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The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.

以4，5-二羧酸咪唑为原料的较佳工艺：1 脱羧反应：4，5-二羧酸咪唑40g，醋酐1200ml，回流10h，过滤并将滤液浓缩至干，所得固体加至50%的乙醇溶液回流，过滤并将滤液自然冷却过夜，过滤得固体；2 酯化反应：4(5)-羧酸咪唑50g，乙醇1000ml和浓硫酸60ml，加热回流2h，5%浓度NaOH溶液调节至pH＝8，减压浓缩至干，加入少量水回流，自然冷却过夜并过滤得固体；3 还原反应：LiAlH410g，乙醚300ml和4(5)-羧酸咪唑乙酯28g，常温反应1.5h，小心滴加25ml水后过滤，滤渣溶于300ml甲醇中并过滤，收集所得乙醚和甲醇滤液浓缩至干，将所得固体溶于300ml乙醇中加热回流，后将溶液浓缩至约30ml，冷却并过滤得固体，该路线总收率为49.6%。

Pass to count to Wisterch parameter , and the steel wire is different from the molding tool get in touch with the length, and settle the path the research taking the length work the stabber angle to get under differently pull to stir the term, mold core adoption of best severally why size, combine the best work stabber of research the Cape, and settle the path to take the length nextly steel wire is in the molding tool of have fever to measure, air inside dispel-heat calories, winding dispel-heat on the coil-canister , and its molding tool dispel-heat calories of, and cause the steel wire the temperature difference pass in and outing the molding tool to influence steel wire machine function, under the experiment inside pull to stir the term according to the same race different work stabber Cape half of adoption the Cape(7 degree,10 degree,12 degrees, the best mold Cape, experience mold Cape) settle the path to take the length(2-3 mm,3-4 mm,4-5 mms, theories length, experience length) to proceed to experiment, and get the conclusion, work stabber the Cape then is more big the steel wire get in touch with the length with

通过对Wisterch参数，钢丝与模具接触长度、定径带长度、工作锥角度的研究得到了在不同拉拨条件下模芯采用的最佳几何尺寸，并研究最佳工作锥角、定径带长度下钢丝在模具中的发热量、空气中散热量、卷筒上的散热量及其模具散热量的不同，导致钢丝进出模具的温度差别对钢丝机械性能的影响，在实验中根据同种拉拨条件下采用不同工作锥角半角、定径带长度进行试验，得出结论，工作锥角越大则钢丝与模具接触长度越短，钢丝变形越剧烈，在模具中发热量就越高，导致钢丝出模温度高，使钢丝强度、硬度升高，弯曲、扭转次数降低，并且降低模具使用寿命。在其它条件相同的情况下，定径带越长则钢丝与定径带简壁磨擦增大，使钢丝发热量加大，从而使钢丝强度、硬度略升高，弯曲扭转次数略降低但定径带的增大减小了钢丝变形产生的弹性后效使钢丝出模直径比较稳定。

First, i want to introduce myself, my name is Zhangsan,I am 24years old,from a small city which in the south of China,,in 2007 ,I was graduate from nomal university,get the baccalaureate of law.After my graduated,I once did some selling work, but I still want to do some work in law, but in China, that the students who's major was law was very difficult for get job,it is quite diffrent from your weatern country. so long ago, I have been get a plan for go abroad to get a master's degree in law. but for my poor English and economy,I think it is very hard to me.

我先向你自我介绍下，我叫张三，今年24岁，来自中国南方的一个小城市，2007年毕业于一所普通的大学，拿到了法学学士，毕业后做过一段时间的销售工作，我一直想从事法律方面的工作，但是在中国教育背景下，法律专业的就业前景不好，这不同于你们西方国家，所以我早就萌发了出国继续深造攻读硕士的念头，但是由于英语水平太差和家庭条件不好，感觉不太现实，一直没有去争取。

We cannt get result on how to change course and speed to make collision avoidance, this can help little on collision avoidance decision.The article aims at the default on Radar simulator and implements the standard result on Radar simulator by making use of MCU.the main production is below:First, we calculate how to chang course and speed on the destine point by MCU. We get the new course and new speed on the destine point,we get the point to resume original course and speed, we get the distance and azimuth to resume original course and speed on given course and speed, the six essential: DCPA, TCPA, distance, azimuth,real speed and real course.

