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In the end, the extractive distillation method was applied to separate and purify the binary azeotrope mixture, methanol-dimethyl carbonate. The isoamyl acetate was used as extractant and the two tower system was introduced to continuous extractive distillation operation. The results show a better separation effect.
最后采用萃取精馏的方法，对甲醇-碳酸二甲酯的二元共沸混合物进行了分离提纯研究，以毒性较低的乙酸异戊酯为萃取剂，采用两塔连续萃取精馏操作，结果表明，分离效果比较理想。
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The purity of Monochloroacetone can be reached to 99% by azeotropic distillation in the ratio of water to the mixture of Monochloroacetone and 1,1-dichloroacetone 1:1.
实验确定共沸剂水的加入量与氯丙酮混合液的比例为1：1时，能达到良好的分离效果，可得到纯度99％以上的一氯丙酮。
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Through the calculation of the relative volatility under different solvents and conditions for some azeotropic systems, optimum solvents have been chosen, and the influences of temperature and ratio of solvent on relative volatility were discussed.
通过对甲醇－乙酸甲酯共沸体系在不同萃取剂和不同萃取条件下相对挥发度的计算，选择出适宜的萃取剂，并讨论了温度和溶剂比对相对挥发度的影响。
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Through computer simulation of azeotropy rectification dehydration tower with benzene as entrainer, the optimal technical parameters were obtained as follows:①the output quantity of top tower was 69 kg／h, return benzene phasor as 58 kg／h and reflux ratio as 3, alcohol concentration in charge the higher the better, however, its maximum value influenced by water content at azeotropy point;②sensitivity analysis results indicated that the sensitivity of output quantity of top tower was the highest, alcohol concentration in charge the second and return benzene phasor and reflux ratio the lowest.
对以苯作为夹带剂的共沸精馏脱水塔进行了计算机模拟，得到了最佳工艺参数：①塔顶采出量为69 kg／h，返回苯相量为58 kg／h，回流比为3，进料乙醇浓度越高越好，但其最大值受共沸点水含量的影响。②敏感性分析的结果为塔顶采出量的灵敏度最大，进料乙醇浓度次之，而返回苯相量和回流比较小。
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Fit , the fractions in different temperature ranges were ingathered by rectifying wash oil azeotropic distillation were done with the different fractions and ethanediol respectively .
首先精馏洗油，切取不同温度段的馏分，然后分别与共沸剂乙二醇进行共沸精馏试验；在共沸精馏中，通过改变馏分与共沸剂的质量比和回流比，考察了不同条件对喹啉纯度的影响。
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Then,the core molecule was used as a coupling agent to condensate with polyethylene glycolsof different molecular weight or polyethylene glycol monomethyl etherin the presence of stannous octoate as catalyst and diphenyl ether as azeotropic agent to remove water.
在辛酸亚锡催化下，以二苯醚为共沸脱水剂，将三官能度小分子TMP-SK3作为偶联剂，进一步与不同分子量的端羟基聚乙二醇和聚乙二醇单甲醚缩合，减压下共沸脱水，制备了以TMP-SK3为核，PEG或PEGm为臂的三臂星形大分子。
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The contents of the method are as follows: addition of entainer such as benzene, hexahydrobenzene and pentene etc, rectification make entainer, alcohol and water form ternary boiling material, then boiling point difference formed and high purity alcohol finally produced.
采用向酒精溶液添加夹带剂进行精馏，使夹带剂、乙醇、水形成三元共沸物，造成沸点差，从而精馏出纯度高的酒精。
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The results showed that entrainer reflux ratio: 1:5 of the top tower, the concentration of separated isopropanol is 99.5%; The maximum yield of isopropanol is 78%; simulation calculation result inosculates with the experimental result. The simulation calculation can reflect actual course.
结果表明，当共沸剂塔顶回流的回流比为1：5时，分离得到的异丙醇浓度可以达到99.5%；异丙醇的收率最高，最大收率可达78%；模拟计算结果与实验结果吻合得较好，模拟计算可以反映实际过程。
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On the basis of summarizing separation method of acetic acid-water system, we studied the azeotropic distillation process of acetic acid-water system, selecting butyl acetate, isobutyl acetate and isopropyl acetate as entrainers. The influence of packing height, ratio of water to entrainer and acetic acid initial concentration to separation effect of azeotropic distillation was studied in detail. Simulation calculations of general distillation and azeotropic distillation were carried out. The influence of reflux ratio, theoretical plate, feed position, feed temperature and feed concentration to distillation process were discussed. Preferred process operation parameter, which had guiding meaning to practical production of distillation process were obtained. Basic data for the process amplifying design of azeotropic distillation tower were provided. Invest and operation energy consumption of two distillation methods were compared. The elementary technical design of azeotropic distillation tower was carried out on the basis of result of simulation calculation. The type of major auxiliary equipments and inner parts of packed tower were selected.The research results are as follows:(1) Butyl acetate, isobutyl acetate and isopropyl acetate could be selected as entrainer, and separation effect was near.
本文在综述醋酸-水体系分离方法的基础上，以醋酸丁酯、醋酸异丁酯、醋酸异丙酯为挟带剂，对醋酸水溶液进行共沸精馏过程研究，详细研究了填料高度、水与挟带剂的配比、醋酸初始浓度等对共沸精馏分离效果的影响；对醋酸-水体系进行普通精馏和共沸精馏过程模拟计算，讨论了回流比、理论板、进料位置、进料温度和浓度对精馏过程的影响，获得了对醋酸-水体系精馏过程实际生产具有指导意义的较佳的工艺操作参数、共沸精馏塔的工艺设计放大的基础数据，并对两种精馏方法的投资、操作能耗进行了比较；同时在共沸精馏模拟计算的基础上进行了共沸精馏塔的初步工艺设计计算，并对填料塔的主要辅助设备及塔内件进行了初步选型。
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DM is mainly used as high-boiling point solvent for printing ink, dyestuff, resin, cellulose and painting.
二乙二醇丁醚醋酸酯有着十分高的沸点，主要用于高温烤瓷以及印刷油墨的高沸点溶剂，也用作乳胶漆的助聚结剂；由于该溶剂挥发速度很慢，在水中溶解度低，所以可作为丝网印刷油墨的溶剂，以及聚苯乙烯涂料印花釉的溶剂；也可作为共沸剂用于醇与酮的分离。
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entrainer：共沸剂
共沸混合物azeotrope | 共沸剂entrainer | 共沸作用azeotropism