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The results indicate that the optimized sulfonylation reaction time is 4 h, the materiel rate of chlorosulfonic acid and 2-chloroimidazo[1,2-α]pyridine is 1.2 : 1, with ethylamine the yield increasing from 15.4% to above 70%; the optimized ammonolysis reaction time is 3 h and the reaction temperature is 27℃, with the acetonitrile yield increasing from 60.1% to above 79.6%.
实验结果表明，磺酰化反应的最佳反应时间为4 h，氯磺酸与2-氯咪唑并[1，-α]吡啶的用量比为1.2：1，加入三乙胺可将收率由15.4%提高到70%以上；氨解反应的最佳反应时间为3 h，反应温度为27 ℃，加入乙腈可将收率由60.1%提高到79.6%；方案经改进后，总反应时间缩短3 h，收率提高了5.5%。
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Effects on the reaction of factors such as reactant ratio, reaction time, and reaction temperature were investigated, and optimum reaction conditions were determined as follows: mole ratio of cyanuric chloride to ethylamine to sodium hydroxide to sodium methyl mercaptide was 1:2.1:2.0:1.7, and the temperature and time of the first, second, and third substitution reactions were -2, 0, and 82℃ and 30, 60, and 180 min, respectively.
讨论了原料配比、反应时间和反应温度等因素对反应的影响，获得了较佳的反应条件。较佳反应条件为三聚氯氰：乙胺：氢氧化钠：甲硫醇钠＝l：2.1：2.0：1.7，第一、第二、第三取代反应的反应温度和反应时间分别为-2℃、0℃、82℃和30、60、180min。
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Impact sequence from big order followed by ratio of oil and extractant,reaction time and temperature.
在双氧水体系中，以HPA-2为催化剂，考察了反应时间、反应温度以及剂油比对脱硫率的影响，实验结果表明，剂油比对脱硫率的影响最大，剂油比越大脱硫效果越好；反应时间的影响次之，脱硫率随着反应时间的延长而提高，在60min左右脱硫反应基本完成；随着反应温度的升高，脱硫率也提高。
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The main content of this paper as follows: The acidic strength, reaction temperature, reaction time of Chlorine-aluminate Ionic Liquids with different structure of cation on the activity of transalkylation of MN with TeMB and the selectivity of 2,6-DMN were studied. The optimum reaction condition was obtained: the molar fraction of AlCl_3 is 0.71, molar ratio of 2-MN and TeMB is 1, the amount of ionic liquid is 32wt%, reaction temperature is 20℃and reaction time is 8h using X-xAlCl_3 and X-xAlCl_3 as catalysts; the optimum reaction time is shortened 6h using Et_3NHCl-xAlCl_3 as catalyst.
本文主要研究了以下内容：分别考察了不同阳离子结构的氯铝酸盐类离子液体的酸强度、反应温度、反应时间等因素对MN和TeMB转移烷基化的催化反应活性和2，6-DMN选择性的影响，优化得到适宜的反应条件为：以X-xAlCl_3和X-xAlCl_3为催化剂时，AlCl_3的摩尔分数x=0.71，2-MN和TeMB摩尔比为1∶1，离子液体用量为32wt％，反应温度为20℃，反应时间为8h；以Et_3NHCl-xAlCl_3为催化剂时，反应时间缩短到6h。
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In the first part, it was investigated the interaction between Pb2+ and La4Ti9O24 ceramic bulk. The result shows that a significant Pb2+ diffusion into La4Ti9O24 ceramic bulk and a significant crystallization of the La2/3TiO3-type phase is clearly observed in the Pb2+ diffusion layer. The reacted zone consists of the La2/3TiO3-type phase exhibits the linear dependence of the square of the thickness, x, on the heat-treated time, t, in excellent agreement with the parabolic law x2 = kt, where k is the growth rate coefficient. The kinetic study thus indicates that the Pb2+/La4Ti9O24 interaction strictly obeys the theory of the reactive diffusion. Furthermore, the experimental k values were used to determine the associated activation energy, Ea, for the formation of La2/3TiO3-type phase using the Arrhenius plot and the following least-square equation, ln =-Ea/RT + A, where T is the annealing temperature, R is the universal gas constant, and A is a constant, resulting in Ea ~ 607 ?b 60 kJ/mol.
