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The effects of above-mentionedconditions on alkylene reaction are studied to obtain the optimum reactive conditionsby orthogonal experiments having seven factors and three levels. GCLE is chosen as material to prepare 7-phenyl acetamideyl vinyl cephalkyl acidp-methoxy benyl eatsr in the experiment. The process is as follow: GCLE reacts withiodide in solvent, and produce 3-iodid, then reacts with PPh_3 to produce Witting agent,and reacts with HCHO to produce 7-phenyl acetamideyl vinyl cephalkyl acid p-methoxy benyl eatsr in alkaline conditions.

试验选用GCLE作为原料制备7-苯乙酰氨基-3-乙烯基头孢烷酸对甲氧苄酯，反应过程如下：GCLE与碘化物、PPh3在溶剂中反应生成3位膦盐，在碱性条件下生成Wittig试剂再与HCHO反应生成7-苯乙酰氨基-3-乙烯基头孢烷酸对甲氧苄酯。

The control of the position of the liquid is very import in the course of the practice produce course, the height of the position of the liquid bring very import infection in the produce. It may influence the produce if the position of the liquid is too below, and it may overflowv if the position of the liquid is too high, it may course the attaint of the equipment, even conduce the casualty of the people!

液位控制在实际的生产过程中非常重要，液位的高低对生产有着重要的影响，液位太底可能影响正常的生产过程，而液位过高则可能出现溶液外溢，会造成设备的损坏，甚至人员的伤亡，给公司造成不可估量的损失！

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

The domestic demand of acetic acid up to 1,440,000-1,620,000 tons can be anticipated in 2010, if 60% is produced by methanol, 520,000 tons of methanol will be consumed;③Methanol can be used as feedstock to directly produce various pesticides ,such as fenitrothion, omethoate, dipterex etc., we anticipate that approximately 340,000 tons of methanol will be used to produce pesticides in 2010.④ Various medicines use methanol as feedstock, such as sulfanilamide, vitamin B6 etc., we anticipate that approximately 180,000 tons of methanol will be used to produce medicines in 2010.⑤ In the duration of dye production, methanol can be used as feedstock or solvent, such as s carlet base RC, disperse red GLZ, phthalocyanin ⑥ Synthetic resin also need methanol as feedstock such as organic glass, we anticipate that about 70,000 tons of methanol will be used to produce synthetic resin and plastics in 2010;⑦Synthetic fibers and synthetic rubber industry, will use methanol about 800,000 tons in 2010;⑧ At present, the production of MTBE is increase rapidly, there are 27 set of plants, total production capacity is 620,000 tons every year, and the demand is about 800,000 tons, there is gap between demand and supply.

预计2010年我国醋酸的需求量将达144～162万吨，按甲醇羰基法占60%计，将需求甲醇达52万吨；③多种农药的生产直接以甲醇为原料，如杀螟松、乐果、敌百虫等，预计到2010年甲醇用于生产农药约为34万吨；④多种医药药品以甲醇为原料，如长效磺胺、维生素B6等，预计到2010年甲醇用于医药约为18万吨；⑤染料生产过程中用甲醇作原料或溶剂，如红色基RC、分散红GLZ、阴率子GRL、酞菁素等等，预计2010年甲醇用量约为10万吨；⑥有机玻璃等合成树脂也需用甲醇为原料，预计到2010年甲醇用于生产合成树脂与塑料用量约为7万吨；⑦合成化纤与合成橡胶工业，2010年甲醇用量约为13万吨；⑧我国MTBE生产正处于快速增长期，现有MTBE装置27套，总生产能力62万吨/年，而年需求量约80万吨，有一定缺口。

The most suitable range of temperature is 25~30℃ and lethal temperature is 56℃ for hypha growth, the most suitable temperature is 25℃ for produce more conidiospore and lethal temperature is 56℃ for conidiospore. Within the pH range of 3~11 the hypha could grow and produce conidiospore. The optimum pH is 5~7 for hypha growth and 3, 9, 10 for produce more conidiospore. The range of glucose concentration is 2%~8% for hypha growth, the most suitable glucose concentration is 2% for hypha growth and produce more conidiospore. The effect of illumination on Bipolaris cynodontis was significance to the growth hypha and spore numbers. The whole light is advantage of hypha growth, but could not produce conidiospore. Alternation of light and darkness for 12 hours is advantage of hypha growth, as well as produce conidiospore.

菌丝最佳生长温度是25~30℃之间，在25℃时最利于产孢，菌丝生长和分生孢子的致死温度是56℃；该菌在pH 3~11范围内均能生长，产生分生孢子，菌丝生长的最适pH 5~7，产孢量最大的pH是3，9，10；糖浓度在2%~8%菌丝能生长，在糖浓度为2%时菌丝生长最好，产孢量最高；光照对病原菌的菌丝生长和产孢有明显影响，在全光照的条件下有利于菌丝的生长，但不会产孢，黑暗12h光照12h既利于菌丝生长又利于产孢，而全黑暗的条件下不利于菌丝生长和产孢。

Germany is one of developed country is stard work to aid already in the world , the produce occupy the well-developed level of the world , the exceptionally grand occasion is grasp in this exhibition , the scale attend the meeting stream of people in case pouring greatly , incalculable , joining an exhibition that produce science and technology content is tall , the produce was successfully open up before one's eyes of self in numerous joining an exhibition businesss that originate the various places in world , I carefully visited the heating heat sink produce , the produce type is diversified , the exterior is beautiful , technology is well-developed , I winden one's view the limit greatly , travels together also acclaim with one voice .

