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Ti-Si composite materials are mixed at atomic scale, and Ti-O-Si bond appears in all of the samples with different TiO2 content; the mixed oxides are mainly existed in the form of amorphous pattern, anatase appears when the TiO2 content is more than 80%, but compared with the intension of pure TiO2, it has not integrate structure. The acetic content has great influence in the specific area and crystal structure of the mixed oxides. 20TiSi has good heat stability, still possesses 11m2/g after calcined at 1100℃; calcinations on the large scale of temperature does not cause the break of Ti-O-Si bond, TiO2 is well dispersed in 20TiSi calcined at 1100℃, and it still existed in the form of amorphous.

结果表明：制得的Ti-Si复合氧化物具有很高的比表面积，在TiO_2含量为10％时达到681.5m~2／g，Ti原子进入Si-O四面体结构中，形成Si-O-Ti键，复合氧化物的稳定性好，当TiO_2含量低于60 wt％时，以无定型形式存在；当含量为80％时，出现锐钛矿型TiO_2，但与纯TiO_2相比晶型不完整：醋酸对Ti-Si复合氧化物的比表面积、晶型都有很大的影响；TiO_2含量为20％的20TiSi经1100℃高温焙烧后，仍有较高的比表面积(11m~2／g)，稳定性好，在较宽的温度范围内焙烧，没有引起Ti-O-Si键的断裂，分散度高，没有出现晶型TiO_2。

With the development of science and technology, sensitive, rapid, reproducible, simple and accurate analytical methods are required for the determination of trace elements in geological, biological and environmental samples. The direct determination of extremely low concentration of trace element with modern atomic spectroscopic method, such as atomic absorption spectrometry is so difficult. On one hand, the limitations are associated not only with the insufficient sensitivity of these techniques but also with matrix interference.

随着科学技术技术的发展，在进行地质、环境、生物等样品中痕量金属元素的测定时，常常要求达到ppb级的水平，虽然火焰原子吸收分光光度法具有很高的灵敏度，但是要直接测定这些样品中的痕量组分却很难，这是因为，一方面，样品本身的物理化学状态有的不适合直接测定，或组分的含量低于分析方法的灵敏度；另一方面是存在基体干扰。

The filled skutterudite compound possesses bcc structure as evidenced by electron diffraction analysis. Powder X-ray diffraction data of filled skutterudite samples were characterized by Rietveld method for some crystallographic parameters such as lattice constant, atomic occupation, atomic position, etc.

另外，通过对化合物电子衍射的分析证实了〓化合物是一种具有bcc结构的化合物；运用Rietveld方法对填充skutterudite化合物X衍射谱线进行了分析，对化合物的晶格常数、原子位置的占有率以及原子位置坐标等晶体学参数进行了表征。

Furthermore, the metallic glass samples are prepared by vacuum injection method and the rationality of above-mentioned relationships and RBF models is directly verified. It is shown that there are extremum phenomena between the Rc andΔd ,Δe and v respectively. However, the positions of the extremum are different from different alloy systems and the extremum phenomena may be related to the optimum composition region and the optimum additive quantity. More elements in the alloy are in favor of the improvement of the GFA. And as for the high GFA alloy, the atomic percentage, atomic radius difference and atomic electronegativity difference are harmoniously matched.

d、Δe和v与临界冷却速度Rc的关系中都出现极值现象，对于不同的合金体系，极值出现的位置不同；金属玻璃的最优成分范围以及各种添加元素的最佳添加量行为，可能与此极值现象相关；合金中包含的组元数目多有利于提高其玻璃形成能力，玻璃形成能力强的合金，其各个组元的原子百分含量、组元原子半径差及其电负性差之间的搭配是很和谐的；融合建模的合金系之间包含的主要组元数量和种类越相近，所建立的模型的可靠程度越高，其预测结果与实测结果越吻合。

With microwave digestion and general digestion , the content of Pb and Cd in shrimp samples was measured by graphite furnace atonic absorption spectrometry .

采用微波消解与常规消解2种方法消解对虾样品，石墨炉原子吸收法测定其Pb、Cd的含量，对样品中Pb、Cd的微波消解与常规消解分析方法做了系统的比较。

Research samples were limited to the attainability of integral financial information during the research period. Correlation Analysis and Multiple Regression Analysis were adopted as the verification methods to explore the influences of textile companies' attributions to their company capital structures.

研究样本以能取得研究期间内完整财务资料者为限，分别以相关分析法与多元回归分析法作为实证研究之方法，探讨纺织纤维业公司其不同属性对公司资本结构之影响。

Another approach in enhancing the light extraction efficiency of AlGaInP LED was accomplished using a surface roughening process. In this process, the Au(170 nm)/AuBe(260 nm)/Au(170 nm) ohmic contact layers were first deposited on the GaP window layer. After the alloy annealing process (480°C for 10 min), the Be atoms will diffuse into the GaP top layer and form non-uniform clusters. The LED samples were then immersed into a mixture 3H3PO4:1H2O2:1H2O solution for 6 min, resulting in a rough GaP surface. The luminous intensity of the AlGaInP LED can increase from 42 to 50 mcd, that is, an 18% enhancement can be achieved via the present non-photolithography surface roughening process.Keywords: LED, AlGaInP, Cu substrate, Reflector, Surface roughening

在实验的第二部份是开发磷化镓窗口层之粗化制程，我们是藉由正面金/铍欧姆接触电极之熔合制程，使铍扩散至磷化镓层，同时利用铍渗入磷化镓造成之特殊组成，可形成不均匀之蚀刻阻挡，而在磷化镓表面形成粗化，我们发现480℃、10分钟的熔合制程，加上浸泡磷化镓蚀刻溶液6分钟，可将四元发光二极体之发光亮度由42 mcd 提升到50 mcd，经由此无光罩粗化制程可将亮度提升18%，明显提升磷化铝铟镓发光二极体之外部量子效率。

Methods DNAs were isolated from antiagglutinated and agglutinated blood samples from auricular veins of 30 healthy subjects.

目的 寻找最佳的从血液尤其是凝血中提取DNA的方法，减少实验和临床检测血液的用量。

For this study, Sadee and his colleagues analyzed 68 autopsy samples of normal human brain tissue.

在此研究中，Sadee和他的同事对68个正常人脑组织进行了解剖和分析。

This indicates the volcanic rocks with the character of autunite alkalescence siries, LREE/HREE=4.31-14.60, with a mean value of 8.74,=3.72-16.16, with a mean value of 9.59, enrichment of LREE,δEu=0.61-1.11, with a mean value of 0.80, majority samples δEu.0, indicate Eu pronounced weak negative abnormalty or no pronounced Eu abnormally.

LREE/HREE=4.31~14.60，平均8.74，=3.72~16.16，平均9.59，具有LREE富集的特征，δEu=0.61~1.11，平均0.80，多数样品δEu.0，表明铕呈弱负异常或不显异常。

Chinese traditional virtue is humility and wariness,the compliment and praise to the others should be declination

中国人的传统美德是谦虚谨慎，对别人的恭维和夸奖应是推辞。如

We bought this house on the never-never.

我们以分期付款的方式买下这座房子。