首先， 以巨观的方式观察PbO与La4Ti9O24陶瓷体介面的反应现象；利用X-ray绕射分析以及扫描式电子显微镜来观察不同的热处理温度以及不同的持温时间所制作的样品，研究结果发现， Pb2+离子会渗入到La4Ti9O24陶瓷内，同时在Pb2+离子所渗入的区域内会产生新的La2/3TiO3-type钙钛矿斜方晶相；藉由量测不同温度与时间之样品，其因Pb2+离子渗入而产生之La2/3TiO3-type相层厚度之关系，符合反应式扩散机制中 x2 = kt 之关系式(其中 x：扩散层厚度； k：反应速率常数； t：反应时间)；进一步将不同实验条件所得到之反应速率常数值代入Arrhenius方程式ln (k =-Ea/RT + A ，其中Ea：活化能； T：绝对温度； R：气体反应常数； A：常数，可以求得Pb2+离子与La4Ti9O24陶瓷发生反应式扩散所需之活化能为607 ± 60 kJ/mol。
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The study of treating dye wastewater with iron scraps and fly ash for electrochemistry principle;2. A study of the reaction on the treatment for blick G dye wastewater using iron scrapshas been carried on by the authors.
研究了废铁屑处理黑G染料水样的反应过程及处理效果：反应介质的pH值和反应停留时间为影响反应效果的两个主要因素，pH值越小，反应时间越长，处理效果越好；停留时间在4～10min，反应过程已基本完成；色度去除率为92％～98％，CODcr的去除率为40％～75％。
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To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.
采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。
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The epoxide-terminated oligomer having ether mesogenic unit wassynthesized for the first time by reacting the diphenol with epichlorohydrin. Theepoxy equivalent increased as the elongation of reaction time or the decrease of theinitial ratio of diphenol and epichlorohydrin, but effect of the reaction time wassmaller than that of the initial ratio.
首次采用直接环氧化的方法合成了含酯类液晶基元的环氧结构预聚物，环氧化反应中反应配比和反应时间会影响产物的环氧当量；缩小反应配比或延长反应时间会使产物的环氧当量增大，反应时间对产物环氧当量的影响较小。5。
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The results show that:First, concentration of hydrogen peroxide have the most obvious influence to oil yield and carbon black yield,with the increase of concentration of hydrogen peroxide the oil yield first increase then decrease,when concentration of hydrogen peroxide is 8.19% or so,the oil yield reach to the biggest value, and with the increase of concentration of hydrogen peroxide carbon black yield decrese;Then,reaction time have more obvious influence to oil yield and carbon black yield,oil yield increase but carbon black yield decrease with the increase of reaction time;Thirdly,reaction tempreture have some influence to oil yield and carbon black yield,samely,oil yield increase but carbon black yield decrease with the increase of reaction tempreture;Finally,reaction pressure does almost no influence on oil yield and carbon black yield.
研究结果表明：过氧化氢质量浓度对产油率和炭黑产率的影响最为显著，产油率随过氧化氢质量浓度的提高先提高后降低，在过氧化氢质量浓度为8.19%左右时达到最大值，炭黑产率随过氧化氢质量浓度的提高而降低；反应时间对产油率和炭黑产率的影响也比较显著，产油率随反应时间的增加而提高，炭黑产率随反应时间的增加而降低；反应温度对产油率和炭黑产率也有一定的影响，产油率随反应温度的提高而相应地提高，炭黑产率随反应温度的提高而降低；在本文实验范围内，反应压力对产油率和炭黑产率基本上没有影响。
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By esterification, saponification, doubledecomposition and formulation, liquid rare earth of monoisooctyl phthalate complex heat stabilizer was prepared with phthalic anhydride, isooctyl alcohol, sodium hydrate, rare earth chloride, mixed solvent and other reagents. The optimum conditions are: the temperature of esterfication is 130～140℃,and the reaction time is 1h. The temperature and time of saponification is 60℃ and 10min respectively. The temperature of double decomposition is 60～70℃,and the reaction ti...
