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In complex 1,Cucan be described as a four-coordinated square planar geometry.Compound 8 is the sodium salt of plumbagin and exists as ionic compound.Compounds 9-16 are the rare earth complexes of plumbagin with La,Y,Dy,Sm,Gd,Nd,Erand Eu.Compound 17 is binuclear Y complex.18 is mononuclear Ycomplex with plumbagin and another ligand from Plumbago Zeylanica.Compounds 19-21 are the ternary complexes with plumbagin and 2,2\'-bpy and phen as assistant ligand.In 19, the geometry of Cucan be described as five-coordinated distorted square pyramid that exists in a dimer through the weak bonding,and 1-D chain structure is formed by intermolecular hydrogen bonds.
化合物1的单晶结构分析表明1具有四配位平面四边形结构，化合物8是白花丹素的Na盐，以离子化合物形式存在；化合物9～16为白花丹素的La，Y，Dy，Sm，Gd，Nd，Er，Eu的稀土金属配合物；化合物17是白花丹素的双核钇结构；化合物18为白花丹素的单核钇结构，该配合物除了含白花丹素外，还有来自白花丹植物中的另一个单体化合物也参与配位；化合物19～21是以2，2\'-联吡啶和邻菲咯啉等含N配体为辅助配体，具有白花丹素—含N配体—金属离子的三元配合物，化合物19是白花丹素和2，2\'-联吡啶与Cu的配合物，具有五配位的四方锥构型，通过Cu…O弱的成键作用形成二聚体，再通过分子间的氢键作用进一步形成一维链状结构，化合物20和化合物21是白花丹素分别与2，2\'-联吡啶和邻菲咯啉的Zn配合物，都具有六配位八面体构型的双核锌配合物，呈一维链状结构，化合物20中链与链之间的大量氢键将一维链扩展成二维层，分子间的π-π堆积作用进一步形成三维结构。
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Three part of research works had been carried out in the dissertation. The first part: a kind of multidentate amine modified silica gel was synthesized through the following steps:(1) introduce the amino groups onto the surface of silica-gel by the treatment of surface silanol groups withγ-aminopropyl trimethoxy silane;(2) michael addition of excess trihydroxymethyl propyl triacrylate to amino groups on the silica gel surface;(3) amidation of the unreacted double bonds of TMPTA on the surface of TMPTA modified silica gel with diethylenetriamine;(4) the multidentate amine modified silica gel was finally obtained by the reaction of amino groups on the surface of DETA modified silica gel with double bond of butyl acrylate.
本论文进行了三部分研究工作，第一部分：通过多步反应对硅胶进行改性合成了一种多齿胺改性硅胶配体，合成过程如下：1通过γ-氨丙基三甲氧基硅烷与硅胶表面的硅羟基反应，使硅胶表面带有氨基；2利用硅胶表面氨基与过量的三羟甲基丙烷三丙烯酸酯发生Michael加成反应；3利用二乙烯三胺与TMPTA改性硅胶表面未反应的双键发生反应使硅胶表面氨基化；4最后用丙烯酸正丁酯与DETA改性硅胶表面氨基充分反应成功合多齿胺改性硅胶配体。
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The paper analyzes the electrical corona phenomena, its effect to high_voltage transmission system and present detecting technology. It puts forward a double spectrums imaging system based on spectrum characteristic of electrical corona. It is all-weather and independent of environment radialization and temperature effect. It responds fast and can work in move .Two light ways image for a scene respectively: one way is UV image ,the other is visible image. Then we use image registration and infusion synthetically to form a complex image .The theory and methods of image infusion is explained.
