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In this paper, acetylsalicylic acid, cyclohexanone Preparation of micro-content of the experimental design, in different reaction conditions were carried out under analysis to optimize the improvements and chemical experiments on the basis of conventional experimental and micro-experimental comparison, being The experimental results consistent with the premise, fully reflects the micro-chemistry experiments to save time, save the amount of reagents, as well as many advantages such as reducing environmental pollution.

本文阐述了乙酰水杨酸、环己酮微型化制备实验的设计内容,在不同反应条件下进行了对照分析,从而进行优化改进,并就基础化学实验中常规实验与微型实验进行比较,在得到一致的实验结果的前提下,充分体现了微型化学实验节省时间、节省试剂用量、以及减少环境污染等诸多优点。

Structural Experiment is a basic subject in the Structural Engineering Major, which weighs heavy to the studying researchers on the experimental data accompanied by the former researchers" achievement and lucubration. And the experimental scope is expanding wider, so that making full use of each laboratory"s experimental equipment to conduct the collaborative experiment is also the developing trend. With the rapid development of the computer and network technology, hardware technique has provided the accessible condition for the Structural Experiment, and database technique has offered the convenience and possibility for the experimental results and datas save and data exchange.

结构实验是结构工程专业的一门基础学科,而且随着研究的深入,前人的研究成果,特别是研究试验数据对于继续研究的人员来说有特别重要的意义,并且实验规模也在不断扩大,充分利用各个实验室的实验设备条件进行协同实验也是发展趋势,随着计算机技术以及网络技术的飞速发展,硬件技术都为这一切提供了可行的条件,数据库技术为结构实验提供了保存实验结果、实验数据以及实验数据交换提供了便利和可能。

RESULTS: Totally 57 rats enrolled in this study, all animals completed Hot pain allergic symptom could not be observed on rats in experimental group during the whole experimental process, but continuously appeared in discharge percentage of nerve fibers at the central end of experimental rat sciatic nerve was remarkably lower than that of the control group 6.79%Sympathetic postganglion nerve fiber budding was not obvious in the slices of entire L4-5 dorsal root neuroganglion of injury side in 6 experimental rats,and basket-shaped cell could not be observed, but sympathetic postganglion nerve fiber budding was obvious in 2 rats in control groups with altogether 41 basket-shaped cells observed.

电生理实验:实验组大鼠坐骨神经中枢端的神经纤维自发放电百分数显著低于对照组(6.79%,46 7%)。③背根神经节切片荧光染色结果:实验组6只大鼠损伤侧L4-5的全部背根神经节切片中看不到明显的交感节后神经纤维芽生,没找到篮状细胞,而在对照组2只大鼠损伤侧L4-5的全部背根神经节切片中可看到明显的交感节后神经纤维芽生,共找到篮状细胞41只。

Electrophysciological indexes: in the experimental group ,the tardy rate of induced motorius action potential ,recovery rates of the amplitude of compound muscle action potential and twitch tension and tetanic tension of triceps surae muscle ,were significantly higher than in the control group.(4) Compared with the control group ,the triceps surae muscle wet weight was significantly greater in the experimental group.(5) histomorphological indexes: the count of myelinated nerve fibers ,diameter of regenerated axon,thickness of nerve myelin sheath and area of capillary were much more in the experimental group than in the control group.(6) observation of ultrastructure with the transmission election microscope: more abundant organella and maturer myelin sheath lay in the injured peripheral nerve of the experimental group, while not lay in the control group.

