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Aiming at above problem, this paper put forward the strategy of separation as follows. Firstly, in view of great amount of coloring matter in solution, the quality of product is declined. So we decolor the solution by acticarbon, which makes 80% coloring matter be removed, but the loss of nucleotides is only about 2%. Secondly, on the basis of physical and chemical properties of four nucleotides, we first synthesized a kind of cation exchange resin by ourselves which is used to separate four matters preliminarily.

针对以上问题,本文提出了如下的分离策略:首先,由于酶解液中色素含量较多,使经树脂分离所得UMP和GMP中色素残留较多,最终导致成品质量的下降,所以我们用活性炭对酶解液进行脱色处理,使溶液中80%以上的色素被吸附除去,而核苷酸的吸附损失仅为2%左右。

The following points are emphasized:The operation models of adiabatic and diabatic distillation have been set up and the operation block, thermodynamics model and mathematical model in the simulation have been determined as well;(2)Based on the simulation and exergy analysis with Aspen Plus program, shortcut distillation design—DSTWU model and rigorous distillation design—RADFRAC model, the author has determined the heat duty, exergy losses and the distribution of exergy losses along the adiabatic column, which will help the simulation and optimization of the diabatic distillation;(3)Diabatic distillation under various operation conditions has been simulated by using energy balance method and exergy analysis;(4)How the different mixture and the various degree of separation, number of trays and feed location influence exergy saving in diabatic distillation have also been discussed;(5)On the basis of the total exergy losses along the column, different schema of the heat transfer distribution along the column have been compared and analyzed;they can be classified in three categories: heat duty equipartition approach, empirical approach, separation degree matching approach. In conclusion, different heat transfer distribution along the column will have effect on total exergy losses. In particular, most satisfactory results have been obtained by using separation degree matching approach. In order to diminish the exergy losses, heat transfer distribution should meet the needs of the request of separation degree.And on this premise, the author makes his suggestion in increasing the proportion of heat supplied to the tray with minimum exergy losses and decreasing the proportion of heat supplied to the tray with the maximum exergy losses.

本文对透热精馏过程进行了模拟并对其节能效果的影响因素做了较为全面的分析和深入的研究,主要研究内容如下:(1)建立了常规精馏和透热精馏过程的模拟操作模块、热力学模型以及数学模型;(2)利用化工模拟软件Aspen Plus并分别采用DSTWU简捷模型和RADFRAC严格计算模型对常规精馏进行模拟计算和有效能分析,确定常规精馏塔的公用工程热负荷、有效能损失及有效能损失在塔内的分布,为透热精馏的模拟和优化提供数据参考;(3)对不同物系在不同分离度条件下进行透热精馏的模拟,分别采用能量衡算法和有效能分析法进行计算和分析;(4)探讨了各种因素如物系的选择、不同分离度、塔板数、进料位置对透热精馏节能效果的影响;(5)以全塔总有效能损失为比较基准,对热量在塔内的三种分布方案即热负荷平均分配法、经验法和分离度匹配法进行了对比分析并得出结论:塔内热量的不同分布方案对于全塔总有效能损失会产生影响,其中以分离度匹配法的节能效果最为理想,为减少有效能的损失,应使塔内的热量分布满足各塔板的分离度要求,并在此前提下,尽量减小有效能损失大的塔板的热负荷和增加有效能损失小的塔板的热负荷。

Mol·L~(-1) individually and also with both heavy metals present. Plasmolysis, concentrated cytoplasm, disappear ance of the cristae of mitochondria, ambiguity of framework and destruction of mitochondria envelope were all symptoms of root cells under Cu stress; hollowing cells was also found in Cd treatment, and there existed some different granule in these hollowing cells.

铜使根细胞产生质壁分离、细胞质浓缩、部分细胞空泡化,使线粒体脊突消失、结构模糊、外膜破坏;镉使根细胞空泡化,并在部分空泡化的细胞里产生大小不等的颗粒状物;铜、镉交互污染使根细胞受害程度加深,并兼有两者的受害症状特征:线粒体结构彻底破坏、空泡化细胞里的颗粒物更大电子密度更高、质壁分离现象更普遍、质膜上的颗粒物沉淀更大。

So young thallus of P.yezoensis should be selected in realwork to form cellular seedings directly from isolated cells.

