查询词典 acid process

Ursolic acid, which has immunity enhancement in the Cornus, was chosen as primary index in this research. The method of reversed-phase high performance liquid chromatography with ultraviolet detector was developed to determine the content of ursolic acid. The L9(34) orthogonal experimental design was used for Cornus to further process and explore its health product using the content of ursolic acid and the rate of paste as the assessment indexes.

本研究以山茱萸中具有增强免疫功能的熊果酸为主要考察指标，采用反相高效液相色谱-紫外检测法作为熊果酸含量的测定方法，以出膏率为参考指标，采用L9(34)设计正交试验，对山茱萸药材进行了深加工，开发其保健品；对所得到的提取物中的多糖进行了定性鉴定。

The experimental results of cyclic operation indicate that, sulfuric acid concentration in feed solutions decreases and sulfuric acid concentration in dialyzate increases in the operational process, furthermore, rejection ratio of rare earth is very high, and DD can achieve the purpose of sulfuric acid separation from rare earth sulfate solutions.

循环式结果表明，渗析过程中，料液中硫酸浓度不断减小，而渗析液硫酸浓度不断增大，而且由于对稀土具有较高的截留率，扩散渗析法能达到硫酸与稀土有效分离的目的。

The results indicate that it is possible to identify and distinguish these siccative oils because the unsaturated acid had changed into azelaic due to oxidation and polymerization during the drying process to make the chromatogram of siccative oils have a typical peak of C9 compound and provide a finger marker of m/z 217, and the concentration ratio of palmitic acid to stearic acid remains constant with time to facilitate the differentiation of oils.

分析时采用了热裂解与甲基化同时进行的技术。分析结果显示，4种干性油的不饱和脂肪酸在成膜后的甲基化产物均为壬二酸二甲酯，离子质量与离子电荷量比值为217，是干性油的特征检测峰。4种油中不同含量的软脂酸和硬脂酸在干性油成膜前后的比值不变，为干性油的甄别提供了可能性。

It was found that sulfuric acid, 2-naphthalenesulphonic acid and sulfurous acid could be effectively separated by competitive exchange adsorption in views of action force difference of the components with the resin. The exchange adsorption dynamic diffusion parameters were calculated with diffusion equation for solids and liquid films, and the rate-determining step was determined. The model of breakthrough curve for the resin bed was suggested, and applied to simulate the breakthrough process for each component.

通过单组分、双组分和多组分平衡数据的测定，发现对于硫酸-萘磺酸-亚硫酸混合体系，可以利用不同组分与树脂作用能的不同，通过竞争交换吸附实现分离；以固相扩散方程和液膜扩散方程对交换吸附动力学参数进行了估算，确定了交换吸附过程的控制步骤；建立了床层穿透曲线模型，并对各组分穿透过程进行了模拟。

The results showed that the crude protein content,the eighteen essential amino acids and the twelve essential amino acids in the powder of tetraploidy black locust for fodder leaves were highly at the four stages,and along with the time process,they were all descending gradually.Moreover,their essential amino acid score were also highly and their amino acid were balanceable.And their essential amino acid index of cattle,pig,chicken,duck,goose,fish,prawn and sheep were higher than 0.86,therefore they can be the excellent fodder of these animals.

结果表明，饲料型四倍体刺槐叶粉4个时期的粗蛋白1、8种氨基酸总量和12种必需氨基酸含量均较高，且呈现随时间的推移而逐渐下降的趋势；其必需氨基酸分均较高，氨基酸组成较平衡；对牛、猪、鸡、鸭、鹅、草鱼、对虾和羊8种动物的必需氨基酸指数4个时期之间无差异，均大于0.86，可作为这些动物的优良植物饲料蛋白源；在7月中下旬其生物量和营养达到了最佳结合点，适宜采摘或刈割。

The invention relates to a process for producing polyethylene terephthalate 1, 3-propanediol, which comprises the following steps: using titanic acid ester as major catalyst, using germanium compounds and cobalt compounds as synergic catalyst, conducting esterification reaction for poly terephthalic acid and 1, 3-propanediol according to the molar 1:1.05-2.2 under the nitrogen pressure of 0.1-0.4MPa and 230-265 DEG C, or conducting ester exchanging reaction for poly terephthalic acid and 1, 3-propanediol according to the molar ratio 1:1.8-2.2 in 160-220 DEG C, decompressing reaction to high vacuum 10-150Pa, wherein the final temperature of reaction is 265-275 DEG C, recovering to normal pressure with nitrogen to obtain the PTT product.