分别在术后第2、4、6周时进行各项指标的检测,结果发现:(1)实验组SD大鼠在整个实验过程中,其精神、毛发、体重,运动灵活性等一般情况优于对照组;(2)实验组的坐骨神经功能指数恢复率显著优于对照组,P<0.01;(3)神经电生理指标:实验组运动神经诱发电位潜伏期的延迟率显著优于对照组,P<0.05;复合肌肉动作电位振幅的恢复率显著高于对照组,两组比较第2周时P<0.01,第4、6周时,P<0.05;小腿三头肌单收缩力和强直收缩力的恢复率实验组显著高于对照组,P<0.01;(4)小腿三头肌湿重的恢复率,第2、4周时实验组高于对照组,差异非常显著,P<0.01;第6周时,差异仍显著,P<0.05;(5)组织形态学指标:有髓神经轴突计数、再生轴突直径的恢复率,毛细血管面积,实验组均显著大于对照组,P<0.01、P<0.05、P<0.001;实验组髓鞘厚度的恢复率也显著高于对照组,第2周时P<0.01,第4、6周时,P<0.05;(6)透射电镜超微结构观察:实验组再生轴突中细胞器丰富,髓鞘结构成熟,神经再生情况优于对照组。

Thirty-six rats ,weighing(250±10)g, were randomly divided into normal group, experimental group and control group.Orthodontical devices were put between the upper incisor teeth and dens molaris in both experimental group and control group.The corrective force was adjusted to 60g.Salvia miltiorrhiza combination was implanted to each rat in the experimental group every day.The animals of both experimental group and control group were killed at 7,14 and 21 days.The upper dens malarias and periodontal tissue slices were observed under the light microscope and transmission electro microscope,and the X-ray dental films were taken and measured with digitization dental scanning apparatus and its software.

以36只体重(250±10)g的雄性大鼠为样本,随机分为正常组、实验组和对照组,设定不同浓度丹参复合膜,以同体对照方式在正常组进行体内植入实验,在2周内观察不同浓度丹参的牙周组织诱导作用,寻找最佳应用浓度;在实验组和对照组的上切牙与磨牙之间隙安装正畸装置,建立大鼠磨牙移动实验模型,矫治力的大小为60g;实验组每日每只体内植入丹参复合生物膜,两组动物于正畸加力7、14、21d,分三批处死;处死后立即切取双侧上颌磨牙及牙周组织制取标本,制片透射电镜和光镜观察;拍摄X线牙片,用数字化牙科扫描仪及软件对其进行测量分析。

The mice in experimental group and control group were exposed to 350 cGy radiation produced by 60Co. After 3 h, karyocytes at different concentrations in the fresh human umbilical cord blood were injected into the mice in experimental group A, B, C via their tail veins, and the equal volume of normal sodium was also injected into control group via tail veins. After one month, carbon tetrachloride (CCl4) was injected into experimental group A, B and control group via abdominal cavity, and the equal volume of normal sodium was injected into experimental group C. After two months, immunohistochemistry and reverse transcriptase polymerase chain reaction were used to detect the expressions of human cytokeratin-18 (CK18), cytokeratin-19 (CK19) and albumin in liver tissues of all mice.

采用60Co治疗仪γ射线对实验组和对照组行350cGy的亚致死剂量照射,实验组A、B、C3组照射后3h内经尾静脉分别输入1.0×10^7个/只、2.0×10^7个/只和3.0×l0^7个/只人新鲜脐血有核细胞,对照组经尾静脉注入等体积无菌生理盐水。1个月后对实验A、B组和对照组裸鼠经腹膜腔注射四氯化碳(CCl4),实验C组注射等体积生理盐水。2个月后采用免疫组化和RT-PCR方法检测裸鼠肝组织人源性CK18、CK19和人源性白蛋白的表达。

This paper to introduce a new experimental method of dispersion phenomena, in this experimental method, it can be directly observed by different substances uneven medium, the dispersion arising from the various phenomena of the material in different light source through uneven medium, the emergence of two different spectral dispersion surface, spectral noodles Bright (Bright-Line Spectrum), and dark lines is how it is formed and a series of important experimental phenomena.

