查询词典 oxidation-reduction titration

Compared with that of 3Cr13 alloy, the oxidation resistance of the composites containing 5 vol.％TiC particle was improved greatly at 850℃, but the improvement was relatively limited at 950℃. But the oxidation resistance of 1Cr18Ni9 composites containing 5 vol.％ TiC particle was obviously improved at 950℃, and at 850℃ the improvement is not large. The TiC particle can improve the oxidation resistance mainly was by developing the oxidation selectiveness of the Cr element as to change the phase constitution of the oxidation film, to alleviate the production of the stress in the oxidation film and to improve the cohesive force of the oxidation film or matrix interface and the chemical combination of the oxidation film.

与3Cr13合金相比，含5％volTiC颗粒的复合材料在850℃的抗氧化性能得到大幅度提高，而在950℃复合材料的抗氧化性能提高作用却是有限的；与1Cr18Ni9合金相比，含5％volTiC颗粒的复合材料在850℃的抗氧化性能略有提高，而950℃复合材料的抗氧化性能提高却是明显的；TiC颗粒可以提高两种基体合金抗氧化性能，主要是通过促进Cr的选择性氧化，进而改变氧化膜的相组成、减缓氧化膜内应力的产生、增加氧化膜/基体界面凝聚力及提高氧化膜化学结合力而实现的。

Thus this method could be applied to monitor the process of producing dinitrogen pentoxide by electrochemical oxidation of dinitrogen tetroxide in nitric acid. The results from the two-step titration method of redox titration combined with acidity titration were well consistent with that from the method of redox titration combined with NMR.

氧化还原和酸度两步滴定与氧化还原滴定结合核磁共振光谱法的分析结果表明，两种方法的分析结果吻合良好，精确度良好，两种方法都可用于N_2O_4-N_2O_5-HNO_3体系各组分的全浓度分析。

In the paper following the change law of concentration and electric potential of different stage oxidation-reduction titration and appling the Nernst formula, it was discussed that the application of Ringbom error formula in symmetry donblet oxidation-reduction titration.

本文遵循氧化还原滴定各个阶段的浓度与电位变化规律，运用能斯特公式，探讨了能适用于氧化还原滴定中对称电对的林邦误差公式，具有便于记忆与应用等特点。

Take for the amount of test materials, precision that set, place beaker, unless otherwise specified, may be added 40ml of water and hydrochloric acid solution (1-2) 15ml, and then set on a magnetic stirrer, stirring allows the dissolved, together with potassium bromide 2g insert platinum - platinum electrode, it will insert the solution of the following buret tip is about 2 / 3, using sodium nitrite titration solution (0.1mol / L, or 0.05mol / L) rapid titration, side drops while stirring, to near point, Burette tip surface will be presented with a small amount of water leaching cutting-edge, lotion, and solution and continue titration slowly until the sudden deflection of galvanometer pointer, namely, titration end point.

取供试品适量，精密称定，放置烧杯中，除另有规定外，可加水40ml与盐酸溶液（1-2）15ml，而后置电磁搅拌器上，搅拌使溶解，再加溴化钾2g，插入铂-铂电极后，将滴定管的尖端插入溶液下面约2/3处，用亚硝酸钠滴定液（0.1mol/L或0.05mol/L）迅速滴定，边滴边搅拌，至近点时，将滴定管的尖端提出液面，用少量水淋洗尖端，洗液并溶液中，继续缓缓滴定，至电流计指针突然偏转，即为滴定终点。

The titrant is a mixture of EDTA and sodium fluoride, both mercury film electrode and fluorinion selective electrode are inserted in the titration solution. In a process of titration, both the added volume of titrant and the concentration of mercury ion at each titration point can be obtained simultaneously from the potentials of two electrodes, and then the concentration of each component in the alloy can be obtained from the titration curves by multivariate calibration.

用ED-TA与氟化钠的混合溶液作为滴定剂，被滴定液中同时插入了汞膜电极和氟离子选择电极，在滴定过程中的任一滴定点，溶液中汞离子的浓度和滴定剂的加入体积可由两个电极的电位测定值同时获得，从而可应用多元校正法由相应的滴定曲线求得混合金属中每一种组分的含量。

With the raw material and the particle size of reducing agent narrowed, the percent reduction of strontia increases.(6) With the barbecuing pressure increasing, the percent reduction of strontia increases, after the certain value, the percent reduction of strontia decreases instead.(7) With reduction temperature increasing, the percent reduction of strontia increases.(8) The percent reduction of strontia is increasing with prolonging reduction time. In this experimental condition, it will become steady after 2.5h.

