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An aminobenzene sulfonate-formaldehyde based polymer dispersant with good grinding efficiency was synthesized under alkaline condition using aminobenzene sulfonate, phenol and formaldehyde as main raw materials.

0引言众所周知，在陶瓷工业生产中，原料细磨是其中一道关键的工序，是一个高能耗、低效率的作业过程，却又是必不可少的一个工艺过程。

An aminobenzene sulfonate-formaldehyde based polymer dispersant with good grinding efficiency was synthesized under alkaline condition using aminobenzene sulfonate, phenol and formaldehyde as main raw materials.

以对氨基苯磺酸、苯酚、甲醛为主要原料，采用碱性合成线路制备了具有助磨效果的氨基磺酸系高效减水剂，系统地研究了单体比例、单体浓度、交联剂用量、反应体系初始pH值、反应时间和反应温度等因素对助剂助磨效果的影响。

On the basis of the comprehensive study and analysis of the literatures concerning the mechanism and properties of CCWC, the substances that can react with anhydrate or hydration products and other supplementary ingredients were selected, and variety of experiments were conducted by means of cross experimental design. The effects of chemical composition and dosage of raw materials, curing condition, and chemical admixtures on waterproofing ability were tested and analyzed.

本文在对水泥基渗透结晶型防水材料的作用机理和应用性能分析研究基础上，选择能与水泥混凝土中未水化水泥及部分水化产物反应的活性物质和其它的辅助成分，利用正交设计方法，研究不同组分对涂料防水性能的影响，并详细分析了原料化学成分、掺量及养护条件等参数的变化对涂料渗透结晶性能的影响，研制成功了一种以硅酸盐水泥为基础的水泥基渗透结晶型防水涂料—GT防水涂料。

As raw materials,and under the condition of 1 250 ℃,the high iron belite aluminate cement is made,whose mineral ingredients are 51 %～55 % of C_2S,20 %～30 % of C_4A_3,and 12 %～25 % of C_4AF;and whose strength in 1 d cement can reach(35 MPa),and that of 28 d cement can reach(66 MPa).

用高碳粉煤灰及石灰石、石膏等为原料，在1 250℃条件下烧成了高铁贝利特硫铝酸盐水泥，其主要矿物组成C2S为51%~55%，C4A3-S为20%~30%，C4AF为12%~25%；水泥1 d强度达35 MPa，28 d强度达66 MPa。

On the condition of using fatty acids of rapeseed oil as raw material,85% acetic acid as solvent, pelargonic acid as recrystalization solvent, this paper prepared azelaic acid and brassylic acid by ozonolysis ,oxidation decomposition ,recrystallization etc.

以蓖麻油酸为原料、85%醋酸水溶液为溶剂，经臭氧化、氧化分解、沸水萃取等过程制备壬二酸的最佳反应条件为：m：m(85%醋酸)=1：4，臭氧化温度20-25℃；氧化分解温度90-95℃，催化剂醋酸锰/醋酸铜用量为原料蓖麻油酸质量的0.09%，氧化分解4h，壬二酸的收率为62.5%。

Mesoporous molecular sieves were synthesized by using natural clay, sodium silicate and aluminum chloride as raw materials and cetyl trimethyl ammonium bromide as template agent at room temperature alkaline condition.

室温条件下以天然黏土、硅酸钠和氯化铝为原料，十六烷基三甲基溴化铵为模板剂合成介孔分子筛。

In recent years, the new technology has been used in the synthesis of chalcone compounds, under the 343 K condition carrying on the response in the temperature. It takes benzaldehyde and acetophenone as raw material, BF4 as resolver and the hydrotalcite as the catalyst, the yield of chalcone can reach 98.5%. This method has some advantages including shorter reaction time, higher yield and simpler operation.

近年来查尔酮化合物的合成采用了新技术，是以苯甲醛和苯乙酮为原料，BF4作为反应溶剂，水滑石为催化剂，在温度为343 K的条件下进行反应，查尔酮产率可以达到98.5%，该法具有反应时间短、操作简便、收率高等优点。

Aiming at demand of national economy and linking the actual condition of domestic refinery chemical , a routine with cyclohexene as main raw material was developed in the thesis.