因而在实际工作中应选择幼嫩的条斑紫菜叶状体,使分离的细胞直接长成细胞苗。

The methodrapidly separates a large amount of different kinds of urushioldiacetates.Because the silver ion is very sensitive to theconfiguration and the degree of unsaturation of the unsaturated bonds,urushiol diacetate were well separated.

本文采用涂渍〓的离心旋转薄层层析法,发挥分离速度快,分离量大,固定相利用率高,分离效果好及〓对双键位置及构型作用灵敏等优点,因而使乙酰化漆酚达到了满意的分离。

Similarly, if the strong shear, which could suppress all the scattering in the quiescent two phase region, stopped, the follow-up phase separation also displayed characteristics of anisotropism and relaxation, In this dissertation, the transposed"butterfly'and"streakpattern were observed for the first time within the shear-history-influenced phase separation, which is found closely relevant to the anisotropical relaxation behavior of macromolecules. 5. The phase separation kinetics of PS/PVME under oscillatory shear was further studied on the base of that done under simple shear. It is found that, under specific temperature and strain amplitude, the occurrence of phase separation is strongly contingent on oscillatory frequency and only intermediate frequency could effectively induce phase separation; If all considered oscillatory shear could stimulate phase separation, a fixed frequency can maintain specific most probable phase size and higher frequency yields smaller phase, which makes a higher elasticity but weaker stress relaxation; Furthermore, higher frequency can produces stronger compulsory oscillation on the MPPS but won't change the mean of the MPPS. Under given frequency and strain amplitude, the phase separation kinetics dramatically depends on the phase angle of oscillation and the phase separation corresponding to different phase angle follows different dynamical process.

在简单剪切场下相分离动力学研究的基础上进一步对振动剪切场下PS/PVME的相分离动力力学进行了尝试性的研究,发现:在一定温度和振幅条件下,相分离的发生强烈的依赖于振动频率,只有中等频率的振动剪切才能有效地促进相分离的发生;在都能使相分离发生的前提下,一定频率的剪切能够使体系维持一定的最可几相尺寸,较高频率的剪切导致体系形成的相区尺寸较小,因而体系的弹性效应较强而应力松弛效应较弱;同时,更高频率的剪切对最可几相尺寸的强迫振动效应越强,但不会使最可几相尺寸的平均值发生改变;在一定的振幅和频率条件下,相分离的动力学过程会强烈地依赖于相位角,不同相位角对应的相分离遵循不同的动力学过程但机理一样。

Organic and compound cation garrulous coagulates the agent is to use chemical law compound a kind of new-style cation garrulous coagulates agent, belong to domestic and international initiate, with other and groovy drug photograph comparing has 5 big advantages: The photograph such as aluminium of as aggregate as commonly used drug chloridize, aggregate and vitriolic iron, vitriolic aluminium is compared, coagulate with garrulous of polypropylene acyl amine the agent is used jointly, medical dose is little, reduce useless water treatment to expend about 20 % thereby, 30 %; Effect of processing liquid waste is good, garrulous is round settling speed is fast, make liquid waste can second birth is used, managing water natural resources; Its garrulous group is sedimentary filterability can be good, slime can reclaim inside entire plant, namely energy-saving be helpful for protecting an environment again; Corrode to equipment small; Have muti_function, have agglomeration effect already, again garrulous coagulates action and the action that aid filter, can serve as filter aid.内容来自www.ch-water.com

