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The surface state and electrochemistry properly platinum-plated on open-cell foamed titanium electrode was investigated and he compared with IrTi anode and platinum-plated titanium toil cathode. The results show that open-cell foamed titanium can uniformly coat with excellent bonding strength platinum-plated, thickness coating 2 μm. The cathode release hydrogen voltage of platinum-plated on open-cell loamed titanium electrode is fall. The anode release oxygen voltage of platinum-plated on open-cell foamed titanium electrode is higher than Irli anode in high current.

采用电镀技术在多孔钛表面沉积了均匀的铂金属层，分析了多孔钛镀铂后的表面状态及电化学性能，并与IrTi涂层阳极及镀铂钛网阴极进行比较，结果显示：多孔钛板开孔孔隙表面可均匀沉积结合力良好的铂层，镀层厚度为2μm；镀铂多孔钛阴极析氢电位比镀铂钛网高，且在大电流下，阳极析氧电位比IrTi涂层阳极高。

There are three platinum catalyst micro channels which have different width ,such as 1000 m , 400m and 40m. The platinum catalyst micro channel reactor is fabricated by MEMS technology. The reactor uses the exothermic reaction of hydrogen and oxygen on the platinum catalyst plate as the heat source and the platinum thin film resistance deposited on a glass chip by face micro machining process as catalyst and temperature sensor. The channel is bonded with a cover plate etched by bulk micromachining technology to become a mico- channel reactor.

实验主要以微机电加工技术制作白金触媒微管道反应系统，利用微机电面型加工技术将白金薄膜电阻制作於基材为玻璃的晶片上，以此为反应所需的触媒及温度量测元件，并用体型加工技术蚀刻出微流道的上盖板相结合成微管道反应系统，本研究以1000μm、400μm及40μm的白金触媒微管进行测试，并利用微管道管壁上触媒表面降低反应活化能的特性来维持反应，此微反应系统利用氢气与氧气在白金触媒平板上的放热反应作为能量的来源。

The method comprises following steps: reacting hydroxylation carbon nano-tube successively with reagent containing halogen and hydrosulphide to prepare sulfhydryl carbon nano-tube; reflowing the sulfhydryl carbon nano-tube and platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum / carbon nano-tube catalyst; reflowing the sulfhydryl carbon nano-tube successively with the hydrochloroauric acid and the platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum-gold / carbon nano-tube catalyst.

本发明将市售羟基化碳纳米管先后与含卤试剂和氢硫化物反应得到巯基化碳纳米管。再将巯基化碳纳米管与铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂/碳纳米管催化剂。将巯基化碳纳米管依次与氯金酸和铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂-金/碳纳米管催化剂。

The thesis studies the difference between GWSs composition and traditional workflow applications, proposes the implement mechanism and technical architecture of GWSs composition and defines the reference model of GWSs composition platform, which provide holistic framework and top-level guidance for studying dynamic GWSs composition technology, designing GWSs composition platform, and implementing representative composite service applications.2、Theories and methods of composite process modeling and process analysis. This thesis proposes a meta-model of Geo-spatial Web services composition process defining from two aspects, i.e. process and resource. According to the process definition meta-model, we propose a new Geo-spatial Web services composition Process/Resource model based on extended WF-net, which effectively resolves the problems on uncertain activity option and dynamic variation of service in composite process model. A notion with regard to soundness of process model is proposed from three aspects, i.e. the structural correctness of process model, validity of data link and validity of resource. The notion of soundness definitely gives a dividing line on correctness of composite GWS process. This thesis analyzes sufficient and essential terms of soundness, and studies compositional property of WSCP/R-net models which provides an effective method to construct a soundness WSCP/R-net model. According to WSCP/R-net, the thesis proposes composition algebra and studies the properties of it. Based on the composition algebra, 6 kinds of composite process reduction rules are induced to optimize the process.3、Geo-spatial Web service QoS model and its application architecture. This thesis proposes an extendable GWS QoS model from three aspects, i.e. Geo-spatial Web Service itself, networking conditions and service consumer which can be used to distinguish GWSs with overlapping or identical functionality. We work over the QoS evaluation methods of composite GWS process which can be used to guide the execution, monitor and service selection of composition process. Aming at some disadvantages in traditional Web service discovery model for its lacking of QoS supporting, this thesis proposes a new service discovery model SDMQ supporting QoS constraints.4、Technologies of composite service executing. SSPL, a new composite service process language, is defined to overcome the disadvantages of existing composite services process languages which can not adapt to the dynamic variation of Geo-spatial Web Services. An algorithm is described to translate WSCP/R-net model into SSPL. The thesis studies the model of dynamic services selection with QoS global optimization, presenting an algorithm GODSS to resolve dynamic services selection with QoS global optimization in GWSs Composition.5、Design and implement experimental system and representative applications. According to the research findings presented above, we design and implement an experimental system and construct two representative applications to show that our achievements are effective and practical.

