查询词典 distillation method

TEM shows that drying by direct heating might result in hard aggregation of the tourmaline powder, while hard aggregation might be avoided by azeotropic distillation. Raman spectroscopy reveals that there are O_H and C_H on the surfaces of the tourmaline powder obtained by azeotropic distillation, which indicates that butoxy is chemically adsorbed on the surfaces of tourmaline particles, but not adsorbed on those formed by direct drying. X_ray powder diffraction shows that the intensity of diffraction peaks decreases after grinding. There is no damage to the tourmaline crystal lattice in the process of direct heating, azeotropic distillation, or ultrafine grinding.

透射电镜分析结果表明，直接加热脱去水或正丁醇会使电气石超细颗粒发生硬团聚，而共沸蒸馏法则可有效防止硬团聚的产生；拉曼光谱结果表明，共沸蒸馏法制备的电气石粉末表面存在O—H和C—H键，说明正丁醇在颗粒表面为化学吸附，而直接干燥法得到的电气石粉末表面则没有；X射线粉晶衍射结果表明，研磨过程降低了粉末衍射峰的强度，但直接加热干燥和共沸蒸馏干燥均未破坏电气石的晶格结构。

The invention relates to a dynamic matrix control system of high-purity distillation, which comprises distillation tower, intelligent checker, DCS system, superior host, and on-site bus, while they are connected. The control system uses tower product group as the object variable, and the reflux ratio and reboil ratio as control variable; the superior receives history temperature and pressure data from the DCS real-time database, via the predict control and dynamic matrix controller, to obtain the output values of present controller as reflux ratio and reboil ratio, then feedback said two values to DCS system, to function the distillation object. The invention can confirm the high-purity stable operation, with better dynamical control.

本发明公开了一种高纯精馏的动态矩阵控制系统和方法；系统包括：精馏塔、智能检测仪表、DCS系统、上位机和现场总线；所述精馏塔、智能检测仪表、DCS系统和上位机通过现场总线依次相连，实现信息流的上传和下达；本发明所涉及的控制系统采用塔双端产品组分为被控变量，回流比和再沸比为对应的控制变量；上位机从DCS实时数据库中获得历史的温度、压力等数据，通过推断控制环节和动态矩阵控制器环节，得到当前控制器的输出值-回流比和再沸比，再把控制器输出值返回给DCS系统，实现了对高纯精馏过程的双端产品高纯控制，对双端组分的高纯度平稳操作，具有很好的动态品质和控制效果。

Molecular Distillation, also termed as Short Path Distillation, is a special distillation technology.

分子蒸馏也称短程蒸馏，是一种特殊的蒸馏分离技术。

In this paper Ⅰ successfully applied these methods to fault diagnosis, and presenting some new innovative machinery fault diagnosis method; First Ⅰ present a new gear wornout fault diagnosis method, this method use the vibration signal's time-frequency attribute and instantaneous phase undulation to accurately detect gear's fault, and by comparing with the traditional frequency domain analysis method, this method reveals that many nonlinear and nonstationary characteristic exist in gear's vibration, this tell us that if we use frequency domain analysis method without pay attention to the signal's characteristic, we could get wrong diagnostic result; Then Ⅰ present a new bearing fault diagnosis method, this method use ATVFD and Hilbert transform to do envelop demodulation,Ⅰ analyze the envelop with time-frequency method and find out that this method is more accurate then traditional method.Ⅰ also explain that the modulation of the fault to the carrier wave may also be non-stationary and nonlinear; Finally Ⅰ present a cylinder pressure measurement method of diesel engine by means of vibration, cylinder pressure is an important parameter of diesel engine fault diagnosis, the pressure measuring is simplified a lot by this method,Ⅰ also use the ATVFD and time-frequency analysis to realize it.

