查询词典 elemental analysis

Its structure was characterized by elemental analysis, Fourier transform infrared spectroscopy and thermal analysis.

采用元素分析、红外光谱和热分析对该固定相结构进行了表征。

[Cu2(H2O)4]2 was prepared by the reaction of aqueous 1,2,4-triazol-5-one solution with the solution of copper picrate Cu2 and characterized by elemental analysis, FT IR and X-ray powder diffraction analysis.

本文通过1，2，4-三唑-5-酮水溶液与苦味酸铜水溶液反应，制备了[Cu2(H2O)4]2，用元素分析、傅立叶变换红外光谱分析、X-射线粉末衍射分析对其结构进行了表征。

Methods Elemental analysis, IR spectrum and X-ray diffraction analysis were used to describe the composition.

采用化学分析、红外光谱分析和X-射线粉末衍射分析等手段。

The copper atom is in a planar coordination site of [N_2O_2] and it devites from the mean plane by only 0.80 pm. Byπ-πstacking interactions, a alabastrine structure was obtained.(2)Schiff-base complex [Cu(H_2O)]·H_2O, where H3GS is the 3-carboxyl -salicylidene glycine, was synthesized and characterized by elemental analysis, IR spectra and single-crystal analysis. The crystal belongs to monoclinic system, space group P2(1)/c, a=848.46(3)pm, b=681.54(3)pm, c=1967.16(8)pm,β=95.8210(10)°, Z=4, R_1=0.0279, wR_2=0.0724. The copper atom is in a square-pyramidal field with the base

结果表明该晶系属单斜晶系，空间群P2(1)/c，晶胞参数：a=848.46(3)pm，b=681.54(3)pm，c=1967.16(8)pm，α=90°，β=95.8210(10)°，γ=90°，Z=4，R_1=0.0279，wR_2=0.0724，Cu原子位于轻微变形的四方锥场底心，底面被氮原子、酚氧原子、甘氨酸羧基的一个氧原子和一个水分子氧原子占据，而甘氨酸羧基的另一个氧原子占据相邻分子的锥顶，因而形成一维链状结构；合成了单核双聚配合物Na_2[Cu_2_2]·2H_2O ，铜三核配合物Cu_3_2·5H_2O和铜锌异三核配合物ZnCu_2_2·5H_2O，并用元素分析，IR光谱，电子光谱和磁化率测定对配合物的组

In this paper, the main work has been focused on the rare reported arsenomolybdates, and nine novel compounds have been synthesized. Sandwich arsenomolybdates:(NH_4)_(12)[Cr_2AsMo_7O_(27_2]·11H_2O (1)(NH_4)_(14)[Cu_2AsMo_7O_(27_2]·13H_2O (2) Double sandwich arsenomolybdates:(NH_4)_(12)Cu(H_2O)_4[As_2Fe_6Mo_(22)O_(85)(H_2O)]·19H_2O (3)(NH_4)_(15)[As_2CoFe_5Mo_(22)O_(85)(H_2O)]·16H_2O(4)(NH_4)_(14)Mn_(0.5)[As_2Fe_5MnMo_(22)O_(85)(H_2O)]·22H_2O(5) Cagelike arsenomolybdate:(NH_4)_(11)[AgAs_2Mo_(16)O_(54)]·9H_2O (6) Organic-inorganic molybdenum arsenate complexes:CuAs_6Mo_6O_(30{[Cu_4]_3[CuAs_6Mo_6O_(30)]}_2·6H_2O (7),[Cu_2]_3[As_3Mo_3O_(15)]_2·2H_2O (8)(NH_4)_(10){Cu(H_2O)_4}[AsMo_6O_(21)(O_2CCH_3)_3]_2·12H_2O (9)All of the above polyoxomolybdates were characterized by IR spectroscopy, TG-DSC, elemental analysis, and single-crystal X-ray analysis to identify their structures and chemical compositions.