本文要介绍一种新的色散现象出现实验方法,在这种实验方法上,可直接观察到不同物质通过不均介质后,所出现的各种不同色散现象,物质在不同光源照射下通过不均介质后,出现的两种不同色散谱面,谱面中明线和暗线是怎样产生等一系列重要实验现象。

In addition, some modifications on several computational methods are also presented. Using LMTO method the electronic structure of several systems are studied, and some results are obtained. They are: The ideal Nb (100) surface has three surface states, the multi-layer relaxed surface has two surface states. The surface energy of the ideal surface is higher than that of the relaxed surface, that means that the multi-layer relaxed surface is more stable than the former one, which supports the LEED results. The mono-layer relaxed Ag (111) surface is the most stable one among several" stable surface models"presented by several researchers. The surface energy of Ag (111) surface is higher than that of surface Ag (001), which supports some experimental results such as different reaction rate at different surface orientations for the same material. The surafce states of Si (111) surface not only locate near the Fermi level, but also in the valence band, which agrees well with Cohen's conclusion. Si (111)-H is an effective model for analysing the surface states and H adsorbed on the back surface is a good method for improving the convincingness of the results obtained on thinner slab models. The surface stability depends on three different kinds of MoSi〓(001) surfaces, the surface with mono-layer Si is the most stable one, and the surface with Mo at the first layer is the most unstable one among them. These are consistant with the Kemoda's experimental results. The valence bands of clean or K adsorbed CdTe (111) surface agrees well with the synchrotron radiation studies. The surface of CdTe (111) consists of four kinds of surface models which show different surface electronic structures and different surface structure stabilities. The conclusion agrees well with Wu's experimental work. The different absorbed alkali metals on the CdTe (111) surface give different adsorption characteristics which have relations not only with the valence electrons, but also with the core ones of the alkali metals. The electonic structures of Si-C alloys are different from that of Si-Ge alloys, and the energy band gaps of Si-C alloys do not increase linearly with Carbon concentration, our conclusion supports Alexander's results, but conflicts with Soref's one.

现分述如下: LMTO方法及其应用方面:1)通过对Nb(100)表面电子态分析发现清洁理想表面有三个表面态,多层弛豫表面有两个表面态;表面能大小说明多层弛豫表面更稳定,支持了LEED结果。2)通过对采用不同方法获得的几种不同Ag(111)表面稳定结构的表面能计算分析,给出了单层弛豫表面为Ag(111)表面的最稳定结构;从Ag(111)单层弛豫表面和Ag(001)表面的表面能比较,发现了Ag(001)表面表面能要比Ag(111)小的,表明了同种物质不同表面取向将表现出不同物理、化学性质,这是与实验中得出的结论是吻合的,3)通过对Si(111)表面态分析,不仅发现了Si(111)表面不仅具有居于费米能级附近的悬挂键所对应的表面态,而且还有很多表面态位于价带能量范围内,与Cohen等结果一致,H饱和slab模型背表面相当于增加了slab层的厚度,是一有效的变相增加slab层厚的方法,弛豫表面较清洁理想表面价带谱们低能端的少许移动,预示着总能降低,说明弛豫表面较清洁理想表面稳定。4)MoSi〓具有三种表面,从费米能级上态密度值大小得到单层Si表面最稳定,Mo原子为表层原子的表面最不稳定,双层Si原子表面居中的结论,这与Kemoda等人实验结果是一致的。5)通过对CdTe(111)表面表面电子态、表面结构稳定性及表面H、碱金属吸附的电子结构系列研究,不仅得出了CdTe(111)清洁及碱金属K吸附价带谱与同步辐射光电子谱相吻合的结果,而且发现了CdTe(111)表面具有四类不同原子近邻特征,表现出四类不同的表面结构及电子结构特征:不同表面态分布、不同的表面结构稳定性(表层原子与次层原子成三键有一悬挂键的表面要比表层原子与次层原子成一键有三悬挂键稳定(与Wu等人实验结果一致))、不同的H吸附特性。

