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In order to isolate the active compounds in ethyl acetate fraction of Psoralea corylifolia L., activity-guided isolation was performed along with chromatographic techniques. Four active compounds were isolated from ethyl acetate fraction and identified by their NMR spectral data and physical-chemical properties. They are corylin and bavachin, which showed stimulating effect on osteoblastic proliferation and differentiation, isopsoralen and psoralen exhibited activity of promoting cell differentiation in some degree.

为了追踪分离补骨脂乙酸乙酯萃取物中的活性成分，本实验采用多种色谱分离技术，以活性测试为导向，结合波谱技术及理化数据，从补骨脂乙酸乙酯萃取物中分离并鉴定了4个活性化合物的化学结构，它们是具有促进细胞增殖和分化作用的补骨脂异黄酮和补骨脂二氢黄酮，对细胞分化有一定促进作用的异补骨脂素和补骨脂素。

The condensation of aromatic aldehydes with active methylene compounds like malononitrile, cyanoacetamide and ethyl cyanoacetate has been found to proceed very efficiently at room temperature giving excellent yields, but the condensation of heteroaromatic,α,β-unsaturated and aliphatic aldehydes with active methylene compounds proceeded smoothly in 50~65℃ with good yields and the reactions of aromatic, aliphatic ketones as well as p-phthalaldehyde with malononitrile also proceeded in 75~85℃ with moderate yields.

芳香醛与活泼亚甲基化合物如丙二腈、氰基乙酸乙酯、氰基乙酰胺的缩合在室温下即能顺利进行，获得了很高的收率；而对于杂环芳醛、α，β-不饱和的醛以及脂肪醛与活泼亚甲基化合物的缩合，需在50~65℃下进行，也取得了很高的收率；对于脂肪酮、芳香酮以及二元醛与丙二腈的缩合在75~85℃下也能顺利地进行，获得中等以上的收率。

In volatile oil of processed Cyperus, the contents of alkene and ketone compounds are more than those in unprocessed Cypreus, while the content of acid compounds is less than that of unprocessed Cypreus.

醋炙香附挥发油的主要成分中各种烯类、酮类化合物含量高于生品中的含量，而酸类化合物的含量低于生品中的含量。

Heterotrophic nitrification bacteria are able to utilize organic carbon sources to grow and produce hydroxylamine, nitrite and nitrate from nitrogen compounds, and most of them can also denitrify these products to gaseous nitrogen compounds simultaneously.

异养硝化细菌能够在利用有机碳源生长的同时将含氮化合物硝化生成羟胺、亚硝酸盐、硝酸盐等产物，多数还能同时进行好氧反硝化作用，直接将硝化产物转化为含氮气体。

For pre-selection of iron compounds that ferrous sulfate, ferrous chloride, ferrous fumarate, carbonyl iron, amino acid chelated iron, iron asporotate, fenic chloride and ferric pyrophosphate were added in reconstituted skim milk to undergo in vitro digestion, respectively, and then the selected iron compounds were added in reconstituted whole milk to compare the iron bioavailability by estimating dialyzable ferrous iron, dialyzable total iron, nondialyzable and total ferrous iron, respectively.

取硫酸亚铁、反丁烯二酸亚铁、氯化亚铁、艰基铁、Iron asporotate、Amino acid chelated iron、氯化铁与焦磷酸铁等不同铁剂添加於脱脂还原乳中进行体外消化试验，并筛选生物利用性佳之铁剂分别添加於全脂还原乳中，以可透析二价铁、可透析总铁、未透析二价铁及总二价铁等作为评估之指标。

For pre-selection of iron compounds that ferrous sulfate, ferrous chloride, ferrous fumarate, carbonyl iron, amino acid chelated iron, iron asporotate, fenic chloride and ferric pyrophosphate were added in reconstituted skim milk to undergo in vitro digestion, respectively, and then the selected iron compounds were added in reconstituted whole milk to compare the iron bioavailability by estimating dialyzable ferrous iron, dialyzable total iron, nondialyzable and total ferrous iron, respectively.

