查询词典 crystal diffraction

Themain contents of this dissertation are as follows:(1) The quality analytiedal results of chitosan are as follows: water for 15.205%;degree of deacetylation 92.671%; the weight average relative molecular weight ofchitosan 195900; the viscosity average relative molecular weight of chitosan 194100;and the decomposing temperature 298℃. The infrared ray IR spectra of chitosanshows that the feature-absorbing band of chitosan amido was 1601cm~(-1), that ofβ-indican bond was 986cm~(-1). The results of the X-ray diffraction of chitosan indicatesthat its degree of deacetylation and degree of crystal are both big.

本文的主要内容如下：(1)对壳聚糖的质量进行分析，其水份为15.205％，脱乙酰度为92.671％，重均分子量为195900，黏均分子量为194100，分解温度为298℃，壳聚糖的红外光谱表明，壳聚糖—NH_2的特征吸收峰为1601cm~(-1)，β-糖苷键的特征吸收峰为986cm~(-1)，壳聚糖的X-衍射图表明壳聚糖原料的脱乙酰度和结晶度均较大。

The grain size in the (101) diffraction direction is in inverse proportion to the crystal distortion.

并观察到（101）晶面上的畸变与晶粒度有着相反的变化趋势。

The molecular structure of this isomer has been determined by X-ray diffraction and it is the first time to report the crystal structure of this kind of isomer which was proposed erroneously in the literature.

采用X-射线衍射的方法测定了其中一个异构体的结构，这是对此类异构体单晶结构的首次报导，纠正了文献中存在的对此类化合物结构的错误认识。

Using 1,3-dicyanobenzene as a precursor, we have obtained two coordination polymer of rare earth metal bridged by isophthalato ligand, Eu complex (4) and Sm complexe coordinated (5). X-ray single crystal diffraction investigation confirms that complex 4 and 5 are isomorphous with near isostructural 〓 unit.

以1，3-苯二氰为前体，合成了两个新的稀土金属与间苯二甲酸根配体桥联的聚合物：间苯二甲酸根配体配合的铕和钐化合物，4和5.X-射线衍射结构分析表明化合物4和5均具有〓基本结构单元且两者结构类似。

Crystal structure was determined by powder X-ray Diffraction and lattice parameters as a function of Sr-concentration x were obtained by using Rietveld method.

在80K-300K温度范围的直流电阻率测量表明，材料的电性质在x=0.2和0.3之间展示了从半导体到金属的相变。x=0.2样品已接近绝缘体-金属相变的边缘。

The composites were tested by X-Ray Diffraction, Scanning Electron Microscopy, Thermal Expansion Coefficient and flexural strength. In these ways, the synthesization of leucite crystal and the preparation of Zro2-KAlSi2O6 Ceramic powder are systemically investigated.

本研究以钾长石、纳米氧化锆和碳酸钾为原料，采用固相反应合成氧化锆-白榴石基烤瓷粉，借助XRD、SEM、TEC和弯曲强度等分析测试方法，对白榴石晶体的合成及氧化锆-白榴石基烤瓷粉的制备进行了较为系统的研究。

The composition, crystal shape, morphology, magnetic characteristic and thermal stability of the samples were characterized by powder X-ray diffraction, transmission electron microscopy, scanning electron microscopy, vibrating sample magnetometry and thermogravimetric analysis, respectively.

张佳 大连理工大学材料科学与工程学院，大连 116085刘顺华大连理工大学材料科学与工程学院，大连 116085冀志江中国建筑材料科学研究总院，北京 100024采用水热合成法，以(NH4)2S2O8作氧化剂，以MnSO4·H2O为锰源，制备了自生核壳结构MnO2粉体。

The crystal structure was perovskite-like type, as evidenced by the results of X-ray diffraction and scanning electron micrography. The distribution of K4Nb6O17 powder with particle size of less than 10 m, which would become larger as the calcining temperature grew.

通过XRD和SEM对样品进行表征，发现该法合成的K_4Nb_6O_(17)均具有钙钛矿结构，样品的颗粒大小分布不均，但大多小于10μm，且合成的温度越高，颗粒粒径越大。

According to the different orientations of domain walls with respect to the (100) observation plane of a foil, 90°domain boundaries may be divided into two kinds. one is thin lens or ring shaped a-a 90°domain boundary, and the domain wall lies on the {110} plane; Usually, most of these domain boundaries are uncharged; according to the extinction rules for the (011) domain walls, the displacement vector 〓 along 〓 can be dertermined, which is parallel to the line of intersection between the domain wall and the plane consisting of spontaneous polarization vectors on both sides of domain boundary; from selected area electon diffraction of crystals including domain boundary, we not only examine slight difference in the crystal parts on both sides of the domain boundary, but also obtain crystallographic relationship between them, that is, there exists a 180°rotation symmetry operator along a normal of domain wall. The other is Z or ring shaped a-c 90°domain boundary along {010} direction, and the displacement vector 〓 runs along 〓 direction.

根据界面相对于样品中(100)观测面取向的不同，90°畴可分为两类：一类为薄透镜片状或环状的a-a90°畴，其界面平行于{110}，多数不带电，由消光规律可确定其位移矢量平行于畴界面与自发极化所在平面的交迹，即，〓方向，而从包含畴界的选区电子衍射图可知，这种不带电的90°畴界两侧存在微小的取向差，其界面两侧的结晶学关系为以界面法线为二次轴的旋转关系；另一类为Z状或环状的a-c90°畴，其界面平行于[010]或[001]，相应的位移矢量为〓方向。

It was found that the Schorl or dravite in schorl-dravite group that is produced from pegmatite and has good crystal degree had a strong intensity of spontaneous polarity by electron-beam bombardment and X-ray diffraction of varying the temperature.

利用电子束轰击结合变温XRD分析发现在Schorl-dravite系列电气石中，产于伟晶岩的，结晶度比较高的Mg电气石或Fe电气石具有较高的自发极化强度。

After explaining total design of automated test system for microcircuit , the thesis introduces GPIB standard .

文章在说明了微电路模块自动测试系统的总体设计后，对GPIB标准进行了介绍。

He interceded in my behalf.

他替我说情。