本论文针对当前雷达模拟器标绘训练中的不足，实现了利用单片机进行雷达模拟器标绘标准值的计算，主要成果有以下方面：首先，利用单片机计算得到了在预定点改变航向和改变航速的计算，求得预定点改向的新航向C_N和预定点变速的新速度V_N，恢复原航向和原航速的时机点的计算；在给定避碰的新航向、航速的条件下，计算出恢复原航向／航速的时机点H的距离R_H和方位θ_H；目标船的六要素，即DCPA、TCPA、距离R、方位θ、真航速V_T和真航向C_T。

He's unbelievable Chorus So tonight I'm gonna get him Got a rendezvous at seven Faire l'amour toujours, so funny Wanna spend all of this money Should I wear a dress and high heels Should I go out in my blue jeans He's the boy I met in my dreams And I tell you girls He's unbelievable Verse 1 Sisters, only sometimes You can meet the kind of boy Who will always give you joy Then grab him, never let him Take him deep into your world Be aware of their girls He's so unbelievable Finally it is me, see me happy Today I have found him He's the boy of my dreams And he's unbelievable So tonight I'm gonna get him Got a rendezvous at seven Faire l'amour toujours, so funny Wanna spend all of this money Verse 2 Brothers, only mothers Have the right to decide What is wrong or what is right But you maybe find a baby Who is no the kind of girl To fit in your mother's world He's so unbelievable Ain't a doubt shout it out that you love her Only such a tough guy Could become my only one Cause he's unbelievable Chorus C-part Sharp dressed you may face your rendezvous Depressed if he's not good looking too Maybe he's a lazy kind of lad Don't forget he could turn into a prince in bed Be sure that he's standing by your side Cowards are a waste of time Get it on if he's always on your mind But avoid being love-blind Look out for his sensitivity Check out if he knows just what it means To give everything that a lady needs To prove that his love is pretty real Some guys only show their sex appeal And who knows why the lord had made 'em If you think he's the right guy fall in love If he's not keepin' your hands off Chorus So tonight I'm gonna get him Got a rendezvous at seven Faire l'amour toujours, so funny Wanna spend all of this money Should I wear a dress and high heels Should I go out in my blue jeans He's the boy I met in my dreams And I tell you girls He's unbelievable Supernatural things will happen I can call you at eleven I will tell you every detail If he's worth it or if he failed But I know he drives me crazy And I want to have his baby So you must excuse me, ladies Did I tell you that He's unbelievable

他难以置信合唱团因此，今晚我一定让他有7个约会放任倾慕始终，所以好笑想花的所有钱如果我穿衣服和高跟鞋我应该走出去在我的蓝色牛仔裤他是我遇到的男孩在我的梦想我告诉你女孩他难以置信新诗1 姐妹们，有时只你能满足什么样的男孩谁将永远给你快乐然后抓住他，从未让他他深入到你的世界知道自己的女孩他是如此难以置信最后，就是我，见我高兴今天，我发现他他是男孩，我的梦想他的令人难以置信因此，今晚我一定让他有7个约会放任倾慕始终，所以好笑想花的所有钱诗二兄弟，只有母亲有权决定什么是错误的或什么是正确的但是，你也许找到一个婴儿没有谁是什么样的女孩以适合您母亲的世界他是如此难以置信不是一个疑问喊出来，你爱她只有这样一个硬汉可以成为我的唯一原因，他难以置信合唱团架C -一部分夏普穿着你可能面临的会合抑郁症患者，如果他不是太漂亮也许他是一个懒惰的小伙子不要忘记他可以变成一个王子在床上可以肯定，他站在你身边懦夫是在浪费时间获取它如果他总是在你心里但是，避免被爱情盲目请注意他的敏感性退房，如果他知道刚才这意味着什么为了让所有需要一位女士为了证明他的爱很真实有的人只展示自己的性吸引力谁知道，为什么大人了他们如果您认为他的权利人爱上如果他不是keepin '你的手离开合唱团因此，今晚我一定让他有7个约会放任倾慕始终，所以好笑想花的所有钱如果我穿衣服和高跟鞋我应该走出去在我的蓝色牛仔裤他是我遇到的男孩在我的梦想我告诉你女孩他难以置信超自然的事情会发生我可以打电话给您， 11 我会告诉你，每一个细节如果他的价值，或者，如果他失败但是我知道他硬盘我疯了和我想他的孩子所以，你必须原谅我，各位我告诉你，他难以置信