论文基于电晕放电的光谱特性，针对现有电晕放电检测手段的优缺点，提出了一种全天候、不受环境辐射和温度影响、响应速度快、可进行航拍的双光谱图像检测方法：两个光路分别对同一场景成像，一路是紫外图像，一路是可见光图像，综合利用图像配准与融合技术，形成合成图像，在合成的图像中保留每个传感器所获取的重要信息，图像里既有紫外光源，也有可见光背景图像。
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Base Station type Software versionTypes of carrier frequency board adoptedTypes of combiner adoptedWhether had obtained the network license or notIndoor type or outdoor type Whether the master port is separated from the remote-port The maximum carrier frequency capacity of single cabinet The maximum supportable sector numbers of single cabinetWhether it is dual-carrier frequency board or notMust it be paired configuration if it's dual-carrier frequency board (namely, the type of single carrier frequency station could only configure the dual-carrier frequency on hardware) The maximum achievable configuration of a single station of the single cabinetReceiver sensitivity The maximum expand capacity of a single base station (the maximum number of TRX in configuration / the number of cabinets which is required)(fill in according with the three sectors) Top box transmitted power (given separately a grade one combine and a grade two combine) The maximum output power of amplifier (voice, a single logical carrier frequency) The maximum output power of amplifier (EGPRS, a single logical carrier frequency)Whether it has tower-interfaceWhether it has built-in lightning protectionWhether it support the ultra-long cover / whether it need for software support (give simple description that how hardware and software could achieve this) The supporting condition of EGSM (it should be supported including by the carrier frequency, combiner) Dual-band carrier wave (whether it supports the mixed use of 900 M/1800M in the same cabinet) The commonality of duplicate parts Whether it can built-in transmission unitThe single cabinet size (high × width × deep) Installation method Whether it can place against the wallThe basic frame full-configured weight and the supportable number of carrier frequencyThe expansion frame full-configured weight and the supportable number of carrier frequency
基站型号软件版本号采用载频板型号采用合路器型号是否已取得入网许可室内型or室外型是否是主远端分离单机柜最大载频容量单机柜最大支持的扇区数是否是双载频板如是双载频板，是否必须成对配置(即单载频站型只能硬件配置双载频)单机柜可达到的单站最大配置接收机灵敏度单基站最大扩展能力(最大配置TRX数/需机柜数)(按3扇区填写)机顶发射功率(分别给出一级合路与两级合路)功放最大输出功率功放最大输出功率(EGPRS，单个逻辑载频)有无塔放接口有无内置避雷装置是否支持超远覆盖/是否需要软件支持(简单描述软硬件如何实现)EGSM支持情况(包括载频、合路器均应支持)双频段载波（是否支持900M/1800M在同一机柜内混合使用）备件通用性是否可以内置传输单元单机柜尺寸安装方式可否靠墙放置基本架满配重量及支持载频数扩容架满配重量及支持载频数是否支持基本架与扩容架跨扇区满配功耗满配时重量供电方式机柜进出线方式合路器损耗合路能力：几合一单扇区最大支持几载频合路到一副天线/采用几个合路器单扇区载频达到需要增加一副天线时，是否支持两级合路换以不增加天线如两级合路插损为是否支持基带跳频和合成跳频每单个合路器在从低载频数向高载频数扩容时，是否还需要增加硬件可用性指标MTBFMTTR系统中断服务时间硬件是否支持EGPRS本次报价软件版本号开始支持EGPRS的软件版本号其他特点注： 1 应分别填写出来按照本次报价要求所采用的全部BTS型号和采用的合路器型号 2 列出本报价要求的全部室外型基站与高功放单元
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Has become a national chain stores had the largest number of beef powder stores, the unique taste, unique moment, it is the most significant feature of the Tang Di Huang strong selection of beef, with dozens of valuable medicinal herbs, the five-hour fire Aozhi to juice for the soup, With beef, scallions, coriander and rice from, the unique secret memorable enough to make you one can not resist eating.
现已成为全国连锁店数目最多的牛肉粉品牌店，口味独特，一时无双，它最大特色是汤底选用精壮黄牛肉，辅以几十种名贵药材，经五小时慢火熬制，以汁为汤，配以牛肉、香葱、芫荽及米粉而成，独有的秘方足以令你回味无穷，一吃便无法抗拒。
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Based on the language materials collected, the third chapter analyses the understanding restriction conditions of "VP+NP_1+DE+NP_2" ambiguity structure from the NP_2"s life and the VP"s mobility. The author comes to the following conclusions: the NP_2"s life rank with the "VP+NP_1+DE+NP_2" structural ambiguity in understanding becomes the correlation dependence, the monosyllable verb which expresses the hands" and the foot"s movement, easily combining with the tense auxiliary, enter the "VP+NP_1+DE+NP_2" structure to form the latent ambiguity structure; the double syllable verb which has the causes feature is easy to enter the"VP+NP_1+DE+NP_2" structure to form latent ambiguity structure; the double syllable "noun-verb", with the influence of the behind noun NP_1, both can be understood as the valency combination, and the non-valency combination, thus causes the "VP+NP_1+DE+NP_2structure to appear ambiguity.
在第三章中，我们将在语料分析的基础上分别从NP_2的生命度和VP的动性这两方面探讨这一歧义结构在理解上的制约条件：NP_2的生命度等级与&VP+NP_1+的+NP_2&歧义结构理解为偏正结构的几率成正相关关系：表示手、脚等的单音节动词容易与时态助词结合，进入&VP+NP_1+的+NP_2&结构形成潜在的歧义结构；带有致使特征的双音节动词容易进入&VP+NP_1+的+NP_2&结构形成潜在的歧义结构；双音节的&名动词&由于受其后所跟的名词NP_1的影响，既能理解为配价组合，又能理解为非价组合，从而使得&VP+NP_1+的+NP_2&结构出现歧义。
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make a pair：配成一双, 结成夫妇
make a packet 发大财, 赚大钱. | make a pair 配成一双, 结成夫妇. | make a parade of 夸耀, 炫示.