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These coatings have been characterized by the state-of-the-art techniques of XRD, nano-indentation, scratch test, SEM, RBS, etc. As the result, it was found that TiN coatings prepared by -100V DC bias are characterized with the (111) preferred orientation and the coatings prepared by pulsed bias with (111),(200) and (220) hybrid orientations.

通过XRD、纳米压痕仪、划痕仪以及SEM、RBS等手段对薄膜的结构和性能进行了测量和分析,结果发现,-100V直流偏压下TiN薄膜有明显的(111)晶面择优取向,而脉冲偏压条件下TiN薄膜为(111)、(200)、(220)混合晶体取向。

This thesis includes five parts as follows.1. The backgrounds and some relative concepts of this work are briefly introduced. The photochemistry of benzamides and compounds with thiourea functional group is also concisely reviewed.2. Total of fourteen benzamides with different substituted groups have been synthesized and structurally characterized. Better photoreaction time for that kind of compounds at given concentrations is confirmed by tracking its'UV spectrum and GC chromatogram. A representative dibenzophenone photoproduct has been determined by X-ray crystallography. The mechanisms of photoreaction of benzamide have been proposed.3. Total of seven N-chloro(phenylmethylenebenzenamines with different substituted groups and sixty-one thiourea derivatives have been synthesized and structurally characterized.

论文的主要内容如下:1、简要介绍本论文工作的研究背景,并对苯甲酰胺和具有硫脲官能团类化合物的光化学研究进展进行简要的总结。2、合成与表征了14个具有不同取代基的苯甲酰胺类化合物,利用紫外光谱和气相色谱确定了此类化合物较佳光照时间,测定了一个具有代表性光解产物的单晶结构,提出了苯甲酰胺类化合物的光反应机理。3、合成与表征了7个带有不同取代基的氯代苯甲酰亚胺中间体及61个硫脲衍生物,测定了两个具有代表性化合物的单晶结构。

Trisodium salt of N,N,N'-ethylenediamine triacetic acid was prepared by hydrolyzing 2-oxo-1, 4-piperazine diacetic acid(3-KP) in the strong base solution. Then it was combined with lauroyl chloride, hexadecanoyl chloride and benzoyl chloride respectively. N-lauroyl-ED3A and N-hexadecanoyl-ED3A were prepared in succsess. The molecular structure of N-lauroyl-ED3A was characterized by ~1HNMR and ~(13)CNMR. The molecular structure of N-hexadecanoyl-ED3A was characterized by 1HNMR.

将3-KP 在强碱性条件下水解,生成ED3ANa3 的水溶液,然后分别与月桂酰氯、棕榈酰氯和苯甲酰氯反应,成功制得N—月桂酰基ED3A 和N—棕榈酰基ED3A,并用~1HNMR 和~(13)CNMR 对N—月桂酰基ED3A 的分子结构进行了表征,用1HNMR 对N—棕榈酰基ED3A 的分子结构进行了表征。

Negative Ce anomaly is one of diagnostic criteria of geotectonic setting of silicalite. Silicalite in Golug, Xinrenlang and Lhazê in the Gangdisê tectonic belt is characterized by unclear negative Ce anomaly characteristic of epicontinental or neritic sediment, while silicalite in Gyüzê La-Jiaqing area is characterized by weak negative Ce anomaly characteristic of sediment in transitional belt between oceanic basin and continental margin.

硅质岩Ce异常特征是构造背景判别的最有效的手段之一,冈底斯构造带谷露、新认朗与拉孜地区的硅质岩Ce负异常不明显,属大陆边缘或浅海环境,而九子拉家青地区的硅质岩具弱的Ce负异常,属大洋盆地与大陆边缘之间的过渡环境中的沉积。

Aggressive students are characterized with high Psychosis scores and relatively extroversive, and bullied students are characterized with high Neurosis score and more introversive.

攻击类学生在个性特征上以高精神质和相对外倾型为典型特征,受害类学生以高神经质和内倾型为典型特征。

The hybrid composite PW11Co/PAMAM was characterized by FT-IR, UV-Vis diffuse reflectance spectra, XPS, XRD and TG/DTA, indicating that the PW11Co was chemically anchored to PAMAM. The morphologies of the title composite were characterized by scanning electron microscopy and transmission electron microscopy. The catalytic activity was evaluated by oxidation of isobutyraldehyde to isobutyric acid in MeCN under mild conditions (20 ℃, ambient pressure), showing that the title compound is a more effective and recoverable catalyst than corresponding PW11Co.

通过FT-IR、DR-UV-Vis、XRD、TEM、SEM、TG/DTA等手段对其进行了表征,并考察了其对异丁醛转化异丁酸的催化活性,实验结果表明,多金属氧酸盐通过配位键与聚酰胺-胺作用形成的无机-有机复合物可望成为一种催化活性高且易于分离和重复使用的多相催化剂。

Based upon the ecoanatomical method, leaf anatomical characters of eleven populations of six evergreen species (Cyclobalanopsis glauca, C. myrsinaefolia, C. gracilis, Castanopsis sclerophylla, C. eyrei and Lithocarpus glaber) from the eastern subtropical area of China were analyzed and compared with SPSS, DCA and TWINSPAN. The results are: 1. Although the leaf structures of the eleven populations still belong to the mesophyll type, they all express the trend of xerophilization. 2. There are some differences in leaf anatomical characters among populations, species and genera, which occur as the results of their adaptation to different habitats. 3. Different leaf anatomical characters have different variations among populations, species and genera, of which leaf thickness and palisade tissue thickness (considered as ecological adaptation characters) have greater variation than sponge tissue thickness, lower cuticle thickness and lower epidermis thickness (as systematical evolution characters). 4. The leaves of C. sclerophylla and C. glauca with thicker lamina, palisade tissue and cuticle (a multilayered upper epidermis in C. sclerophylla) are thought to better adapt to their dry habitat. The leaves of C. eyrei with thicker sponge tissue, although characterized by a multlayered upper epidermis, adapt to their humid and warm habitat. The leaves of C. myrsinaefolia and C. gracilis characterized by a thinner lamina, a less palisade tissue and a moderate cuticle thickness adapt to the humid and cool habitat in a middle mountain.