Results In this group of cases,68 cases get bronchopneumonia(53.1%),30 cases get stromalatic pneumonia(23.4%),12 cases get big focal pneumonia(9.4%),10 cases get lobar pneumonia and segmented pneumonia(7.8%).

结果：本组病例中支气管肺炎68例（占53.1％），间质性肺炎30例（占23.4％），大病灶肺炎12例（占9.4％），大叶和节段性肺炎10例（占7.8％），心后影征5例(占3.9%)，上纵隔心缘、横膈模糊征3例(占2.3%)。

Know i can be what i wanna be if i work hard at it i'll be where i wanna be (i'll be where i wanna be) be, b-boys and girls, listen up you can be anything in the world, in god we trust an architect, doctor, maybe an actress but nothing comes easy it takes much practice like, i met a woman who's becoming a star she was very beautiful, leaving people in awe singing songs, lina horn, but the younger version hung with the wrong person gotta astrung when i heard when cocaine, sniffing up drugs, all in her nose coulda died, so young, no looks ugly and old no fun cause when she reaches for hugs people hold they breath cause she smells of corrosion and death watch the company you keep and the crowd you bring cause they came to do drugs and you came to sing so if you gonna be the best, i'ma tell you how put your hands in the air and take the bell [chorus -2x] i know i can be what i wanna be if i work hard at it i'll be where i wanna be (i'll be where i wanna be) be, b-boys and girls, listen again this is for grown looking girls who's only ten the ones who watch videos and do what they see as cute as can be, up in the club with fake id careful,'fore you meet a man with hiv you can host the tv like oprah winfrey whatever you decide, be careful, some men be rapists, so act your age, don't pretend to be older than you are, give yourself time to grow you thinking he can give you wealth, but so young boys, you can use a lot of help, you know you thinkin life's all about smokin weed and ice you don't wanna be my age and can't read and right begging different women for a place to sleep at night smart boys turn to men and do whatever they wish if you believe you can achieve, then say it like this save the music y'all, save the music y'all save the music y'all, save the music y'all save the music be, be,'fore we came to this country we were kings and queens, never porch monkeys it was empires in africa called kush timbuktu, where every race came to get books to learn from black teachers who taught greeks and romans asian arabs and gave them gold when gold was converted to money it all changed money then became empowerment for europeans the persian military invaded they learned about the gold, the teachings and everything sacred africa was almost robbed naked slavery was money, so they began making slave ships egypt was the place that alexander the great went he was so shocked at the mountains with black faces shot up they nose to impose what basically still goes on today, you see?