取硫酸亚铁、反丁烯二酸亚铁、氯化亚铁、艰基铁、Iron asporotate、Amino acid chelated iron、氯化铁与焦磷酸铁等不同铁剂添加於脱脂还原乳中进行体外消化试验，並筛选生物利用性佳之铁剂分别添加於全脂还原乳中，以可透析二价铁、可透析总铁、未透析二价铁及总二价铁等作为评估之指標。

The interaction of tributyltin, the main components of antifouling paint of ships, and its degradation products of monobutyltin and dibutyltin with human serum albumin was investigated by ultraviolet, fluorescence and circle dichromism spectra. The influences of the concentration, acidity, organic solvent such as ethanol and ionic strength on the interaction of butyltin compounds and HSA molecule were examined to find that the interaction of butyltin compounds and HSA was dual.

通过紫外、荧光和CD光谱，研究了船体防污漆中主要防污成分——三丁基锡化合物及其降解产物——一丁基锡和二丁基锡与人血清白蛋白相互作用的方式与程度，考察了浓度、酸度、有机溶剂和离子强度等因素对相互作用的影响。

Our research focused on the synthesis of heterocyclic compounds through the reaction between the dihalogen compounds and amides or carbamates.

我们小组首次进行了二卤代化合物和酰胺或氨基酸酯之间偶联反应的研究，以期发展构筑氮杂环化合物的新方法。

Three aspects were included here:The derivatives of dihydrol,2,4,5-tetrazine-3,5-dicarboxylic acid were synthesized via three different routes:(1) four new compounds were synthesized via the reaction bet ween dihydrol,2,4,5-tetrazine-3,5-dicarboxylic acid, thionyl chloride and corresponding alcohol ;(2) first ,dimethyl dihydro-1,2,4,5-tetrazine-3,5-dicarboxylate wer e synthesized, then ,another four new compounds were obtained t hrough the alcoholysis under the catalyst ;(3) three acylamines were got through the ammonolysis betw een dimethyl dihydro-1,2,4,5-tetrazine-3,5-dicarboxylate and amines.

本论文分别通过三条不同的路线合成了1，4-二氢-3，6-二甲酸-s-四嗪的衍生物：(1)通过1，4-二氢-3，6-二甲酸-s-四嗪与氯化亚砜和相应的醇反应，制备了四个新化合物；(2)合成1，4-二氢-3，6-二甲酸甲酯-s-四嗪，在催化剂的作用下，与高沸点的醇进行酯交换反应，合成了四个新化合物；(3)合成1，4-二氢-3，6-二甲酸甲酯-s-四嗪后，与胺进行氨解反应，合成三个新的1，4-二氢-3，6-二甲酰胺-s-四嗪化合物。

From the point view of product distribution, conversion of dimethyl ether and energy consumption, with RCD plasma DME conversion was higher and was hardly affected by the residence time of dimethyl ether, and hydrogen, carbon monoxide and unsaturated hydrocarbons with RCD plasma were more than those with DBD plasma.There was no liquid product with RCD plasma, but the liquid product obtained with DBD plasma consisted of aldehydes, alcohols and methoxy-containing organic compounds, for instance, formaldehyde, methyl alcohol, dimethoxy ethane and so on.Moreover, most compositions of liquid product were methoxy-containing compounds, and the liquid product selectivity was as high as 32.23%.However, energy consumption for the reaction with DBD plasma was more than that with RCD plasma.

从产物分布、转化率及能耗上看，利用RCD所获得的二甲醚的转化率高，几乎不受二甲醚停留时间的影响，且氢气、一氧化碳和不饱和烃的含量大，几乎没有液相产物，而利用DBD能获得较多的液相产物，包括一些醇、醛和含有甲氧基的有机化合物，如甲醛、甲醇和二甲氧基乙烷，且大部分组成都是含有甲氧基的化合物，液相产物的选择性高达32.23％，但是能耗较大。

There had been a moment during the breakfast meeting, though, after the backslapping and the small talk and when all of us were seated, with Vice President Cheney eating his eggs Benedict impassively and Karl Rove at the far end of the table discreetly checking his BlackBerry, that I witnessed a different side of the man.

那次早餐会期间，在表示过关心和寒暄以后，我们所有人坐了下来，我注意观察了一下，副总统切尼面无表情地吃着班尼迪克蛋（Eggs benedict，源自美国，以英式松饼、火腿、水煮蛋以及荷兰酱组合而成），卡尔。罗夫在餐桌的远端谨慎地经常查看他的黑莓手机，我目睹了他所不为人知的一面。

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