针对当前空间信息服务聚合研究中存在的若干不足，本文重点在基于工作流的空间信息服务聚合框架、空间信息服务聚合流程建模和分析技术、空间信息服务QoS模型及应用体系以及空间信息服务聚合流程执行等几个方面进行深入研究，主要工作和创新点包括：1、基于工作流的空间信息服务动态聚合框架：研究了空间信息服务动态聚合和传统工作流应用的不同，在此基础上提出了基于工作流技术的空间信息服务动态聚合实现机制、技术体系和参考模型，为研究空间信息服务聚合的关键技术、开发服务聚合支撑平台以及在此基础上构造特定的空间信息服务聚合应用提供了总体框架和顶层指导。2、空间信息服务聚合流程建模和分析技术：首先基于动态服务聚合流程建模的需求和空间信息服务动态变化的应用实际，从服务聚合的过程维和资源维出发定义了服务聚合流程定义元模型；与之相对应，对基本的WF-net进行扩展，提出服务聚合流程/资源网作为空间信息服务聚合流程的形式化描述模型，有效解决了现有的基于基本Petri网和工作流网的服务聚合建模方法所不能解决的不确定路径选择和服务的动态变化性问题；从流程结构正确性、数据依赖有效性和资源实现有效性三个方面提出了WSCP/R-net健壮性的概念，明确界定了聚合流程正确性的标准，并对WSCP/R-net模型的健壮性分析方法和WSCP/R-net模型的组合特性进行了研究；提出了空间信息服务聚合代数算子并对其性质进行了研究，在此基础上提出了6种聚合流程约简规则，从而可达到优化聚合流程、提高聚合流程执行效率的目的。3、空间信息服务QoS模型和应用体系：从服务本身、网络环境和服务消费者三个层次出发，提出了一个可扩展的空间信息服务QoS模型GSQM，实现了对空间信息服务的度量和评价，并对GSQM不同质量要素信息的客观、公正采集方法进行了研究；研究了空间信息服务聚合流程QoS评价方法，有效支持了空间信息服务聚合流程的执行、监控以及服务选择等操作；针对目前的服务发现模型仅支持服务功能性描述、不能有效满足空间信息服务应用需求的现状，提出了一种新的支持QoS约束的服务发现模型SDMQ，并对模型的实现框架进行了研究。4、空间信息服务聚合流程执行技术：针对现有的服务聚合流程描述语言不能有效满足空间信息服务动态聚合流程描述的特点，基于BPEL4WS提出了一种新的空间信息服务聚合流程描述语言SSPL；研究了满足健壮性要求的WSCP/R-net模型向SSPL的转换算法，在此基础上可以满足用户无显式编码来实现空间信息服务聚合应用的目的；研究了服务动态选择QoS全局优化模型，并在此基础上提出了一种解决服务动态选择QoS全局优化问题的实现算法GODSS.5、基于论文研究成果，设计实现了"空间信息服务聚合实验系统"，并构建了"矿产资源评价"和"城市消防应急响应"两个典型应用案例，对论文所述模型、方法的可行性和有效性进行了验证。