知道我可以。是我想。如果我努力学习它。我将会在哪里，我想我将会在哪里，我想。是，b-boys和女孩，仔细听好了你可以在这个世界上，我们相信上帝建筑师、医生、也许是一名演员但什么是轻易造成大量练习喜欢，我遇见了一个女人的成为一个明星她非常美丽，让人敬畏唱歌，埃德喇叭，但年轻的版本挂着一个错误的人当我听到时要astrung 闻起来，可卡因，在她的鼻子的药物本来，年轻，没有死亡，看起来很丑陋当她到达任何有趣的原因，人们认为他们拥抱气息因为她的腐蚀和死亡的主要原因。气味看你的人群，你带因为他们来做药物和你来唱所以如果你要成为最好的，我会告诉你怎么做把你的手在空中和带铃 [合唱-2x] 我知道我可以。是我想。如果我努力学习它。我将会在哪里，我想我将会在哪里，我想。是，b-boys和女孩，再听一遍这是为了寻找女孩长大的只有十分钟那些看录像，他们看到了些什么作为可爱，就可以在俱乐部和假身份证小心，你遇到一个人涌现hiv病毒你可以在电视主持人奥普拉·温芙瑞一样无论你决定，要小心，一些人你的年龄，所以法案强奸犯，不要假装比你大，给自己时间长你认为他能给你的财富，而是这样年轻的男孩，你可以用很多的帮助，你知道的你thinkin生活的全部smokin杂草和冰你别想成为我的年龄和不能读英语和正确的为不同的女性乞讨，晚上睡不着觉聪明的男孩把男性做任何他们的愿望如果你相信你能达到的，就像这样说保存音乐偷鸡摸狗，节省了音乐偷鸡摸狗保存音乐偷鸡摸狗，节省了音乐偷鸡摸狗节省的音乐是，是，脱颖而出，我们来到这个国家我们被国王和王后们，从不门廊的猴子它是在非洲帝国库廷巴克图，在每一场比赛来买书如何从黑教师教希腊人和罗马人亚洲的阿拉伯人，并给他们黄金的时候金子被转化为钱都改变了钱便成了权力为欧洲人波斯的军队入侵他们知道金子、教导和一切圣物非洲几乎抢走了赤裸奴隶制是钱，于是他们开始做奴隶船埃及是亚历山大大帝的地方去他是如此的震惊和黑色的脸山上他们的鼻子强加给射击基本上什么今天还在继续，你看到了吗？

Know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) Be, B-Boys and girls, listen up You can be anything in the world, in God we trust An architect, doctor, maybe an actress But nothing comes easy it takes much practice Like, I met a woman who's becoming a star She was very beautiful, leaving people in awe Singing songs, Lina Horn, but the younger version Hung with the wrong person Gotta astrung when I heard when Cocaine, sniffing up drugs, all in her nose Coulda died, so young, no looks ugly and old No fun cause when she reaches for hugs people hold they breath Cause she smells of corrosion and death Watch the company you keep and the crowd you bring Cause they came to do drugs and you came to sing So if you gonna be the best, I'ma tell you how Put your hands in the air And take the bell I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) Be, B-Boys and girls, listen again This is for grown looking girls who's only ten The ones who watch videos and do what they see As cute as can be, up in the club with fake ID Careful,'fore you meet a man with HIV You can host the TV like Oprah Winfrey Whatever you decide, be careful, some men be Rapists, so act your age, don't pretend to be Older than you are, give yourself time to grow You thinking he can give you wealth, but so Young boys, you can use a lot of help, you know You thinkin life's all about smokin weed and ice You don't wanna be my age and can't read and right Begging different women for a place to sleep at night Smart boys turn to men and do whatever they wish If you believe you can achieve, then say it like this I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) Be, be,'fore we came to this country We were kings and queens, never porch monkeys It was empires in Africa called Kush Timbuktu, where every race came to get books To learn from black teachers who taught Greeks and Romans Asian Arabs and gave them gold when Gold was converted to money it all changed Money then became empowerment for Europeans The Persian military invaded They learned about the gold, the teachings and everything sacred Africa was almost robbed naked Slavery was money, so they began making slave ships Egypt was the place that Alexander the Great went He was so shocked at the mountains with black faces Shot up they nose to impose what basically Still goes on today, you see?

