查询词典 elemental analysis

The main research contents are as follows:1. Through massive calculation, analysis and comparison, sum up the similarities and differences between the special-shaped cross sections and rectangular cross sections in mechanical features, between reinforced concrete special-shaped columns and rectangular columns in load-bearing capacity, ductility performance and provide necessary basic concepts and data for further understanding the characteristics of the special-shaped columns;2. Through massive elastic calculations and elasto-plastic analysis, under the preconditions of satisfying the code's requirements for axial compression ratio, limit value of lateral displacement and load-bearing capacity of normal section,oblique section and beam-column joint, under circumstances of different intensity of earthquake, structure dead weight, sort of site and column grid bay dimension, the variation regularity of maximum suitable height of structure, and thus sum up the maximum suitable height of structure for code for the purpose of macro-control while deciding the design scheme;3. Make a preliminary study on the stress feature of reinforced concrete special-shaped column and Z-shaped column of which the ratio of limb length to limb thickness is between 4~5 ,and the preliminary design method is suggested;4. Through elato-plastic time history dynamic analysis of typical projects, check up the weak storey of the special-shaped column structure and yielding, breaking and collapse mechanism to satisfy the earthquake resistant requirement to buildings of remaining stand under strong earthquake;5. Derive for project use simplified calculation formula of vibration period, suitable vibration period, suitable rigidity of special-shaped column structure through theoretical analysis, and provide an easy and practical method for deciding the structure scheme economically, safely and reasonably;6. Based on the study achievements in theory and massive analysis and calculations of this paper, sum up the regularities of inner force, deformation of special-shaped column structure and seismic conceptual design, and thus the suggection of seismic design of special-shaped column structures is presented.

本文研究的主要内容如下：通过大量的计算、分析和对比，总结出异形截面与矩形截面在力学特性、钢筋混凝土异形截面柱与矩形截面柱在承载能力、延性性能等方面的异同，为深入了解异形截面柱的特点提供必要的基本概念和数据；通过大量的弹性及弹塑性计算分析，在满足规程对轴压比、侧移限值及正截面、斜截面、节点承载力抗震验算要求的前提下，在不同抗震设防烈度、结构自重、场地类别及柱网开间尺寸情况下最大适宜高度的变化规律，并在此基础上总结归纳出异形柱结构的最大适用高度规定，可用于规程，以便于在确定方案时起到宏观控制的作用；对肢长与肢厚比在4～5的钢筋混凝土异形截面柱及Z形柱的受力特点进行初步探讨，提出初步的设计方法；通过对典型工程的弹塑性动力时程分析，检验异形柱结构的薄弱层及屈服、破坏、倒塌机制，以达到建筑物大震不倒的抗震设防要求；通过理论分析，推导出异形柱结构自振周期，以及适宜自振周期、适宜刚度的工程实用简化计算公式，为经济、安全、合理地确定结构方案提供简便实用的方法；在本文理论分析、计算以及大量的研究成果基础上，总结归纳出异形柱结构内力、变形的规律及抗震概念设计内容，并在此基础上提出异形柱结构的抗震设计建议。

Through the briefings and case analyses of Traditional Analysis, Hindemith Analysis, Schenkerian Analysis , Allen Forte Set Analysis, this thesis is to compare differences in the theoretical basis, analytical steps and analytical results of the above four mentioned harmony analysis.

本文通过对传统分析、申克分析、亨德米特分析、艾伦·福特集合分析中有关和声的分析方法的概要阐述与实例分析，比较这四种和声分析法的理论基础、分析步骤、分析结果等方面的差异。

Their structures were confirmed by elemental analysis, 1H NMR, and IR spectral data. The preliminary bioassay results showed that α-phenyl-sul-fonylcyclododecanone oxime 2,4-dichlorophenoxy acetate (8p) had inhibition ratio 100% and 80.07% against Digitaria sanguinalis Scop., and 100% and 88.70% against Abutilon theophrasti Medic. at concentrations of 100 and 1 mg/L.

初步生物活性测定结果显示，部分化合物具有一定的除草活性，如α-苯磺酰基环十二酮肟-2，4-二氯苯氧乙酸酯(8p)在浓度为100和1 mg/L时对马唐的抑制率分别为100%和80.07%；对苘麻的抑制率分别为100%和88.70%。

The structure of octadecyl acrylate were identified by elemental analysis, IR and (superscript 1)H NMR.

产物结构经元素分析，IR和(上标1)H NMR表徵。

Quantitative studies of UV absorption show that the content of acyl group is consistent very well with elemental analysis result.

通过UV吸收对产物中的酰基进行了定量，结果与元素分析结果基本一致。

The alkaline-earth metal complexes with mucic acid was successfully prepared via gel formation and characterized by elemental analysis,FT-IR measurements.

采用凝胶法合成了碱土金属—粘液酸配合物的晶体。

Novel chitosan derivative with long alky groups as the hydrophobic moieties and carboxymethyl groups as the hydrophilic moieties was synthesized. The chemical structure of N-octyl-O, N-carboxymethyl chitosan was characterized via FTIR, 1H NMR and elemental analysis. The physical properties were analyzed with wide angle X-ray diffraction and differential scanning calorimetry.

以天然可生物降解的壳聚糖为原料，通过在壳聚糖6位羟基上引入羧甲基，在2位氨基上引入疏水烷基链，制得N-辛基－O，N-羧甲基壳聚糖两亲性衍生物，分别用FTIR、1H NMR和元素分析等技术对其结构进行表征，用广角X射线衍射和差示扫描量热法对具物理性质进行分析，并考察其在各种溶剂中的溶解性能及其对难溶性药物的增溶能力。

A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3，3'-偶氮双(6-氨基-1，2，4，5-四嗪)新合成路线、采用3，5-双(3，5-二甲基吡唑-1-基)-1，2，4，5-四嗪为原料，由文献报道的4步反应缩减为2步，经高压氨解、高锰酸钾氧化合成了DAAT，总收率大幅提高，达到58.1%，并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

All these compounds were characterized by azeotrope and elemental analysis, as well as by spectral measurements.

对所制成的衍生物均采用了共沸混合物分析、元素分析和光谱测定等进行了表征。

Three new fluo-rine-containing nitro benzimidazole derivatives were synthesized in the presence of 4-dimethylaminepyridine andtheir structure and configuration were confirmed by elemental analysis, IR, and 1HNMR.

在碱性条件下由2-(4′-羟苯基)-5-取代苯并咪唑与氯乙酸作用得到5个新化合物取代苯并咪唑基苯氧乙酸。

The changes of the HAF after liver injury may be related to the volume of blood loss, the intraabdominal pressure and the pneumoperitoneum duration.

肝撞击伤伴失血后肝动脉血流量的变化与失血量、气腹压力以及气腹持续时间等有密切联系。

Reneging on our commitments to the world's poor cannot be an austerity measure, she said.

放弃我们给世界上的穷国的承诺不能成为一种紧缩措施。