Main points of the thesis are as follows:(1) The main function models and information relations between these models in the CAPP system in the integrated CAD/CAM project are explained, a new process plan design method is mentioned based on analyses of process plan design. This method is based on the process plan prototype, and develops the prototype little by little until the perfect process plan is completed, the prospect of this method is discussed;(2) The feature abstracting rules and methods are studied, a feature coding system is developed based on GT, all the defined feature models are described by the mathematical methods;(3) The integrated method of CAD/CAPP based on features is mentioned, this method defines a feature exchanging model, and develops an interface software to exchange design data into technology data base, this technology data base includes the design and technology information of the parts;(4) The process plan reasoning method based on features is created, this method uses Mycin algorithm to solve the reasoning of the feature process plan. A process plan making system is developed. In this system part process plan is made by the semi-intelligent method, this method uses the feature reasoning, feature process chain searching and man-computer talking together;(5) The main structure of the HOPE system is introduced, a shaft drawing and its process plan made by this system are shown, the data process problem in process drawing making is also discussed;(6) A new method of describing process rule is introduced, this method uses IfThen rules and neural nets weight values together to describe process rules, the BP algorithm is adopted in this method;(7) The optimal machining sequence problem of the process steps on the same fixturing is discussed, optimal algorithms SA is applied to solve this problem, the result shows that this method is more efficient than the traditional method;(8) All jobs in the thesis are summarized. In order to carry out the research in the future, some rational proposals are given.

全文论述的内容主要有下列几个方面：(1)较为系统地阐述了CAD／CAM一体化工程项目中CAPP系统的主要功能模块及其信息流程，在分析工艺设计过程的基础上，提出了基于特征原型的渐进式工艺设计方法，并探讨了该方法的应用前景；(2)研究了零件特征提取的原则和方法，在成组技术的基础上，开发了一套基于特征的分类编码系统，并在提取零件特征的基础上，定义了零件特征的数据模型，开发了基于轴类零件特征的参数化设计系统；(3)研究了基于特征的CAD／CAPP集成的方法，通过定义零件特征数据模型的存储结构，开发了将设计数据转换到工艺数据库中的接口程序，为后续的CAPP系统提供必要的零件形状和工艺信息；(4)研究了基于特征的工艺推理方法，将Mycin算法应用到工艺决策中，开发了基于特征的工艺推理及工艺方案生成系统，在系统中综合运用特征推理、特征加工工艺链查询及人机对话相结合的半智能化方法确定零件加工工艺；(5)介绍了整个HOPE系统的总体结构，通过运行HOPE系统绘出了一轴类零件的零件图，并生成了该零件的加工工艺方案，初步探讨了基于特征的工序图生成技术中数据处理问题；(6)研究了工艺设计过程中知识如何有效表示的问题，提出了将显式的IF-THEN规则表示与隐式神经网络权值表示相结合的工艺知识表示方法，并利用BP算法进行了工艺知识表示的初步研究；(7)研究了工艺设计过程中同一安装下工步优化排序问题，利用神经网络中基于模拟退火的理论来解决该工步优化排序问题，实践证明该方法较传统的算法具有更高的效率；(8)总结了本文所进行的研究工作，为今后进一步开展工作提出了较为合理的建议。

And then the functionalized carbon nanotube, partial platinum salt and all transition metal M salt are stirred and reflow for certain time, added with rest platinum salt to continue to reflow, cooled, washed centrifugally, dried and carried out heating treatment in a hydrogen atmosphere, thus obtaining the anchoring platinum catalyst of the transition metal on the carbon nanotube.

然后将功能化的碳纳米管与部分铂盐和全部过渡金属M盐在多元醇溶剂中搅拌回流一定时间后，加入剩余的铂盐继续回流，冷却，离心洗涤，烘干，最后在氢气气氛中热处理，得到碳纳米管上过渡金属锚定铂催化剂。