f the truth is told， the youth can grow They learn to survive until they gain control Nobody says you have to be gangstas， hoes Read more learn more， change the globe Ghetto children， do your thing Hold your head up， little man， you're a king Young Prince thats when you get your wedding ring Your man is saying "She's my queen" I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) I know I can Be what I wanna be If I work hard at it I'll be where I wanna be (I'll be where I wanna be) Save the music y'all， save the music y'all Save the music y'all， save the music y'all Save the music 我认识我能是什么我想要当如果我工作难的在它我将是我想要当的地方我认识我能是什么我想要当如果我工作难的在它我将是我想要当的地方是， B-男孩和女孩，听在你能是任何事在世界上，在上帝我们信赖一位建筑师医生，也许一个女演员但是无来容易的它拿很多练习同类，我遇到了合式的一个女人一星她非常美丽，离开敬畏的人歌唱歌， Lina 喇叭，但是年纪较小者版本和错误的人吊必须 astrung 当我听到的时候当古柯碱，在药物上面嗅，所有的在她里面鼻子 Coulda 死了，如此年轻，没有容貌丑陋和旧的没有乐趣因素当她延伸为拥抱人把握他们呼吸引起她腐蚀和死亡的味道手表公司你保存和那群众你带来引起他们开始做药物和你开始唱因此如果你去是那最好， I'ma 告诉你如何把你的手放入那空气而且拿铃我认识我能是什么我想要当如果我工作难的在它我将是我想要当的地方我认识我能是什么我想要当如果我工作难的在它我将是我想要当的地方是， B-男孩和女孩，再听这是为长大的看只是十的女孩那人手表影像而且做什么他们见到当做可爱的当做能是，向上的在那以假的身份证联合行动小心的，'在前的你会一个患有爱滋病毒的男人你能主人像 Oprah Winfrey 一样的电视无论你决定，很小心什么，一些男人是强奸者，因此行为你的年龄，做不假装当资深者超过你是，给予你自己时间生长你思考他能给予你财富，但是如此年轻的男孩，你能使用许多帮忙，你知道你 thinkin 生活所有有关 smokin 杂草和冰的事你做不想要当我的年龄和不能阅读和权利为一个地方请求不同的女人到睡眠在晚上聪明的男孩求助于男人而且做任何的他们希望如果你相信你能达成，然后发言权它同类这我认识我能是什么我想要当如果我工作难的在它我将是我想要当的地方我认识我能是什么我想要当如果我工作难的在它我将是我想要当的地方是，是，'在前的我们总计了这国家我们是国王和皇后，从不门廊猴子它在叫做 Kush 的非洲是帝国 Timbuktu，哪里每个比赛开始拿书从教希腊人的黑色老师和罗马人了解亚洲人阿拉伯人而且给予了他们黄金当黄金是转换至钱它全部改变钱然后变成了欧洲人的赋与权能波斯的军队侵入他们有学问的大约黄金、教学和每件事物神圣的非洲几乎抢夺赤裸的奴隶的身份是钱，因此他们开始赚奴隶船埃及是地方亚历山大棒者去他是如此震动在山与黑色的脸注射在他们上面鼻子强加什么基本上仍然继续进行今天，你见到？

If hip hop should die before i wake i'll put an extended clip inside of my ak roll to every station, murder the dj roll to every station, murder the dj hip hop just died this mornin' and she's dead, she's dead [verse 1] yeah, niggaz smoke, laugh, party, and die in the same corner get cash, live fast, body their man's mama rich ass niggaz is ridin' with three llamas revenge in their eyes, hennesy and the ganja word to the wise with villain state of minds grindin', hittin' brazilian dimes from behind grindin', hittin' brazilian dimes from behind (grindin', hittin' brazilian dimes from behind) whenever, if ever, i roll up, it's sown up any ghetto will tell ya nas helped grow us up my face once graced promotional sony trucks hundred million in billin', i helped build 'em up gave my nigga my right, i could have gave left so like my girl foxy, a nigga went def so nigga, who's your top ten?

如果嘻哈应死之前，我醒来我将提出延长剪辑内，我的AK 轧辊，以每个车站，谋杀金大中轧辊，以每个车站，谋杀金大中嘻哈刚刚去世，这mornin '她的死，她的死亡 [诗1 ] 是啊， niggaz烟雾，笑，党，及模具在同一个角落获得现金，生活快，身体他们的人的妈妈丰富的驴niggaz是ridin '三马驼报复，在他们眼中， hennesy和印度大麻 Word中的英明与小人国的头脑 grindin '， hittin '巴西角从背后 grindin '， hittin '巴西角从背后（ grindin '， hittin '巴西角从背后）每当，如果，我卷起来，它的播种面积最多任何聚居区会告诉亚的NAS帮助我们成长起来我的脸，一旦交织的促销索尼卡车亿在billin '，我帮助建立了'射击给我nigga我的权利，我可以离开了因此，喜欢我的女孩推动国内， nigga到高清因此， nigga ，谁是你的十大？

Who? I never heard of him, Paul said, before asking teammate James Posey if he had heard of him.

赛后，科比说，他一直都是一名非常出色的射手，今天他打得很棒。

When I joined the company, I rotated around the different sections.

我加入这个公司时，轮换过几个不同的部门。