查询词典 crystal diffraction

By means of modern analysis and testing tools such as X-ray diffraction and flurescence spectrum research the crystal constitution and luminescence performance of materials.

结合X射线衍射仪、荧光分光光度计等现代分析测试手段，研究了其晶体结构和发光性能。

The result of X-ray diffraction analysis showed that Ni-Fe-Cr alloy is characterized by face-centered cubic crystal structure.

Ni–Fe–Cr合金的电沉积研究也被广大学者所关注[1-11]，通常是以铜作为研究基体。

High-resolved X-ray diffraction measurements show that the crystal quality of high aluminum mole fraction(x=0.1) is poor and it may cause a large dark current. The window layer acts as a band-choice role. It induces a high responsivity and a wide response band for a higher aluminum mole fraction.

高分辨率X射线衍射仪对材料的测试结果表明，高铝组分(0.1)窗口层薄膜材料的晶体质量较差，导致暗电流增大，而其窗口层的窗口选择作用则可以得到较高的响应率和较宽的响应波段。

In the second chapter, the complex Cd 〓(RB is the abbreviation of rhodamine B) has been synthesized and characterized by means of elemental analysis, molar conductivity, IR,〓 NMR and MS. The crystal structure of the complex has been determined by X-ray diffraction.

第二章 合成了配合物〓，通过元素分析、摩尔电导、红外光谱、核磁共振氢谱和质谱对配合物的组成和性质进行了表征，并测定了其单晶结构。

This dissertation aims at finding anticancer and antibacterial polynuclear complexes targeting DNA with high activity and low toxicity. Sixteen compounds were synthesized, and characterized by means of X-ray single crystal diffraction, elemental analysis, molar conductivity and IR, and the influencing factors on structures of the compounds have been investigated. The actions of these compounds to DNA were also investigated by spectral, electrochemical and hydromechanical methods.

本论文以DNA为靶点，以寻找新结构类型的高效、低毒的抗癌、抗菌多核配合物为目标，从分子设计出发，共合成得到了16个化合物的单晶结构，对其进行了结构表征，探讨了结构影响因素，并研究了其超分子结构；采用紫外-可见吸收光谱法、荧光光谱法、电化学和粘度法，从分子水平上研究了所得配合物与DNA的相互作用；在细胞水平上，研究了草酰胺桥联双核配合物的抗菌和抗肿瘤活性。

In this paper, a turbostratic CN precursor was prepared by means of pyrolysis of melamine, then it was treated by high temperature and high pressure. The pyrolysis process of melamine, mechanism of hydrogen elimination and the effect of catalysts on pyrolysis of melamine were studied. The crystal structures, bonding states and chemical compositions of CN precursor obtained by pyrolyzing melamine are analyzed by X ray diffraction, burning spectrum, scanning elecron microscope and Fourier transform infrared Spectroscopy.

本文采用三聚氰胺热解法制备了乱层石墨结构的碳氮前驱物并进行了探索性的高温高压实验；研究了三聚氰胺热解的工艺、去氢机理以及催化剂对三聚氰胺热解过程的影响规律；借助 X 射线衍射、燃烧谱、透射电镜和红外光谱等手段，对获得的碳氮前驱物进行了成分、晶体结构、价键结构的分析。

The crystal structures of the two polymorphs are so similar that they can hardly be distinguished by usual polycrystalline X-ray diffraction methods.

后者是一种亚稳相。这两种多型体的结构非常相似，用通常的多晶衍射方法难以区分。

The instruments for protein crystal diffraction data collection have been improved very much, for example, the use of synchrotron technique increased data collecting rate and improved the data qualities and resolution.

用于蛋白质晶体衍射数据收集的仪器有了很大进步，同步辐射光源的使用大大加快了数据收集的速度，提高了数据的分辨率，改善了数据质量。

Two coordination polymers [Pb6(H2O)24]·3H2O(1)(H3cit=citric acid)and Pb(H2O)2(2)(tar=tartaric acid)were synthesized under hydrothermal conditions and characterized via IR,TG-DTA,C,H,N elemental analysis,XRD and single crystal X-ray diffraction analysis.

在水热条件下，合成了2个含柔性配体柠檬酸和酒石酸的二价铅配位聚合物[Pb6(H2O)24]。3H2O(1)(H3cit=citricacid)及Pb(H2O)2(2)(tar=tartaricacid)。用红外光谱、差热-热重、元素分析、粉末X射线衍射及单晶X射线衍射等手段对化合物进行了表征。化合物1属三斜晶系，P1空间群，a=0.97053(19)nm，b=0.9764(2)nm，c=1.0955(2)nm，α=109.016(3)°，β=98.380(3)°，γ=92.136(3)°，V=0.9671(3)nm3，Z=2，R1=0.0420，wR2=0.1049，GOF=1.064。

Transmission electron microscope, selected area electron diffraction and tilting experiment along the crystal a-axis are applied and two completely different phase compositions and structure are found in the light and dark regions of the ring-banded spherulites.

采用透射电子显微镜、选区衍射和倾斜实验技术确定了PTT溶液浇铸薄膜在较低温度下形成的环带球晶的相结构和组成。

After explaining total design of automated test system for microcircuit , the thesis introduces GPIB standard .

文章在说明了微电路模块自动测试系统的总体设计后，对GPIB标准进行了介绍。

He interceded in my behalf.

他替我说情。