有机复合阳离子絮凝(使液体中悬浮微粒集聚变大或形成絮团,从而加快粒子聚沉,达到固-液分离的过程)剂是利用化学法合成的一种新型阳离子絮凝(使液体中悬浮微粒集聚变大或形成絮团,从而加快粒子聚沉,达到固-液分离的过程)剂,属国内外首创,与其他常规药剂相比具有五大优点:与常用药剂聚合氯化铝、聚合硫酸铁、硫酸铝等相比,与聚丙烯酰胺类絮凝(使液体中悬浮微粒集聚变大或形成絮团,从而加快粒子聚沉,达到固-液分离的过程)剂联合使用,药剂量少,从而降低废水处理(通过物化方法去除水中一些物质的过程)费约20%—30%;处理废水效果好,絮团沉降速度快,使废水能再生利用,节约水资源;其絮团沉渣过滤性能好,煤泥可全部厂内回收,即节能又有利于保护环境;对设备腐蚀小;具有多功能,既有凝聚作用,又有絮凝(使液体中悬浮微粒集聚变大或形成絮团,从而加快粒子聚沉,达到固-液分离的过程)作用和助滤作用,可作为助滤剂。

The results showed: when TLC solvent system was: chloroform - methanol - diethyl amine = 90:9:1, alkaloids from lotus leaves were well isolated, and five components were isolated and identified by spraying Dragendorff reagent. The optimal conditions of HPLC solvent system were: methanol- water - diethyl amine = 75:25:0.0125. Under the conditions, components of alkaloids from lotus leaves were separated very well, and ideal RP-HPLC peaks were obtained.5、Methods of High Speed Counter Current Chromatography and preparative High Performance Liquid Chromatography applied to identify and purify alkaloids from lotus leaves were set up. When solvent system of HSCCC was: chloroform - methanol - water (pH=4.00)= 4:3:2, speed of chromatogram was 700rpm, flow speed of the mobile phase was 2mL/min, four pure components relatively were attained by isolation and purification.

结果表明:薄层层析溶剂系统为氯仿:甲醇:二乙胺=90:9:1,使荷叶中的生物碱达到了较好的分离效果,并用改良的碘化铋钾试剂喷雾显色,共分离鉴别出了5种荷叶生物碱;分析型HPLC分析检测的较优溶剂系统为甲醇:水:二乙胺=75:25:0.0125,使荷叶生物碱的各个组分达到了基线分离,并获得了较好的峰形。5、建立了高速逆流色谱和制备型HPLC技术分离纯化荷叶生物碱的具体方法。H(来源:ABC46论文网www.abclunwen.com)SCCC法在溶剂系统为氯仿:甲醇:pH4.00的水=4:3:2,色谱仪转速为700rpm,流动相流速为2mL/min的条件下,分离纯化得到了4个纯度较高的化合物。

Based on the idea of QR decomposition, a geometric blind separation algorithm is proposed for uniform distribution source signals in this paper. It is known that if source signals follow uniform distribution, the scatter plots of source signals and mixtures will show special geometrical property. Firstly, the mixture signals are whiten so that the scatter plot of which is changed into the scatter plot when they are independent, and then the scatter plot of whiten signals is rotated by C ~2 n times Givens transformation.

该文提出了一种多个均匀分布的源信号混叠的盲分离几何算法,该算法以矩阵的QR分解原理为分离的理论指导,并结合信号在各个阶段其scatter图所具有的特殊几何性质,首先将混叠信号进行白化,使其scatter图恢复为独立时的scatter图形状,然后将白化后的scatter图通过C2n次旋转变换,使其与各坐标轴平行,从而得到n个信号的分离。

The availability of plastic bags with attached satellite bags that can be centrifuged in the lab makes it possible to separate out a variety of different components.

可在实验室离心的多联袋的使用使分离多种不同血成分成为可能。

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Do not gum up the work by telling mother what we are going to do .

别告诉母亲我们要干的事,那会把事情搞糟的。

In recent years, application of the partial prestressed concrete beam s is developed.

近年来,随着部分预应力砼梁应用的推广,发现我国规范所采用的名义拉应力法的计算结果不稳定。

Gorky once said:"If it is not a book, I'd be stupid and indecent drowning."

高尔基曾说:"如果不是书籍的话,我就要被愚蠢和下流淹死。"