本文中将上述理论方法成功地应用到故障诊断中去，提出了几点创新性的诊断方法；提出了一种齿轮磨损故障诊断的新方法，该方法利用振动信号能量的时频域分布特征与瞬时相位波动特征可以进行精确的齿轮故障诊断，并通过与传统的频域诊断方法的比较，揭示出齿轮振动中存在的明显的非线性与非平稳特征，说明了不加选择地利用频域分析方法进行齿轮故障诊断很可能会得到错误的诊断结果；提出了一种轴承故障诊断的新方法，该方法利用ATVFD分解与Hilbert变换进行包络解调，并对解调得到的包络信号进行时频域分析，可以实现更加准确轴承故障诊断，说明了故障对载波信号的调制往往也是非平稳与非线性的；提出了一种利用振动信号进行柴油机汽缸内压力检测的新方法，柴油机汽缸压力的变化是柴油机故障诊断的重要参数，利用振动方法可大大简化汽缸压力的检测过程，该方法也是综合利用ATVFD分解与时频域分析方法实现的。

This train classifies "information carrier adhering to the build" as design elements, and probes into integrated design method of it and single building separately: method of definite position, method of definite form and method of combination; Then, this train probes into integrated design method of it and colonys building , that bases on the cognitive design method: method of rhythm controls,method of node outstanding, and that aims at the design method to protect: method of protect original, method of repairing and method of renewal.

本文的第四部分提出了一体化设计的思路，将建筑附着信息载体作为设计元素，探讨了它与建筑单体一体化设计的方法：定位法、定形法、混合法；以及它与建筑群体一体化设计时，基于认知的设计方法：节奏控制法、节点突出法，旨在保护的设计方法：存真法、修缮法、更新法。

The Bidiagonal matrix method for the simulation of distillation and catalytic distillation is developed. The bidiagonal matrix method is proved to be better in convergcnce and stability by compared with the tridiagonal matrix method.

在多组分精馏塔的稳态模拟计算中，三对角矩阵法具有占用计算机内存少，无需计算偏导数矩阵等优点，但对强非理想性体系有时计算不收敛。

The test method is to fetch the urea of the same quality and coated material of different quality first, make coating material parcel evenly the urea particle s surface, grant them into the soil, eluviate with the distilled water every 24 hours, collect the eluviationing solution, titrate the eluviationing solution with distillation titrimetric method, that is, add alkali distillation, make the ammonia release out, absorb with boric acid solution, then titrate it with standard acid.

试验方法是称取相同质量的尿素和不同质量的包膜材料，将包膜材料均匀地包裹在尿素颗粒的表面，将包裹后的包膜肥料施入模拟试验的土壤中，每隔24个小时用蒸馏水淋溶，收集淋溶液，用蒸馏滴定法滴定淋溶液，即加碱蒸馏，使氨释放出来，用硼酸溶液吸收，而后用标准酸滴定之。

Firstly, this paper investigated roundly the basic theory of the ambient vibration method, analyzed systematically the main methods of ambient vibration identification, and discussed their advantages and disadvantages. Then we established the finite element model of structural dynamics and test model and analyzed their mutual relation, improved MUSIC method and correlation function method in the harmonic identification, and gave the subspace method and correlation function method based on continuous model, which is multi-harmonic retrieve technique. And then, this paper also puts forward least-squares method to estimate directly structural physical and modal parameters; this approach replaced the derivative operator in the continuous time model with an equivalent approximation, and estimated the physical parameters of structures by the least-squares method. And then, we discussed the approximation methods of derivative and their convergence. Finally, this paper researched the modal parameters of a frame structure by the simulation and test. The results demonstrated that subspace method, correlation function method and the least-squares method are effective and stable respectively.

全面地研究环境振动识别方法的基本理论，系统地分析环境振动识别方法的主要方法，讨论它们的优点和不足；建立结(来源：6666AB44C论文网www.abclunwen.com)构动力学的有限元模型和试验模型，分析有限元模型与试验模型之间的相互关系；改进谐波识别中的MUSIC识别方法和相关函数识别方法，给出大型结构模态识别的连续型的子空间分解识别方法和相关函数识别方法，这个方法是多元谐波识别方法；提出直接识别结构的物理参数和模态参数的最小二乘方法，这个方法利用导数的近似值代替导数值，并运用最小二乘方法识别结构的物理参数，讨论导数近似值的选择方法，分析算法的收敛性；通过仿真计算和模型实验，研究高层框架结构的模态参数识别，验证子空间分解识别方法、相关函数识别方法和最小二乘识别方法的有效性，算法的稳定性；从理论和试验两个方面分析和研究噪声对识别精度的影响，影响识别精度的因素，以及部分模态成分的模态参数不能够被识别的原因。

The revised Hargraves formula has the best result compared with Penman-Monteith formula, the average relative error is 6%, moreover, Hargaves method requiring the least data in calculating ETo, so this method has the high actual application value; The following are Radiation method and Blaney-Criddle method ; The worst is the Pan method, even after revised, the highest and average relative error is 36% and 10%, respectively. So, in this study, Penman-Monteith method, Radiation method, Blaney-Criddle method and Hargraves method are used except Pan method.

