc to cop live it just sip the caffeine i gotta get it one step to step the routine got it now it's going down now no time dont mess boy let's show you how just to move it let me show you just to groone now come inside let me show you how no time dont mess around boy let show you how just to move it work it out lets do girl so flwxible, accessible so hot like the sunshine mexico just feel the beat mr.bexter flow so hot so hot hot check the routine work it out just work it out mr.bexter jc turm it out sing it so fly show you what i'm about so hot so hot hot check the routine got it now it's going down now no time dont mess boy no time baby dont mess around check the routine now lets get down come inside let me show you how no time dont mess around boy no time baby dont mess around check the routine now lets get down

没有睡的时间没有怜悯我得打时间低低地，我低调，当我吐出来减少碳水化合物的蛋白质我的身体装一步一步的两个常规没有迹象吗啡需要我的身体是Iy 采取以法团，前往现场有警察刚喝咖啡因我得得到它一步步走向常规现在得到它现在下降没有时间请勿乱男孩让我们告诉您如何只将它让我告诉你现在只是groone 里面让我来告诉你如何周围没有男孩的时间请勿乱让我们告诉您如何只将它的工作中可以做女孩如此flwxible，访问这么热的阳光一样墨西哥只是觉得节拍mr.bexter流这么热这么热热例行检查工作，这只是工作中出 mr.bexter Jc的页转到出来这样唱飞告诉你什么，我对这么热这么热热例行检查现在得到它现在下降没有时间请勿乱男孩没有时间大约婴儿请勿乱现在的例行检查可以坐下里面让我来告诉你如何周围没有男孩的时间请勿乱没有时间大约婴儿请勿乱现在的例行检查可以坐下

Studied the effect of quality of the one step liquid to the second step fermentation rate and periods first time, confirmed the effect factor of the one step leavens process versus the second step.

首次研究了从一步发酵工艺的醪液质量对二步发酵的收率及周期影响，并确定了一步发酵工艺对二步发酵工艺影响因素。

On one side, it criticizes the traditional way of value view education in our country including the critique to dualistic-opposition method, the rejection to formalism method and the sublating to indoctrination method. On the other side, it argues the application of value view education including both drawing lessons from traditional persuading methods, model demonstration method, edification method, self-cultivation method and applying to the dilemmatic story method, character-acting method, value-clarifying method.

最后，对价值观教育方法的运用进行了分析，一方面，对我国传统价值观教育方法进行了检讨，它包括对非此即彼二元对立方法的批判，形式主义方法的拒斥和灌输方法的扬弃；另一方面，论述了我国价值观教育方法的运用，它既包括对传统的说服教育法、榜样示范法、陶冶教育法和自我修养法的借鉴，又包括对两难故事法、角色扮演法和价值澄清法等新方法的运用。

"Second Life is remarkably easy to work with, and is very popular,"

"第二次生命是显着容易的工作，并且很受欢迎，"

For example, we usually assume that materials are homogeneous and isotropic and free of internal defects or flaws.

为了得到适合有限元分析的模型，我们必须经过如图2所示的简化步骤。