本文针对国民经济发展的需求，结合我国精细化工行业的实际，进行了以环己烯为主要原料，合成1，2-环己二醇的研究。

The growth inhibiting rate of T24 cell lines were detected by MTT methods, apoptosis of cells were detected by flow cytometry, the mechanism of apoptosis was analyzed by detecting the protein expression of Bcl-2, Bax, Caspase-9, Caspase-3 and cytoplastic protein Cytochrome C. 4 We injected live T24 cells into the subcutaneous space of nude mice and successfully built up the animal model of bladder carcinoma. The effect of CS-PAA-EPI polymer magnetic microspheres targeting chemotherapy was investigated by HE staining, TUNEL ,tumor weight and volume inhibition rate. Results: 1 TEM revealed that the CS-PAA polymer magnetic microspheres were regular spherical shape,the average diameter was 80nm in dry condition. By controlling the pH value of the medium,polymers had positive or negative zeta potential. VSM showed the CS-PAA polymer magnetic microspheres had superparamagnetic. The diameter of CS-PAA-EPI polymer magnetic microspheres were 200nm in solution by DLS examining,the embedding ratio was 20%,the EPI loading rate was 15%, which was higer than reported in other articles. 2 Raw eye observation found that the rat"s bladder of treatment group was brown color,which meaned the aggregation of iron particles, compared with the control group, iron stain found iron particles were assembled in rat"s bladder of the treatment group, the amount of iron particles in liver and spleen were less obviously.

研究结果：1合成的CS-PAA磁性聚合物微球呈球形，大小均一，TEM测定其干态下粒径为80nm左右，磁化曲线证实具有超顺磁性，具有一定的PH敏感性，固载表柔比星后，水溶液性状稳定，无沉淀物，DLS测定直径约200nm左右，测定载药率为15％，较文献报道高，包封率为20％。2肉眼观察试验组大鼠膀胱表面呈褐色，可见大量的Fe粒子聚集，普鲁士兰染色法显示，试验组大鼠膀胱壁内有大量的Fe粒子，分布至膀胱壁全层，与对照组大鼠相比，试验组大鼠的肝、脾内的Fe粒子聚集量明显降低；HPLC测定结果与Fe染色相同；高剂量磁性CS-PAA-EPI生理盐水组及单纯EPI生理盐水组均在给药后14天出现血肌酐和尿素氮的升高，其他组大鼠血生化指标没有明显变化。3MTT法发现，高、中、低剂量磁性CS-PAA-EPI生理盐水组在外加磁场的协同作用下杀伤T24细胞效应明显高于单纯的EPI生理盐水组，FCM发现试验药物组可引起明显的肿瘤细胞凋亡，试验药物治疗组细胞胞浆内出现了由线粒体释放出的细胞色素C，试验组细胞Bcl-2蛋白减少，Bax蛋白变化不明显，Caspase-3、Caspase-9蛋白受到了激活活化。4高、中、低剂量磁性CS-PAA-EPI生理盐水组的瘤重抑制率和瘤体积抑制率均明显高于单纯的EPI生理盐水组(P＜0.01)，其中高剂量组的抑制率最高。

Two estolide are that the ester melts an agent take amylum as raw material , with smooth butylene , the ester carrying out the solid room's spends reaction under the situation of there being no menstruum,ester composing smooth amylum butylene diacid Shan, and by having optimized reaction condition , having improved reaction efficiency.

以淀粉为原料，以顺丁烯二酸酐为酯化剂，在无溶剂的情况下，进行固体间的酯化反应，合成淀粉顺丁烯二酸单酯，并通过优化反应条件，提高了反应效率。

Objective To investigate the effects of interleukin-1 β converting enzyme gene on the biologic characteristics of ovarian cancer cells.

目的 探讨白细胞介素-1 β转换酶的表达，对卵巢癌细胞生物学特性的影响。

Campylobacter: This illness is the most commonly identified cause of diarrheal illness in the world.

弯曲：这种病是最常见的原因查明腹泻病，在世界上。