摘 要：以邻苯二甲酸酐、异辛醇、氢氧化钠、氯化稀土、混合溶剂、助剂为原料，通过酯化反应、皂化反应、复分解反应以及复配制备了以邻苯二甲酸单异辛酯稀土为主要成分的液态稀土复合热稳定剂，其工艺条件为：酯化反应的温度控制在 130～ 14 0℃，反应时间为 1h ；皂化反应的温度为 6 0℃，反应时间为 5min ；复分解反应的温度在 6 0～ 70℃，反应时间为 1h ；水洗温度控制在 6 0～ 6 5℃；混合溶剂的用量为 5 0 %，稀土含量为 6 0 3%；在复配过程中，采用亚磷酸酯作为辅助热稳定剂，其用量为 5 %～ 7%，PVC中加入 2 %的这种稀土复合热稳定剂，在185℃下，其热稳定时间为 4 5min。
- 更多网络解释与反应时间相关的网络解释 [注：此内容来源于网络，仅供参考]
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discrimination reaction time test：鉴别反应时间试验
频率分割(制) frequency division | 鉴别反应时间试验 discrimination reaction time test | 睡眠觉醒周期 sleep-activity cycle
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reaction time：反应时间
1.反应时间(Reaction Time) 指仪器的一个分析周期中,试剂和样品混合最末一点测定读数时间. 它对终点法尤其重要,是终点法的瓶颈. 有的仪器多个反应时间可选L如Hl-TACHI 7170),须预先选定. 多数仪器10分钟左右,这对试剂提出了较高要求.
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reaction time：制动反应时间
充分发出的平均减速度 mean fully developed braking deceleration (MFDD) | 制动反应时间 reaction time | 促动时间 actuating time
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simple reaction time：单纯反应时间
"单纯反应","simple reaction" | "单纯反应时间","simple reaction time" | "单体;单纯","simplex"
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response time：反应时间
信息:播出实时本公司经营42寸液晶电视(专业酒店用),质量保证,欢迎咨询洽谈. 42" 液晶电视详细说明 屏尺寸 (display size) 42" tft lcd 屏的供应商 (panel vender) 屏幕比例 (aspect ratio) 16:9 反应时间 (response time) 8ms
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transient response time：暂态反应时间
4.有效值杂讯 RMS Noise | 5.暂态反应时间 Transient Response Time | 6.暂态电压 Transient Spike
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falltime：下降时间
阿庆嫂:好你个刁德一,果然是刁钻的狠啊!这响应速度也称反应时间是液晶电视各像素点对输入信号反应的速度,即像素由暗转亮或由亮转暗所需要的时间. 一般将反应时间分为两个部分:上升时间(Risetime)和下降时间(Falltime),而表示时以两者之和为准.
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sensorial reactiontime：感觉的反应时间感觉的反应时间
sensorial area 感觉中枢 | sensorial reactiontime 感觉的反应时间感觉的反应时间 | sensorimetabolism 感觉性代谢
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sensorial reaction?time：感觉的反应时间感觉的反应时间
sensorial area 感觉中枢 | sensorial reaction?time 感觉的反应时间感觉的反应时间 | sensorimetabolism 感觉性代谢
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machine reaction time：计算器反应时间
machine program 机器程序 | machine reaction time 计算器反应时间 | machine ringing 自动振铃,机械振铃