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To study the chemical constituents from the leaves of Celastrus gemmatus Loes., chromatographic methods were used to isolate and purify the chemical constituents, their structures were elucidated by the physiochemical characteristics and spectral data.

为研究哥兰叶(Celastrus gemmatus Loes。)中的化学成分,用Diaion HP-20,Toyopearl HW-40,silica gel等柱色谱方法,从其70﹪含水丙酮提取物中分离得到化合物,并根据理化性质和波谱数据鉴定其结构。

RESULTS:12 compounds separated from Dendranthema nankingense were elucidated as cerotic acid,β-sitosterol,ursolic acid,chrysoeriol,luteolin,caffeic acid,daucosterol,chrysoeriol-7-O-glucoside,luteolin-7-O-glucoside,linarin,rutin and potassium nitrate.

结果:从菊花脑中分离得到12个化合物,即正二十六烷酸、β-谷甾醇、熊果酸、金圣草黄素、木犀草素、咖啡酸、胡萝卜苷、金圣草黄素-7-O--βD-葡萄糖苷、木犀草素-7-O--βD-葡萄糖苷、蒙花苷、芦丁、硝酸钾。

To study the bioactive components from water soluble extract of the Chinese eaglewood, various column chromatography of Chinese eaglewood led to the isolation of ten compounds. Their structures were elucidated as 2,3-bis(3-hydroxyphenyl)- propan-1-ol (1), [(2R,3R)-3-(4-amino-3,5-dimethoxyphenyl)oxiran-2-yl]methanol (2), 8-chloro-4'- methoxy-5,6,7,3'-tetrahydroxy-2-(2-phenethyl)-5,6,7,8-tetrahydrochromone (3), 4'-methoxy-5,6,7,3'-tetrahydroxy-2--5,6,7,8-tetrahydrochromone (4), the isomer of 4 (5), 4'-methoxy-5,6,7,8-tetrahydroxy-2-(3'-hydroxyphenethyl)-5,6,7,8- tetrahydrochromenone (6), 4'-methoxyisoagarotetrol (7), 6-hydroxy-2-(2-hydroxy-2- phenethyl)-chromone (8), 6-hydroxy-2-(2-phenethyl)-chromone (9), 6-hydroxy-2-(4'- hydroxy-2-phenethyl)-chromone (10), and Guaiacylacetone (11) by means of spectral analysis and comparison with references.

为了进一步发现沉香中具有生理活性的化学成分,本文对国产沉香的水溶性成分进行了研究,从中分离得到11个化合物,通过红外、紫外、质谱、核磁共振(1H-NMR, 13C-NMR, COSY, HSQC, HMBC, ROESY)波谱解析,分别鉴定为:2,3-二(3-羟基苯基)-丙-1-醇(1),[(2R,3R)-3-(4-氨基-3,5-二甲氧苯基)-2-氧化烯基]甲醇(2),8-氯-4'-甲氧基-5,6,7,3'-四羟基-2-(2-苯乙基)-5,6,7,8-四氢色原酮(3),4'-甲氧基-5,6,7,3'-四羟基-2-(2-苯乙基)-5,6,7,8-四氢色原酮(4),化合物3的差向异构体(5),4'-甲氧基-5,6,7,8-四羟基-2-(3'-羟基-2-苯乙基)-5,6,7,8-四氢色原酮(6),4'-甲氧基异沉香四醇(7),6-羟基-2-(2-羟基-2-苯乙基)色原酮(8),6-羟基-2-(2-苯乙基)色原酮(9),6-羟基-2-(4'-羟基-2-苯乙基)色原酮(10)和Guaiacylacetone (11)。

At the last of this chapter, based on the above research significance and research actuality,an original solution,on the other hand,my own research content is presented and the creationary point in my research content is briefly elucidated.

最后根据以上的研究意义和研究现状,提出了自己的解决方案,也就是自己的研究内容,并粗略阐述了自己研究内容当中的创新点。

Two oleanane type triterpenes were isolated from the crude drug Lu Lu Tong , the fruits of Liquidambar formosana and their structures were elucidated as 2α,3β dihydroxy 23 norolean 4(24), 12(13) dien 28 oic acid(1), 2α,3β,23 trihydroxyolean 12(13) en 28 oic acid(2), based on 13 C NMR, DEPT, 1H NMR, 1H 1H COSY, 13 C 1H COSY, IR, MS and elemental analysis.

