查询词典 glucamine

The operation condition of N-methyl glucamine is, columniation temperature is 30℃, detection temperature is 35℃, flow rate is 0.3mL/min, the mobile phase is methanol: water (2% trifluoroacetic acid)=5: 95 .

确定的色谱操作条件为核糖胺：柱温30℃，流速0.7mL/min，检测波长244nm，流动相甲醇：水=40：60；葡甲胺：柱温30℃，检测池温度35℃，流速0.3mL/min，流动相为甲醇：2％三氟乙酸水溶液=5：95。

The HPLC methods for analysis of N--ribitylxylidine and N-methyl glucamine were established. After optimizing the operation conditions, the principal product and main impurities were well separated. And they were determined by LC-MS. The operation condition of N--ribitylxylidine is, columniation temperature is 30℃, flow rate is 0.7mL/min, UV wave is 244nm, the mobile phase is methanol: water=40: 60 .

首次建立了对葡甲胺和核糖胺的高效液相色谱分析方法，通过对色谱操作条件的优化，成功分离了主产物和杂质，在此条件下，应用液相色谱-质谱联用仪对糖基胺及生成杂质进行了指派定性，并测定了两种糖基胺及其主要杂质的含量，获得了满意的结果。

N-(2-hydroxyethyl)-glucamine was dehydrogenated to 6-(2-droxyethyl) amino-6-deoxy-a-L-sorbofiuanose the key intermediate of miglitol by the resting cells of Gluconobater oxydans Gouv2007 through aeration. 6-(2-Droxyethyl) amino-6-deoxy-a-L-sorbofiuanose was hydrogenated catalyticlly to miglitol. In the transformation of N-(2-hydroxyethyl)-glucamine to miglitol, the transformation rate was 77.3%.

氧化葡萄糖酸杆菌Gouv2007的静息细胞在通气下氧化N-羟乙基葡糖胺脱氢生成米格列醇的前体物质6-脱氧－6-羟乙基氨基－α-L-呋喃山梨糖，再催化加氢生成米格列醇，对从N-羟乙基葡糖胺生成米格列醇的底物转化率为77.3%。

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具有扎实的专业知识和很强的适应能力，能很快投入到自己的工作。