查询词典 crystal diffraction

The tetravalence vanadium was found in V2O5 gel thin films by measuring the electrical resistance change of V2O5 gel thin films with temperature, ESCA and X-ray diffraction analysis. in this paper, from miniamount redox in melting V2O5 and crystal structure, the influencing mechanism of miniamount redox on changing valence of vanadium was analyzed and discussed in detail.

通过对V2O5凝胶薄膜试样的电阻随温度的变化测试和电子能谱和X射线衍射分析发现V2O5凝胶薄膜中有四价钒的存在，本文从V2O5熔体的微量氧化还原和晶体结构的角度分析讨论了微量氧化还原影响钒离子价态变化的机理。

In this article, three novel cyclopalladated ferrocenylimine triphenylphosphine complexes 2-4 were easily synthesized and characterized by elemental analysis, IR, 1H NMR, 31P NMR and X-ray single crystal diffraction.

为筛选高效催化Suzuki反应的催化剂，合成了3种新的环钯化二茂铁亚胺-三苯基膦配合物2~4，经元素分析、红外光谱和核磁共振谱对其结构进行了表征，并通过X射线单晶衍射测定了化合物3的晶体结构。

In this thesis, on the one hand, two new tripodal ligands and twenty-three of their lanthanide complexes were synthesized, and their fluorescence properties were investigated, on the other hand, nine new copper and silver complexes with six kinds of tripodal ligands were synthesized and their crystal and molecular structures were determined by X-ray diffraction analysis.

本论文一方面合成了两个新三脚架配体的23个稀土配合物，并对它们的发光性能进行了探讨；另一方面得到了涉及六种三脚架配体的9个铜、银配合物，并测定了它们的晶体结构。

Compound 1 and 2 are pure tungstosilicate cluster,the others are transition-metal tungstosilicate clusters All compound characterized by elemental analyses,IR,TG,and single-crystal X-ray diffraction..

其中，前两个化合物为纯硅钨簇，后三个化合物为含有金属的硅钨簇。所有的化合物都通过元素分析，IR，TG和单晶X-射线分析进行了表征。另外，对于化合物3、4和5，我们还对其电化学性质进行了研究。

The microstructure of the magnesium alloy before and after ECAP were examined by means of OM and TEM. The hardness of the as-extruded and unextruded Mg-6Zn-1Gd-0.6Zr magnesium alloy was examined by vickers hardness tester. The rolling of the crystal plane in the process of ECAP was analyzed by X-ray diffraction.

采用光学显微镜和透射电子显微镜分析了试样ECAP变形前后的显微组织变化，采用显维硬度计对Mg-6Zn-1Gd-0.6Zr合金ECAP变形前后进行了硬度测试，采用X-射线分析法分析了ECAP变形过程中晶面的转动。

Through chemical analysis and X radiation diffraction, the composition of the synthetic powder is obtained. In the synthetic powder, there are crystal NaCl and noncrystal Fe〓O〓 and BaCO〓.

通过化学分析和X射线衍射的检测，得出了合成料粉中所含成分及其存在状态，除了助熔剂氯化钠以晶态存在外，其它均是非晶态物质。

Then GaN nanostructured thin films comprised of regular hexagonal crystal grains have been successfully synthesized by ammoniating Ga2O3 films at the temperature of 850℃ for 15 rain in a quartz tube. X -ray diffraction reveals that the synthesized GaN is of a hexagonal wurtzite structure with lattice constants a =0.318 nm and c =0.518 nm.

然后将硅基Ga2O3置于管武石英炉中，在850℃的氨化温度下氨化15min后，成功制备出GaN薄膜，该薄膜由正六边形的晶粒组成。X射线衍射表明GaN具有六方纤锌矿结构，晶格常数为a=0.318nm和c=0.518nm.X射线光电子能谱的测试确定了样品中Ga-N键的形成，并且Ga和N的化学计量比为1：1。

The crystal structures have been determined by X-ray diffraction method, which show that the new complex [Co2-Co(2)(0H2)s] belongs to the bridging binuclear complex and the system of monoclinic with space group P211~,unit cell parameters a8.3850(10)A, b=27.386(4) A, c=9.610(2) A,~=98.280(10)~,V=2 183.8(6) A3 , Z=4, Dc=l.746Mg/m3,~i =l.597mm, F(000)=1168, Final R=O.0253 and wR=O.0610 S1.009 ,The two Co2~ are in distorted octahedrons. The part of [2Co] possess an approximate D2d symmetry, while the part of [OCo(2)(0H2)5] has an approximate C2 symmetry.

结构分析表明配合物(1)[Co1，(DPC2-Co(2)(OH2)5]是一个未见报导的桥联双核配合物，属单斜晶系，空间群为P2_1／c，晶胞参数：a=8.3850(10)A，b=27.386(4)A，c=9.610(2)A，β=98.280(10)A，V=2183.8(6)A~3，Dc=1.746Mg／m3，Z=4，μ=1.597mm-1，F(000)=1168，结构偏离因子R=0.0253和ωR=0.0610，吻合因子S=1.009，Co_(1)和Co_(2)的配位多面体皆为扭曲正八面体，[_2Co_(1)]部分具有近似D_(2d)对称性，[OCo(2)(OH_2)5]部分具有近似C_2对称性。

In this paper several technologies, such as Fourier transform infrared spectroscopy, elemental analyzer, wide angle X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy and high resolution transmission electron microscopy were used to systemically investigate the evolution of crystal structure, chemical structure, microstructure and properties of wet-spinning and dry-jet wet-spinning PAN precursor fibers during proxidation and carbonization process, analysis the structural change of carbon fibers during graphitization, and discuss the correlation between the structure and properties.

本文采用傅里叶变换红外光谱、元素分析仪、X射线衍射仪、场发射扫描电镜、透射电镜以及高分辨透射电镜等测试技术，分别系统研究了湿纺原丝和干喷湿纺原丝在预氧化和碳化过程中纤维晶体结构、化学结构、微观结构和力学性能的演变规律，分析了碳纤维在石墨化过程中的结构转变，并对碳纤维结构与性能的相关性问题作了探讨。

An optical microscope, atomic force microscope, scanning electron microscope, high resolution double crystal X-ray diffraction, and Raman shift spectrum are used to analyze the sample.

采用光学显微镜、原子力显微镜、扫描电子显微镜、高分辨率双晶X射线衍射和喇曼谱测试对薄膜进行分析。

After explaining total design of automated test system for microcircuit , the thesis introduces GPIB standard .

文章在说明了微电路模块自动测试系统的总体设计后，对GPIB标准进行了介绍。

He interceded in my behalf.

他替我说情。