通过实验研究确定以SrCl_2-SrF_2-SrCO_3的纯锶盐体系作为电解质，实验中还采用了我们最新研制的熔盐电解监控仪对电解过程进行测量和系统的研究，得出以下结论：(1)增加电流强度，反电动势亦随之增加，而升高温度反电动势则有所降低；(2)随着电流密度的升高和电解时间的延长，电流效率逐渐增加，达到峰值后稳步下降；(3)延长电解时间，合金中锶的含量逐渐增加，最高可达18.1％；(4)开始电解后，反电动势逐渐增加，但向熔体中加入SrCO_3后，反电动势明显降低，因此认为在正常电解时是SrCO_3在分解。

In the paper,the transmission of designed roller oscillating tooth reduction gear adopts osci llating tooth gear drive without exception,one-stage reduction gear and two-stage reduction gear have joined through spline coupling band;The joining way of shock wave thellomble and oscillating tooth adopts the biserial bearing of without inner ring of needle bearing,and directly adopts bearing outer ring as shock wave thellomble;Center wheel of two-stage reduction gear and center wheel of two-stage reduction gear passes through taper thread,and center wheel is fixed;As soon as the flange of input end and center wheel of one-stage reduction gear,the flange of export end and center wheel of two-stage reduction gear makes monobloc structure.

本文预设的井下减速器的传动均采用活齿传动，一级减速器的输出轴和二级减速器的输入轴通过花键联轴套联接；激波环与活齿的毗连方式采用能蒙受较大载荷的无内圈双列滚针不锈钢管，且直接采用不锈钢管外圈作为激波环；一级减速器的中心轮和二级减速器的中心轮是通过锥螺纹毗连的，且中心轮固定；一级减速器的中心轮与输入端的法兰盘，二级减速器的中心轮与输出端的法兰盘均做成整体的结构。

In the paper,the transmission of designed roller oscillating tooth reduction gear adopts oscillating tooth gear drive without exception,one-stage reduction gear and two-stage reduction gear have joined through spline coupling band;The joining way of shock wave thimble and oscillating tooth adopts the biserial bearing of without inner ring of needle bearing,and directly adopts bearing outer ring as shock wave thimble;Center wheel of two-stage reduction gear and center wheel of two-stage reduction gear passes through taper thread,and center wheel is fixed;As soon as the flange of input end and center wheel of one-stage reduction gear,the flange of export end and center wheel of two-stage reduction gear makes monobloc structure.

本文设计的井下减速器的传动均采用活齿传动，一级减速器的输出轴和二级减速器的输入轴通过花键联轴套联接；激波环与活齿的连接方式采用能承受较大载荷的无内圈双列滚针中国财经圈，中国财经圈，且直接采用进口中国财经圈外圈作为激波环；一级减速器的中心轮和二级减速器的中心轮是通过锥螺纹连接的，且中心轮固定；一级减速器的中心轮与输入端的法兰盘，二级减速器的中心轮与输出端的法兰盘均做成整体的结构。

If by means of a prereduction MRI or after neurologic deterioration during closed reduction, the surgeon becomes aware of a fragment of disc material displaced into the spinal canal, then an anterior discectomy, open reduction, fusion, and plating becomes necessary.2,7,9 In approximately half of the cases, a closed reduction will be successful in reducing the dislocation before surgery.50 In the majority of the others, an intraoperative reduction performed after the discectomy and decompression will achieve anatomic reduction.9,51 For those patients in whom an anterior discectomy and decompression have not been successful in reducing the dislocation, then a supplemental posterior open reduction should be performed.52

假如借助MRI检查，或在闭合复位过程中神经症状进一步加重，外科医生意识到有椎间盘碎片突入了椎管，此时就需要前路椎间盘切除减压、开放复位和固定融合。大约有一半的病例手术以前能够通过闭合复位来成功的将脱位复原，剩下的病例则需要在术中将椎间盘切除减压来达到解剖复位。假如有病人经过前方的椎间盘切除和减压后仍然不能成功的还原脱位，则需要再行后方的开放复位术。

Use AgNO3 titration testing,acid and alkali titration, automatic electrical potential titration respectively to detect the dialdehyde content.

通过四种醛基检测方法的比较，AgNO3滴定法是测定醛基含量最适宜的，从分析手段来讲，也是简便易行成本较低的。

Warden: That's a beautiful dog, but don't bring her again.

那是条漂亮的狗，但是不要再把她带来了。

You get up in the morning – no hangover!

你第二天早上起来的时候—不会宿醉！