本发明涉及一种生产聚对苯二甲酸1，3-丙二醇酯的方法，采用以钛酸酯为主催化剂，锗化合物和钴化合物为协同催化剂，对苯二甲酸二甲酯和1，3-丙二醇按摩尔1∶1.05-2.2，在0.1-0.4MPa氮气压力和230-265℃下进行酯化反应，或对苯二甲酸二甲酯和1，3-丙二醇按摩尔比1∶1.8-2.2，在160-220℃进行酯交换反应，将反应减压至高真空10-150Pa，反应终温在265-275℃，用氮气恢复到常压，得到本PTT产品；大大缩短了反应时间，直接聚合制备特性粘度在0.7-1.05dL/g的PTT切片，使反应产物色相良好，PTT产品可用于纤维加工及工程塑料领域。

The invention relates to a preparation process for synthesizing polyethylene terephthalate 1, 3- terephthalate catalyst, which comprises adding titanic acid ester, germanium compounds and cobalt compound into liquid dispersed phase of organic solution, wherein the total weight concentration is 4-10%, and preparing the catalyst through mechanical stirring or ultrasonic wave mixed ligand for 10-60 minutes in 0-120 DEG C, wherein the adding content of titanic acid ester, germanium compounds and cobalt compound are respectively 200-500ppm, 50-300ppm and 100-400ppm of reaction monomer mass of terephthalic acid or dimethyl terephthalate.

本发明涉及一种合成聚对苯二甲酸1，3-丙二醇酯催化剂的制备方法，将钛酸酯、锗化合物和钴化合物加入到有机溶剂的液体分散相中，总重量浓度为4～10％，在0-120℃通过机械搅拌或超声波混配10-60min制得；钛酸酯、锗化合物和钴化合物加入量分别是对苯二甲酸或对苯二甲酸二甲酯反应单体质量的200-500ppm、50-300ppm、100-400ppm；用此催化剂制备PTT产品，酯化和缩聚反应时间相对于单独使用钛酸四丁酯缩短了30-60min，产品特性粘数0.70-1.05dL/g，色相b值在2-6之间，切片可用于加工新型合成纤维及工程塑料产品。

Synthesis process Molecular Formula:〓 Molecular Weight: 394 Chemicla name: N-(2, 3-dihydro-2, 7-dimethyl-benzofuran-1-acyl)-N'-tert-butylN'-(3, 5-dimethyl benzoyl) hydrazine Structural formula:〓 This article define a synthesis method of JS118 with (2, 3-dihydro-2, 7-dimethylbenzofuranyl)-6-formic acid, tert-butyl hydrazine hydrochloride acid and 3, 5-dimethyl benzoic acid as main intermediate through four steps of reaction involving, acyl chloridation condensation and so on.

本文主要的研究工作内容：(1)以N-特丁基双酰肼为先导结构，利用分子等排原理和类同合成法进行先导设计，有目的、有选择地重点改变R〓、R〓基团，将具有不同取代基的苯环以及呋喃环、苯并呋喃环、吡咯环、吡啶环等杂环、稠杂环与先导结构进行有机的组合。

The preparation process includes the following steps: mixing 10 mM concentration water solution of chloropalladic acid and 12.5-25 mM concentration water solution of ammonium hexadecyl trimethyl bride in the volume ratio of 1 to 20, heating to 65-95 deg.c, adding 100 mM concentration water solution of ascorbic acid in the volume ratio to the water solution of chloropalladic acid of 0.16 to 1 to react for 30 min, centrifugal separation to collect precipitate, water washing, and drying to obtain cuboidal nanometer Pd material.

该钯纳米长方体材料的制备方法的步骤和条件法如下：把体积比为1∶20的10mM氯钯酸水溶液和12.5-25mM十六烷基三甲基溴化铵水溶液混合，加热至65-95℃，然后加入与10mM氯钯酸水溶液的体积比为0.16∶1的100mM抗坏血酸水溶液，反应30分钟，将溶液离心分离，收集到的沉淀用水洗涤，干燥，得到钯纳米长方体。

Optimal process conditions for preparing 2-oxo-1, 4-piperazine diacetic acid(3-KP): 2-oxo-1-piperazine acetic acid was combined with chloroacetic acid at a mole ratio of 1 to 1.1, at temperature 40℃for 8 hours.

通过单因素分析，合成3-KP 的最佳反应条件为：反应温度为40℃，反应时间为8 小时，氯乙酸∶S-KP 的摩尔比为1.1∶1。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。