本文选择目前报道尚少的砷钼杂多化合物为研究重点，合成了不同结构类型的九个新的杂多化合物：单夹心化合物：(NH_4)_(12)[Cr_2AsMo_7O_(27_2]·11H_2O(1)(NH_4)_(14)[Cu_2AsMo-7O_(27_2]·13H_2O(2)双夹心化合物：(NH_4)_(12)Cu(H_2O)_4[As_2Fe_6Mo_(22)O_(85)(H_2O)]·19H_2O(3)(NH_4)_(15)[As_2CoFe_5Mo_(22)O_(85)(H_2O)]·16H_2O(4)(NH_4)_(14)Mn_(0.5)[As_2Fe_5MnMo_22_O_(85(来源：AbcccBC论文网www.abclunwen.comH_2O]·22H_2O(5)笼状结构化合物：(NH_4)_(11)[AgAs_2Mo_(15)O_(54)]·9H_2O(6)有机配体修饰的化合物：CuAs_6Mo_6O_(30{[Cu_4]_3[CuAs_6Mo_6O_(30)]}_2·6H_2O(7) [Cu_2]_3[As_3Mo_3O_(15)]_2·2H_2O(8)(NH_4)_(10){Cu(H_2O)_4}[AsMo_6O_(21)(O_2CCH_3)_3]_2·12H_2O(9)对上述新化合物进行了瓜光谱分析、元素分析、热分析和X-射线单晶衍射测试，确定了它们的组成和结构，对部分化合物还进行了UV-vis及荧光光谱分析和循环伏安表征。

The structure was characterized by elemental analysis and IR spectroscopy as well as thermal gravimetric analysis.

对该配位聚合物进行元素分析、红外光谱表征、热重分析和X-射线单晶衍射测定。

Then mensurate their physical property and do elemental analysis ,infrared spectrum analysis to them .

依次测定了它们的物理性质，元素分析及红外光谱数据，并通过波谱数据表征了它们各自的构象，证实其确为目标产物，从而验证了此合成路线的可行性和可靠性。

This thesis investigated the influence of the structure of LHTO on thermalcracking reaction by using elemental analysis,NMR,GPC,Quinoline-lnsolubles analysis and micropolariscope .

本文利用元素分析、核磁共振波谱分析、相对分子质量分布分析、喹啉不溶物分析和偏光显微镜测试等试验方法研究了辽河稠油的组成结构特点对热转化反应过程的影响。

This could be a fascinating method for the practical syntheses of chiral synthons as valuable building blocks and important medicinal intermediates.3.Series of novel optical pureγ-aryl-1H-1,2,4-triazole derivatives were designed and synthesized by using the chiral auxiliary(Oppolzer\'s sultam),and all these target compounds were structurally characterized by ~1H NMR,~(13)C NMR,MS and elemental analysis,at the same time,some representative compounds have been elucidated by X-ray diffraction analysis.

应用手性辅剂樟脑磺内酰胺的手性诱导作用，设计合成了一系列光学纯的γ-芳基-1H-1，2，4-三唑类衍生物，所有目标化合物都采用了~1H NMR、~(13)C NMR、MS和元素分析进行了结构表征，同时也获得了部分代表性化合物的晶体结构，进一步确证了化合物的结构。

Their molecular compositions and structures were characterized by means of elemental analysis, EDTA titrimetric method, conductivity determination, FT-IR and UV spectroscopies; their thermal properties were studied by thermal analysis instrument.

通过红外光谱分析、紫外光谱分析、元素分析、EDTA配位滴定分析以及电导率的测定对铕三元荧光配合物的组成及结构进行表征。

Must have Coordination and negotiation skill, flexible ideas, and be punctilious person.

必须具备较好的协调与谈判能力，头脑灵活，工作认真仔细

Result: 18 patients are all with simple eye.The pigment mole lies in nasal and temple sides of the ball conjunctiva,in which 2 lie in lacrimal caruncle and semilunar plica.

结果：18例患者均为单眼，色素痣大多数位于内外侧睑裂部球结膜面，2例位于泪阜及半月皱襞，经激光治疗后，10例色素痣消失，有5例行再次激光后消失，2例行第三次激光后消失，1例第四次激光后消失。