The shops sell professional-series of temperature control, high-temperature-series, electric products, the company is involved in: TDA series of temperature control instrumentation, TDW series of temperature control instrumentation, TEA series of temperature control instrumentation, XMT series of temperature control instrumentation, XMTA series of temperature control instrumentation , XMTD series of temperature control instruments, temperature control switches, temperature table, pressure gauge, double-metal thermometer, WRN thermocouple, WRE thermocouple, WRP thermocouple, WZP thermocouple, WRNK thermocouple, WREK thermocouple , WRCK thermocouple, WZPK thermocouple, sensors, Yahuang dual, dual screw, handheld digital thermometer, CU50 copper resistance, Pt100 ceramic platinum resistance, Pt100 stainless steel platinum resistance, Mica platinum resistance, high temperature wire, wire compensation , High temperature resistant fabrics, high temperature tape, yellow wax tube, since the income of resin, stainless steel tube of electric, electric carbon steel pipe tubes, electric heating of the brass, titanium tube electric tube, the single electric, electric water heaters use of, water, Pot use of electric heating, the sauna, explosion-proof electric heating pipe, iron core, Dianre Dai, box-type electric furnace, an electric stove, oven, the oven, melting furnace tin, nickel chromium resistance wire, iron wire chromium resistance, resistance zone, civilian Furnace wire, high-power industrial furnace silk, mica films, a variety of high temperature ceramic beads, ceramic pads, hairdryer batteries, electric furnace set, the furnace Church, outside the wire, stainless steel bolts, 2.60, 2.60, stainless steel bolts, stainless steel - Head bolt, the first half of stainless steel bolts, stainless steel pan head bolts, stainless steel expansion bolts, self-tapping stainless steel, stainless steel core pulling rivets, stainless steel jets hoop, stainless steel wire hoop, stainless steel plates, stainless steel bar, stainless steel flanges, stainless steel pipe, Stainless steel wire, a variety of metal hose bridge.

本门市部专业销售温控仪系列、高温线系列、电热系列产品，产品涉及：TDA系列温控仪表、TDW系列温控仪表、TEA系列温控仪表、XMT系列温控仪表、XMTA系列温控仪表、XMTD系列温控仪表、温控开关、水温表、压力表、双金属温度计、WRN热电偶、WRE热电偶、WRP热电偶、WZP热电偶、WRNK热电偶、WREK热电偶、WRCK热电偶、WZPK热电偶、传感器、压簧偶、螺钉偶、数显手持式温度计、CU50铜电阻、Pt100陶瓷铂电阻、Pt100不锈钢铂电阻、云母铂电阻，耐高温导线、补偿导线、耐高温布、耐高温胶带，黄腊管、树脂自息管、不锈钢管电热管、碳钢管电热管、铜管电热管、钛管电热管、单头电热管、热水器用电热管、电水壶用电热管、桑拿管、防爆电热管、电熨斗芯、电热带、箱式电炉、民用电炉、烘箱、烤箱、熔锡炉、镍铬电阻丝、铁铬电阻丝、电阻带、民用电炉丝、大功率工业电炉丝、云母片、各种规格的耐高温瓷珠、瓷垫片、吹风芯、电炉盘、炉堂、外丝管、不锈钢外六角螺栓、不锈钢内六角螺栓，不锈钢沉头螺栓、不锈钢半圆头螺栓、不锈钢盘头螺栓、不锈钢膨胀螺栓、不锈钢自攻丝、不锈钢抽芯铆钉、不锈钢喉箍、不锈钢钢丝箍、不锈钢板材、不锈钢棒材、不锈钢法兰、不锈钢管件、不锈钢丝、各种规格的金属软管、桥架。

The results show that the three kinds of heteropolyacid modified platinum electrodes have the higher electrocatalytic activity to methanol oxidation, PMnMo11 modified platinum electrode has the highest electrocatalytic activity. Meanwhile the anti-poison effect to carbon monoxide of platinum electrode can been improved by modification of transition metal substituted phosphomolybdic acid.

结果表明，三种过渡金属取代磷钼酸修饰铂电极均能够提高铂电极的催化活性，其中PMnMo11修饰铂电极对甲醇的催化活性最高，同时铂电极经三种过渡金属取代磷钼酸修饰后抗一氧化碳毒化能力增强。

The system can be widely used in belt weighing and batching process control,etc.

介绍了基于智能模糊控制的嵌入式配料系统的设计方法，对模糊PID控制过程和系统调零作了重点的讨论，同时给出了PID控制的程序流程图和系统定长调零子程序。

"I dunno," she answered,"but if you show me aroun', I'll recognize it from the lighthouse just outside the porthole."

"我不知道，"她回答说，"如果你能带我转转，我能认出来的，因为灯塔就在舷窗外。"