从生药路路通分离得到2个齐墩果烷骨架的五环三萜类化合物。通过13CNMR,DEPT,1HNMR,2D1H-13CCOSY,2D1H-1HCOSY,IR,MS和元素分析阐明了它们的结构。(1)为2α,3β-二羟基-23-去甲-齐墩果-4(24),12(13)-二烯-28-羧酸,(2)为2α,3β,23-三羟基齐墩果-12(13)-烯-28-羧酸,(1)未见文献报道,(2)是首次从这一植物中分离得

Some isoforms were detected in the serotonin dimeric sprcies The structure of these isoforms need to be elucidated in the future. In conclusion, the dimeric species of serotonin is strongly related to pigment on rice.

目前的研究结果无法确定二聚体的结构,但由结果显示二聚体的含量似乎与水稻外壳的色素变化相关,因此推测 serotonin 二聚体极有可能改变水稻外壳色素。

The corrosion circumstance and corrosion mechanism form the tip of distillatory tower were elucidated,and efficacious countermeasure were introduced.

本文对独山子石化公司炼油厂加工哈国进口原油蒸馏造成蒸馏装置常压塔顶的腐蚀问题进行论述,阐明了蒸馏装置常压塔顶腐蚀环境及腐蚀机理,介绍了所制定的有效的防护措施。

Twenty compounds have been isolated and structure-elucidated, ten of which were new compounds including one new skeleton diterpene malloapeltin A, 5 cembrene-type diterpenes, two dolabradane-type diterpenoids, one triterpene ester malloapeltin B and one coumarinolignoid compound 5'-demethyl aquillochin.

其中有10个是新化合物,包括一个新骨架的二萜,五个枯烯类的二萜,两个罗柏烷型的二萜,一个三萜的对苯二甲酸酯和一个香豆素木脂体类化合物。

The organoboron compounds in this paper are based on triarylboranes, boronic acids and boronic esters. The structure-property relationship and sensing mechanism are elucidated. Organoboron compounds as Lewis acid can be used as fluoride probe with high sensitivity and selectivity because they have a unique LUMO in which the π-conjugation is divergently extended through the vacant p-orbital of the boron atom. The complexation of the boron π-electron systems with fluoride ion would interrupt the π-conjugation extended through the boron atom, causing the change of photophysical properties.

介绍了基于三芳基硼化合物、硼酸和硼酸酯的有机硼化合物在氟离子检测中的应用,评述了这些化合物的结构和检测性能之间的关系,讨论了检测机理,即有机硼化合物中硼原子空的p轨道使其作为路易斯酸能够选择性地结合氟离子,硼原子与氟离子的结合破坏了硼中心与芳香取代基的p-π共轭,引起有机硼化合物光物理性质的变化,从而实现对氟离子的高选择性检测。

The mechanism in which trehalose is produced from dextrin or starch hydrolyzate by endocellular enzymes of bacterium D-97 can be elucidated by high performance liquid chromatography with differential refraction detection basically, including the effect of the different carbon sources on the endocellular trehalose-producing enzymes in bacterium D-97 and the possibility or ability of the endocellular enzymes to produce trehalose using maltooligosaccharides of different chain lengths.

通过高效液相色谱/示差折光检测系统分析可获得细菌D-97利用糊精或淀粉水解物合成海藻糖的基本生物学信息,包括微生物培养碳源对细菌D-97胞内海藻糖合成酶系的影响以及该酶系利用不同种类或不同分子链长度的麦芽寡糖合成海藻糖的能力及作用过程。

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Chrysanthemum of 10 thousand birthday is lax to edaphic requirement, with the arenaceous qualitative loam with fecund, good drainage had better.

万寿菊对土壤要求不严,以肥沃。排水良好的砂质壤土为好。

He unstepped the mast and furled the sail and tied it.

他拔下桅杆,把帆卷起,系住。

Therefore, positively advances the interest rate marketability reform is one of current our country finance reform important tasks.

因此,积极推进利率市场化改革是当前我国金融改革的重要任务之一。