选取亚热带东部替代分布明显的壳斗科6种常绿树种(青冈、小叶青冈、细叶青冈、苦槠、甜槠和石栎)的11个种群叶片进行生态解剖,并用SPSS, DCA和TWINSPAN比较分析,结果表明:①尽管6种11个种群叶的结构仍属中生叶型,但有着不同程度的趋旱适应;②叶的解剖性状在属间、种间和种群间均存在着不同程度的差异,这是它们适应各自生境的结果,青冈和石栎的种内差异较大,反映出它们对环境变化有较强响应能力;③叶片的不同解剖性状在属、种类和种群间的变化并不同步,其中叶片和栅栏组织厚度等性状差异突出,反映它们更易受环境的饰变,是生态适应性状,而海绵组织、下角质膜,特别是下表皮厚度等性状差异较小,显示出这些性状的稳定性,可以认为是系统演化性状;④苦槠、青冈具有较厚的叶片、栅栏组织、角质膜和发达输导和机械组织,苦槠还具有复表皮,表现出对旱化生境的适应;甜槠尽管具有复表皮和较厚的叶片,但这是海绵组织增厚的结果,是对中生生境的适应;小叶青冈和细叶青冈具有较薄的叶片和栅栏组织、角质膜厚度居中等特点,可能是对中山凉湿生境的适应。

On the basis of our series and the findings of Yapar et al, the sonographic features of pelvic TB may be categorized as wet type or dry type as follows. The wet type, found in 12 (75%) of 16 patients, is characterized by incompletely septated ascites, particulate ascites, loculated fluid (although clear ascites can also be commonly associated with tuberculous peritonitis ), a thickened peritoneum or omentum, and an adnexal mass, mimicking ovarian cancer; the dry type, found in a small number of cases, is characterized primarily by adnexal masses, adhesions, and loculated fluid, mimicking tubo-ovarian abscesses or complexes.

根据咱们和Yapar等人的发明,骨盆内部空腔TB的超声特征可以分为湿型或干型。16例病人中发明12例湿型TB,其特点是水臌内存在不完全的分隔、光点和多房性积液(尽管清亮的水臌通常也能归并结石性腹膜炎),和腹膜或网膜增厚和容易误诊成卵巢癌的附件团块;少量的病例呈干型TB,其特点主要是附件团块、粘连和多房性积液,象是输卵管-卵巢脓肿或复合体。

On the basis of our series and the findings of Yapar et al, the sonographic features of pelvic TB may be categorized as wet type or dry type as follows. The wet type, found in 12 (75%) of 16 patients, is characterized by incompletely septated ascites, particulate ascites, loculated fluid (although clear ascites can also be commonly associated with tuberculous peritonitis ), a thickened peritoneum or omentum, and an adnexal mass, mimicking ovarian cancer; the dry type, found in a small number of cases, is characterized primarily by adnexal masses, adhesions, and loculated fluid, mimicking tubo-ovarian abscesses or complexes.

根据我们和Yapar等人的发现,盆腔TB的超声特征可以分为湿型或干型。16例病人中发现12例湿型TB,其特点是腹水内存在不完全的分隔、光点和多房性积液(尽管清亮的腹水通常也能合并结核性腹膜炎),以及腹膜或网膜增厚和容易误诊成卵巢癌的附件团块;少量的病例呈干型TB,其特点主要是附件团块、粘连和多房性积液,象是输卵管-卵巢脓肿或复合体。

On the basis of our series and the findings of Yapar et al, the sonographic features of pelic TB may be categorized as wet type or dry type as follows. The wet type, found in 12 (75%) of 16 patients, is characterized by incompletely septated ascites, particulate ascites, loculated fluid (although clear ascites can also be commonly associated with tuberculous peritonitis ), a thickened peritoneum or omentum, and an adnexal mass, mimicking oarian cancer; the dry type, found in a small number of cases, is characterized primarily by adnexal masses, adhesions, and loculated fluid, mimicking tubo-oarian abscesses or complexes.

根据我们和Yapar等人的发现,盆腔TB的超声特征可以分为湿型或干型。16例病人中发现12例湿型TB,其特点是腹水内存在不完全的分隔、光点和多房性积液(尽管清亮的腹水通常也能合并结核性腹膜炎),以及腹膜或网膜增厚和容易误诊成卵巢癌的附件团块;少量的病例呈干型TB,其特点主要是附件团块、粘连和多房性积液,象是输卵管-卵巢脓肿或复合体。

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Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克,果实色泽鲜艳,汁多味浓,甜酸适口,离核仁甜,清末时就驰名陕、甘两省,清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异:红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感,ED90值分别为47.65、71.67和29.17g/hm2;春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感,ED90值分别为96.91、114.20g/hm2;而番茄不敏感。

However, I have an idea.

不过,我有个主意。