硫胺

Starting with two reactive methylene compounds, ethyl cyanoacetate and malononitrile, two 5-amino-1H-pyrazoles were prepared through the intermediates ketene dithioacetal.

从两个活泼亚甲基化合物开始，经过乙烯酮二硫代缩醛中间体，合成了两个5-氨基-1H-吡唑，以这个两个化合物为中间体，与芳香族和脂肪族α-溴代酮反应，而后经酸催化亚胺化互变异构后得到含咪唑并[1，2-b]吡唑甲硫醚类化合物6a-6g。

To synthesize the octreotide, Phe-Leu-Glu-Glu-Leu and C_(15)H_(31)-CO-Lys-Thr -Thr-Lys-Ser peptides, the strategies are as followings: Fmoc- group as protective group for α-NH_2; TBTU, DIEA and HOBt as coupling reagent; and ethanedithiol -phenol - thioanisole - H_2O - TFA ( 2.5:5:5:5:82.5 , V/V ) as cleaving solution.

采用Fmoc固相合成法，以苯并三哗四甲基脲四氟硼酸盐、二异丙基乙胺和1-羟基苯骈三氮唑为缩合剂；苯酚—乙二硫醇—苯甲硫醚—水—三氟乙酸(5：5：2.5：5：82.5，V/V)为切割试剂，合成了奥曲肽、Phe-Leu-Glu-Glu-Leu及C_(15)H_(31)-CO-Lys-Thr-Thr-Lys-Ser三种小分子多肽，并对奥曲肽的合成规模进行了放大。

S: The interface formation and magnetism of Fe, Co overlayer on sulfur passivated GaAs(100) by using CH 3CSNH 2 have been studied with synchrotron radiation photoemission and ferromagnetic resonance.

利用同步辐射和铁磁共振研究了经硫代乙酰胺硫钝化处理的GaAs(1 0 0 )表面生长的Fe、Co超薄膜与衬底的界面形成及磁性。

The X-ray diffraction shows that the resin is crystalline. The heat analysis shows that the resin is well heat-resistant and has very good thermal stability and T=101℃. The T is better 10℃ than polyphenylene sulfide. The PASI resin will be applied abraod.

表征结果表明，聚合物为设计聚芳硫醚酰亚胺结构；X射线衍射表明聚合物为结晶性聚合物；热性能测试表明，聚合物的玻璃化温度为101.91℃，高于聚苯硫醚(87.00℃)，聚合物具有良好的热性能。

The adsorption behaviour of chemically different superplasticizers, such as melamine formaldehyde sulphite polycondensate,β-naphthalene sulfonate formaldehyde polycondensate and polycarboxylate, on early hydrating cement phases was studied. For this purpose, pure ettringite AF(subscript t, monosulfate AF(subscript m and syngenite were prepared. The adsorbed amount and zeta potential of early hydration products were measured.

制备了钙矾石AF(下标 t、单硫型硫铝酸钙AF(下标 m和钾长石类单矿物，并研究了三聚氰胺磺酸盐甲醛缩聚物、β-萘磺酸盐甲醛缩合物及聚发酸盐等几种化学成分不同的超塑化剂在其早期水化颗粒表面上的吸附行为。

Therefore, in the laboratory, a 2L gasliquid equilibrium measurement device was used to measure the equilibrium solubility of H2S, CO2, CH3SH and COS in the mixed solutions of Methyldiethanolamine, Tetramethylene sulfone respectively under different temperatures and different proportions. With the relevant parameters being correlated from the measured data, a corresponding thermodynamic calculation model was set up, based on the gasliquid two phase state equilibrium equation, and in combination with the overseas research results.

为此，在实验室利用容积为2 L的气液平衡测定装置，测定了不同温度和溶液配比条件下硫化氢、二氧化碳、甲硫醇、硫氧碳在甲基二乙醇胺（Methyldiethanolamine，MDEA）、环丁砜（Tetramethylene sulfone，TMS）水溶液中的平衡溶解度，并根据气液两相平衡状态方程，结合国外研究成果，利用测定的平衡溶解度数据关联出相关参数，建立了相应的热力学计算模型，用于预测该复杂体系中酸气分压与溶液负荷的气液平衡关系。

Ten novel derivatives of 1-phenyl-5-[5-(substituted anilinocarbonylmethylthio)-4-phenyl-1,2,4- triazol-3-ylmethylthio]-tetrazole were synthesized rapidly in high yields by the reaction of N--2-chloryacetanilide (3) with 1-phenyl-5-(5-mercapto-4-phenyl-1,2,4-triazol-3-ylmethylthio)-tetrazo- le (2) under microwave irradiation and phase transfer catalysis conditions.

采用微波和相转移催化法通过1-苯基-5-(4-苯基-1，2，4-三唑-5-巯基-3-甲硫基)四唑(2)与2-氯乙酰芳胺(3)反应高效、快速地合成了10种尚未见文献报道的1-苯基-5-[5--4-苯基-1，2，4-三唑-3-甲硫基]四唑。其结构经IR，1HNMR，13CNMR和元素分析表征。生物活性实验结果表明，该类化合物在较低浓度下部分化合物对小麦芽有很好的促进作用

Barium carbonate,trontium carbonate,potassium carbonate,barium sulphate precipitated,barium nitrate,barium chloride,industrial sodium sulfide,sulphur,sodium thiosulphate, thiourea,melamine,ammonium bicarbonate (food grade,lasting effect,big granular grade).

提供产品：&五洲&牌，碳酸钡碳酸锶，碳酸钾，硫酸钡，硝酸钡，氯化钡，工业硫化钠，硫磺，硫代硫酸钠，硫脲，三聚氰胺，&青山&牌：碳酸氢铵（食品级，长效型，大颗粒）。

Barium carbonate,trontium carbonate,potassium carbonate,barium sulphate precipitated,barium nitrate,barium chloride,industrial sodium sulfide,sulphur,sodium thiosulphate, thiourea,melamine,ammonium bicarbonate (food grade,lasting effect,big granular grade).

&五洲&牌，碳酸钡碳酸锶，碳酸钾，硫酸钡，硝酸钡，氯化钡，工业硫化钠，硫磺，硫代硫酸钠，硫脲，三聚氰胺，&青山&牌：碳酸氢铵(食品级，长效型，大颗粒)。

Alteration and modification on two-dimensional electrophoresis in Arabidopsis thaliana , such as improvements in protein extraction, lyses buffer, adding thiourea, provide a better separation result. This paper has an optimism of the experimental conditions on two-dimensional electrophoresis.

通过对拟南芥双向电泳技术过程中的适当改进，如蛋白质的提取与溶解方法、上样量和聚丙烯酰胺凝胶浓度，加入硫脲，硫代硫酸钠等，对拟南芥双向电泳技术进行了优化，提高了双向电泳图谱的蛋白质点数目与分辨率。

Certain types of sockets are ''connectionless'', most commonly

某些类型的套接字是无连接的，大多数是UDP协议。

Take it in to his nibs yourself .

你自己拿进去给头儿吧。