在这四种方法中，修正后的Hargraves方法与彭曼—蒙特斯方法的计算结果符合最好，其平均相对误差为6％，而Hargraves方法需要的气象数据只有计算时段的最高、最低温度，该方法具有较高的实际应用价值；辐射方法和布兰尼—克里德尔方法次之；蒸发皿方法最差，即使在修正后，E601型蒸发皿的最大误差也高达36％，平均为10％，所以在预报系统的研究设计中采用了除蒸发皿方法之外的四种方法。

The primary studying works and characteristics:1 To summarize reinforcing theory of cement mixing pile composite foundation2 To analyze the primary mechanics characters and changing rules of cement mixing pile, based on analysis of test data both indoor and outdoor.3 To discuss siding frictional resistance, ending resistance, ultimate bearing capacity of simple mixing pile and effectiveness factor of grouped piles, loading ratio of soil between piles under cushion cap of grouped piles and stress ratio of pile and soil and so on, and use many computation method and experimentation method to ensure bearing capacity of mixing piles composite foundation.4 To point out and analyze eight sides flaws and problems of the bearing capacity calculation method of mixing pile compositefoundation which ensured by national and normative method/ formula.5 To apply test results of loading tests and a few settlement observation data, use gray theory to predicate ultimate bearing capacity of deep mixing piles, actual example demonstrate engaging between theoretical predicted value and actual value.6 To apply groovy layerwise summation method to discuss entity piles method, double foundation method, equivalent layerwise summation method and consolidation theoretical method and so on, especially by combination of engineering example, use FEM to calculate or discuss the settlement and changing rules of composite foundation.7 To discuss problems of critical length of composite foundation by combination of engineering example and numerical analysis method, and analyze the contrast of critical length between simple pile load and most area load of composite foundation, not only critical length of composite foundation is relative to modulus ratio between piles and soil, but also upside load distribution area of composite foundation.

主要的研究工作与特色为：(1)总结了水泥搅拌桩复合地基的加固原理；(2)在对室内外试验资料进行统计分析的基础上，系统分析了搅拌桩水泥土的主要力学特性及其变化规律；(3)探讨了搅拌单桩的侧摩阻力、端阻力、极限承载力及群桩效率系数、群桩承台下桩间土荷载分担比及桩土应力比等，提出用多种计算方法并结合试验方法来综合确定搅拌桩复合地基的承载力；(4)明确指出和分析了按国家有关规范的方法确定搅拌桩复合地基承载力所存在的八个方面的缺陷与问题；(5)利用过去没有加载至破坏阶段的载荷试验成果和较少的沉降观测数据，尝试了用灰色理论预测深层搅拌桩的极限承载力，实例表明理论预测值与实测值吻合较好；(6)在常规分层总和法的基础上，探讨了复合地基沉降计算的实体墩基法、双层地基法、等效作用分层总和法、固结理论法等，特别是结合工程实例，用有限元数值计算等方法计算和讨论了搅拌桩复合地基的沉降及其变化规律；(7)结合工程实例，用数值分析方法探讨了复合地基临界桩长的问题，指出和分析了单桩荷载下的临界桩长与复合地基大面积荷载下的临界桩长存在很大的差别，复合地基的临界桩长不仅与桩土模量比有关，而且与复合地基上部荷载分布面积有关。

When this condition occurs, inbound replication with the source partner is stopped on the destination domain controller and event ID 2042 is logged in the Directory Services event log.

计算机密码学是研究计算机信息加密、解密及其变换的科学，是数学和计算机的交义学科，也是一门新兴的学科。

Instructions: click on the thumbnails to see a larger image, then use the left-right arrow keys to scroll through the slideshow.

使用说明：滑鼠点在小图上即可放大观赏。开启后键盘左右键可用来换照片。