德国是世界上工业经济发达国家之一，产品居于世界先进水平，这次展览会盛况空前，规模大，到会人流如涌，数不胜数，参展产品科技含量高，来自世界各地的众多参展商成功展示了自己的产品，我仔细参观了采暖散热器产品，产品样式多样，外观靓丽，工艺先进，我大开眼界，同行们也交口称赞。我们以饱满的热情认真搜集了大量产品、技术工艺信息，展览会给参展商和八方宾朋提供了一个具有吸引力的打开国际市场的渠道，也是我们了解当前世界散热器产品发展的重要窗口。

The authentication by means of ISO9000-2001's grade quality assurance setup of corporation and effectively runs causes that corporation produce technique level and the quality grade all dwells domestic colleague's trade first place , the rich special subject of technical personnel pestles an organization , yet each year wholly continuously puts out the fresh produce to meet the actual and latent demand that the vacuum tube produce was adjust in the wide door in the past few years , the different main economic target of corporation all increases by degrees with velocity over 30%, and the multiple items produce captures the province grade scientific and technical payoffs reward , and that the business is awardded the high and new technique business name corporation in Liaoning shall steadfast that the earth with shopper is fundamental , and administer with continuously to innovate by means of the scientific knowledge , and in the interest of the marketplace suppling the service of international quality produce and classic with all one's heart , to supply the well-developed quality of performance the dependable high grade produce in the interest of consumer is the target that the corporation was pursue .

公司通过ISO9000-2001级质量保证体系的认证和有效运行。使得公司产品的技术水平和质量档次均居国内同行业首位，技术力量雄厚的专业研发机构，每年都不断推出新产品来满足广大可户对电子管产品的现实和潜在的需求。近年来，公司各主要经济指标均以30%以上的速度递增，多项产品获省部级科技成果奖励，企业被授予辽宁省高新技术企业称号。公司将始终不渝地以顾客为根本，通过科学管理和不断创新，竭诚为市场提供国际品质的产品和一流的服务。为用户提供性能先进质量可靠的优质产品是公司追求的目标。

The construction in the future: 6 produce 10000 tons of HFC-152a, the substitute of ODS and 4000 tons of HCFC-142b a year; 7 produce 7000 tons of HCFC-123 and 3000 tons of-113a; 8 build PEVE rosin production with annual output of 5000 tons; 9 produce 3000 tons of PVDF a year; 10 produce 2000 tons of fluorobenzene and 1000 tons of dichlor fluorbenzene a year; and 11 fluoride salt combine device with annual output of 3000 tons.

远期建设：6、ODS替代品HFC-152a年产1万吨联产HCFC-142b4000吨；7、年产HCFC-123产品7000吨、联产二氯三氟乙烷-113a产品3000吨；8、年产PEVE树脂5000吨生产线；9、年产3000吨PVDF氟碳涂料树脂；10、年产2000吨氟苯，二氯氟苯1000吨；11、年产3000吨氟化盐联产装置。

The new great machine factory of BeiHAI is a professional factory producing fish meal complete sets of wet law of our country, since founding the factory, is it process equipment with domestic research institution , fish meal expert of trade to tropical fish and inferior tropical complete wet law fish meal of fish to develop together, there are 30 tons , 50T , 80T , 150T , many kinds of specifications , by land , can all use on the ships, and 30T can produce 50T , 50T and can produce 70T , 80T can produce 100T , 150T can produce 200T , the production technology has reached or exceeded the domestic like product, is well received by many customers.

北海新宏机械厂是我国专业生产湿法鱼粉成套设备的厂家，建厂以来，与国内研究机构、鱼粉行业的专家共同开发了针对热带鱼和亚热带鱼类的全套湿法鱼粉加工设备，有30吨、50T、80T、150T、多种规格，在陆上，船上都可使用，而且30T能生产50T、50T能生产70T，80T能生产100T，150T能生产200T，生产技术达到或超过了国内同类产品，受到多家客户好评。

The speed of produce tin,the time return tin,the interval time of produce tin can be adjusted steady and with tin back adjustable features,which can reduce the waste of welding 3 the mode of produce tin mode: automatic and manual produc tin for the selection of tin (produce tin manually can match a tin foot switch or manual switch out of tin), and the number of the tin can be set 4 all of the settings using DIP switch settings, easy to operate; 5 anti-static design can avoid sensitive electronic components damaged due to static electricity and 6 optional universal bracket solder 7 simple and easy welding to reduce the welding welding achieve the desired effect of waste, improve efficiency significantly.

产品说明Product description；1）采用步进电机，出锡精确且可灵活控制。2出锡速度、出锡量、回锡时间，出锡间隔时间均可调节且稳定，且设有可调的回锡功能，以减少焊接的浪费3出锡模式：全自动出锡与手动出锡可供选择（手动出锡可选配脚踏出锡开关或手动出锡开关），且出锡次数可设置4所有设置采用拨码式开关设置，方便操作；5防静电设计，能避免敏感电子零件因静电而受损坏6可选装万能焊锡支架7焊接简单容易、减少焊接的浪费达到理想焊接效果，工作效率显著提高。

For those who choose to go with Scryer, the main perks of aligning your character with them is the added critical strike rating once you gain enough reputation with them.

如果说王小波的作品是茶，那么对不起，只能说他心中都是茶，不是王小波改行当了采茶女。

The secret is not to "think" about the thoughts but to allow them to flow through your mind,while keeping your mind free of afterthoughts.

其中的诀窍就是不要去&想&念头，让它流贯心头，保持心的自由和开放。