Combining the experimental results and theoretical analysis, the following work has been accomplished.(1) Reasons of the decrease of interelectrode capacitance and the increase of discharge gap caused by the powder suspended in dielectric fluid are explained. And the mechanism that surface quality of workpiece improved by powder-mixed EDM is analyzed from this viewpoint.(2) The variation regularity of the percentage of silicon on the machined surface of workpiece has been summarized according to the experiment results when silicon powder was added into the working fluid. The entropy is introduced to explain the reasons for this variation regularity by thermodynamics.(3) The dimensional accuracy is greatly influenced by the overcut resulting from discharge gap and electrode wear in practice application. Empirical formulas for the overcut in EDM and powder-mixed EDM are established based on the experimental results using the ternary linear regressive method in this paper.(4) The influence of main factors on the machined surface characteristics has been evaluated based on the orthogonal experimental design method.

通过一系列普通电火花加工与混粉电火花加工的对比实验,运用工艺实验和理论分析相结合的方法,重点做了以下工作:(1)探讨了粉末颗粒导致极间电容减小、放电间隙增大的原因,并从这个角度解释了混粉电火花加工可以改善工件表面质量的机理;(2)以混合硅粉的电火花加工为例,实验得出峰值电流和脉冲宽度对加工表面层成分中硅元素含量的影响规律,并引入熵的概念从热力学的角度对硅元素含量变化的原因寻找了理论依据;(3)在实际加工中,由于粉末的加入使放电间隙变大,这使得混粉电火花加工的尺寸精度难以控制,本文利用三元线性回归的方法,在实验数据的基础上,建立了两种电火花加工过切量的计算公式;(4)将正交试验法应用于混粉电火花加工实验研究,并通过对实验指标极差的直观分析,得出各电参数对加工指标影响的敏感程度。

Firstly, we used the Raman scattering method which can calibrate in real time to measure the O2 (a1 Δ) yield of SOG for the first time in China. The measurement relative error is less than 8%. Based on the data from the experiments, we report the results that the diluent category and ratios influence the O2 (a1 Δ) yield. The relationship of P-τ values and the O2 (a1 Δ) yield of this SOG were given. The effects of distance and bypass of gas transportation on the O2 (a1 Δ) yield are investigated. Secondly, the chlorine utilization was measured by using Raman spectroscopy simultaneously when the O2 (a1 Δ) yield was measured. This method originated with us. The result about the chlorine utilization is coincident with other theoretic and experimental conclusions. The relationship given in this paper between gas stay time in SOG and chlorine utilization offers reference to improve the reaction efficiency and chemical efficiency of COIL. Finally, the partial water vapor pressure at the exit of SOG was measured by absorption spectroscopy. The water vapor fraction and partial pressure have trends changed with the generator total pressure, the diluentratios, and the BHP temperature. These experimental results are very important to improve experimental conditions of SOG, reduce the water vapor fraction, and enhance the output power of COIL.

由侧得的数据得到了加入稀释气体、稀释气体种类以及稀释比例对单重态氧产率的影响,给出了该发生器P一:值与仇产率的关系,还考察了传输距离对仇产率的影响;在国际上首创利用喇曼散射光谱法在侧量产率的同时进行了氯气利用率的检侧,侧试结果与其他理论及实验结果十分相近;给出了气体在发生器中的滞留时间与氯气利用率之间的关系,该结果为提高氧碘化学激光器的反应效率和化学效率提供了参考依据;另外采用了吸收光谱法对发生器出口处的水汽含量进行了测量、得到了水汽分压和百分含量随着发生器压力、稀释气体比例以及BHP温度等的变化情况,该实验结果对于改进发生器工作条件、减少水汽含量、提高氧碘化学激光器的出光功率具有十分重要的指导意义。

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"The operators will suffer a temporary decrease in the number of consumers and short message services as people may not like having to provide their ID cards for a phone number," Xu Junqi, vice-dean with the Policy-Making Institute of the Telecommunications Research Centre under MII, said yesterday.

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我不相信这些虚构的故事。

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